Ultrafast synthesis of crystalline Cu 2 ZnSnS 4 nanoparticles by solid state microwave heating technique and study of their electrochemical behavior

AbstractThe synthesis of the tri-coordinated ferrocenecarbonitrile silver(I) complex [Ag(N≡CFc)3]OTf (3) is reported. Its electrochemical behavior shows that the three ferrocenyl units are oxidized in a very close potential range. In addition, the molecular structure of 3 in the solid state is discussed, showing that silver(I) is exclusively coordinated by three ferrocenecarbonitrile molecules.

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Thiol end-capped titanium–copper complexes: Synthesis, solid state structure and electrochemical behavior

Inorganica Chimica Acta ◽

10.1016/j.ica.2007.03.012 ◽

2008 ◽

Vol 361 (6) ◽

pp. 1659-1667 ◽

Cited By ~ 6

Author(s):

Heinrich Lang ◽

Katrin Rößler ◽

Deeb Taher ◽

Rudolf Holze ◽

Bernhard Walfort

Keyword(s):

Solid State ◽

Electrochemical Behavior ◽

Copper Complexes ◽

State Structure ◽

Solid State Structure

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Self-supported multidimensional Ni–Fe phosphide networks with holey nanosheets for high-performance all-solid-state supercapacitors

Journal of Materials Chemistry A ◽

10.1039/c9ta04832d ◽

2019 ◽

Vol 7 (29) ◽

pp. 17386-17399 ◽

Cited By ~ 13

Author(s):

Shuo Li ◽

Minghao Hua ◽

Yuan Yang ◽

Wei Huang ◽

Xiaohang Lin ◽

...

Keyword(s):

Solid State ◽

Dft Calculations ◽

Electrochemical Behavior ◽

High Performance

Comprehensive research of the chemosynthesis, electrochemical behavior and DFT calculations of a multidimensional Ni–Fe–P electrode for all-solid-state supercapacitors.

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Microwave-assisted solid-state synthesis of NaRE(MO4)2 phosphors (RE = La, Pr, Eu, Dy; M = Mo, W)

Dalton Transactions ◽

10.1039/d0dt00999g ◽

2020 ◽

Vol 49 (23) ◽

pp. 7914-7919 ◽

Cited By ~ 1

Author(s):

S. Sameera Perera ◽

Hashini N. Munasinghe ◽

Emily N. Yatooma ◽

Federico A. Rabuffetti

Keyword(s):

Rare Earth ◽

Solid State ◽

Metal Ions ◽

Microwave Heating ◽

Rare Earth Metal ◽

Earth Metal ◽

Double Molybdate ◽

Microwave Assisted ◽

Double Tungstate ◽

Phase Pure

Microwave heating provides rapid access to crystalline and phase pure double molybdate and double tungstate phosphors activated by rare-earth metal ions.

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Cover Feature: Ru II and Ru III Chloronitrile Complexes: Synthesis, Reaction Chemistry, Solid State Structure, and (Spectro)Electrochemical Behavior (Z. Anorg. Allg. Chem. 22/2020)

Zeitschrift für anorganische und allgemeine Chemie ◽

10.1002/zaac.202070222 ◽

2020 ◽

Vol 646 (22) ◽

pp. 1783-1783

Author(s):

Sebastian Scharf ◽

Eduard Kovalski ◽

Tobias Rüffer ◽

Alexander Hildebrandt ◽

Heinrich Lang

Keyword(s):

Solid State ◽

Electrochemical Behavior ◽

Synthesis Reaction ◽

State Structure ◽

Solid State Structure

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Synthesis and Microstructural Control of In2O3(ZnO)3 Layered Compound by Microwave-Heating

Materials Science Forum ◽

10.4028/www.scientific.net/msf.620-622.85 ◽

2009 ◽

Vol 620-622 ◽

pp. 85-88 ◽

Cited By ~ 3

Author(s):

Shouhei Yanagiya ◽

Yamato Hayashi ◽

Hirotsugu Takizawa

Keyword(s):

Solid State ◽

Microwave Heating ◽

Band Gap Energy ◽

Layered Compound ◽

Bottom Part ◽

Heated Sample ◽

Powder Bed ◽

Silica Substrate ◽

State Diffusion ◽

Plane Direction

In2O3(ZnO)3 layered compound was synthesized by 2.45 GHz microwave heating in a solid state reaction. Microwave-processed samples were obtained at low temperature by the enhancement of solid state diffusion and sublimation of the powder bed. Plate-like grain microstructures formed on the bottom part of the pellet, and vicinity of the surface was dense. The plate-like grain was oriented in the ab-plane direction. Compared with a conventional heated sample, the electrical conductivity increased and the band gap energy decreased. In the case of deposition on a silica substrate by microwave heating, the plate-like grain film was synthesized.

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