Effect of heat treatment and hot isostatic pressing on the microstructure and mechanical properties of Inconel 625 alloy processed by laser powder bed fusion

2017 ◽  
Vol 689 ◽  
pp. 1-10 ◽  
Author(s):  
Alena Kreitcberg ◽  
Vladimir Brailovski ◽  
Sylvain Turenne
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Hot Isostatic Pressing ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Isostatic Pressing ◽  
Microstructure And Mechanical Properties ◽  
Inconel 625 Alloy

scholarly journals Structure and Properties of Ti/Ti64 Graded Material Manufactured by Laser Powder Bed Fusion

Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6140
Author(s):  
Evgenii Borisov ◽  
Igor Polozov ◽  
Kirill Starikov ◽  
Anatoly Popovich ◽  
Vadim Sufiiarov
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
Hot Isostatic Pressing ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Isostatic Pressing ◽  
Graded Material ◽  
Single Part

Multimaterial additive manufacturing is an attractive way of producing parts with improved functional properties by combining materials with different properties within a single part. Pure Ti provides a high ductility and an improved corrosion resistance, while the Ti64 alloy has a higher strength. The combination of these alloys within a single part using additive manufacturing can be used to produce advanced multimaterial components. This work explores the multimaterial Laser Powder Bed Fusion (L-PBF) of Ti/Ti64 graded material. The microstructure and mechanical properties of Ti/Ti64-graded samples fabricated by L-PBF with different geometries of the graded zones, as well as different effects of heat treatment and hot isostatic pressing on the microstructure of the bimetallic Ti/Ti64 samples, were investigated. The transition zone microstructure has a distinct character and does not undergo significant changes during heat treatment and hot isostatic pressing. The tensile tests of Ti/Ti64 samples showed that when the Ti64 zones were located along the sample, the ratio of cross-sections has a greater influence on the mechanical properties than their shape and location. The presented results of the investigation of the graded Ti/Ti64 samples allow tailoring properties for the possible applications of multimaterial parts.

scholarly journals On the Hot Isostatic Pressing of Inconel 625 Structures built using Laser Powder Bed Fusion at Higher Layer Thickness

2021 ◽  
Author(s):  
Saurav Kumar Nayak ◽  
Arackal Narayanan Jinoop ◽  
Christ Prakash Paul ◽  
Vesangi Anil Kumar ◽  
Dineshraj Subburaj ◽  
...  
Keyword(s):  
Layer Thickness ◽  
Volume Fraction ◽  
Hot Isostatic Pressing ◽  
Microstructural Analysis ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Isostatic Pressing ◽  
Elemental Segregation

Abstract This paper reports the effect of Hot Isostatic Pressing (HIPing) on the porosity, microstructure and mechanical properties of Laser Powder Bed Fusion (LPBF) IN625 structures built at a higher layer thickness of 100 µm. It is observed that the process-induced pores/voids of volume fraction (Vf) 0.43% in as-built IN625 structures are reduced significantly to ~ 0.01% after HIPing treatment. The microstructure is changed from fine columnar dendrites to coarse equiaxed dendrites. The microstructural analysis of as-built structures reveals the presence of cellular/ dendritic growth along with elemental segregation of Nb, Si and C and precipitation of Nb-rich carbides. Whereas, coarse recrystallized microstructure along with elemental segregation of Si and precipitation of Nb, Mo and Cr rich carbides are observed in Hot Isostatic Pressed (HIPed) samples. HIPed structures exhibit lower tensile s trength, higher ductility, and lower anisotropy as compared to LPBF built structures. There is a reduction in the Vickers micro-hardness of IN625 samples after HIPing and the values are observed to be similar to their conventional counterparts. Further, an increase in the energy storage capacity of the material is observed after HIPing treatment through Automated Ball Indentation (ABI®) studies. The study paves a way to develop ~100% dense, defect-free and isotropic engineering components using LPBF.

scholarly journals Hot Isostatic Pressing of Aluminum–Silicon Alloys Fabricated by Laser Powder-Bed Fusion

Technologies ◽  
2020 ◽  
Vol 8 (3) ◽  
pp. 48
Author(s):  
Stephan Hafenstein ◽  
Leonhard Hitzler ◽  
Enes Sert ◽  
Andreas Öchsner ◽  
Markus Merkel ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Supersaturated Solid Solution ◽  
Hot Isostatic Pressing ◽  
Powder Bed Fusion ◽  
Solution Annealing ◽  
Laser Powder Bed Fusion ◽  
Sand Cast ◽  
Powder Bed ◽  
Isostatic Pressing ◽  
Direct Aging

Hot isostatic pressing can be utilized to reduce the anisotropic mechanical properties of Al–Si–Mg alloys fabricated by laser powder-bed fusion (L-PBF). The implementation of post processing densification processes can open up new fields of application by meeting high quality requirements defined by aircraft and automotive industries. A gas pressure of 75 MPa during hot isostatic pressing lowers the critical cooling rate required to achieve a supersaturated solid solution. Direct aging uses this pressure related effect during heat treatment in modern hot isostatic presses, which offer advanced cooling capabilities, thereby avoiding the necessity of a separate solution annealing step for Al–Si–Mg cast alloys. Hot isostatic pressing, followed by rapid quenching, was applied to both sand cast as well as laser powder-bed fused Al–Si–Mg aluminum alloys. It was shown that the critical cooling rate required to achieve a supersaturated solid solution is significantly higher for additively manufactured, age-hardenable aluminum alloys than it is for comparable sand cast material. The application of hot isostatic pressing can be combined with heat treatment, consisting of solution annealing, quenching and direct aging, in order to achieve both a dense material with a small number of preferred locations for the initiation of fatigue cracks and a high material strength.

scholarly journals Multi-Laser Powder Bed Fusion Benchmarking—Initial Trials with Inconel 625

2019 ◽  
Vol 105 (7-8) ◽  
pp. 2891-2906 ◽  
Author(s):  
H. Wong ◽  
K. Dawson ◽  
G. A. Ravi ◽  
L. Howlett ◽  
R. O. Jones ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Production Rate ◽  
Single Mode ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Single Laser ◽  
Stress Relieving

Abstract Production rate is an increasingly important factor in the deployment of metal additive manufacturing (AM) throughout industry. To address the perceived low production rate of metal AM systems based on single-laser powder bed fusion (L-PBF), several companies now offer systems in which melting has been parallelised by the introduction of multiple, independently controlled laser beams. Nevertheless, a full set of studies is yet to be conducted to benchmark the efficiency of multi-laser systems and, at the same time, to verify if the mechanical properties of components are compromised due to the increase in build rate. This study addresses the described technology gaps and presents a 4-beam L-PBF system operating in “single multi” (SM) mode (SM-L-PBF) where each of the four lasers is controlled so that it melts all of a particular components’ layers and produces specimens for comparison with standard L-PBF specimens from the same machine. That is all four lasers making all of some of the parts were compared to a single-laser manufacturing all of the parts. Build parameters were kept constant throughout the manufacturing process and the material used was Inconel 625 (IN625). Stress-relieving heat treatment was conducted on As-built (AB) specimens. Both AB and heat-treated (HT) specimen sets were tested for density, microstructure, tensile strength and hardness. Results indicate that the stress-relieving heat treatment increases specimen ductility without compromising other mechanical properties. SM-L-PBF has achieved a build rate of 14 cm3/h when four 200 W lasers were used to process IN625 at a layer thickness of 30 μm. An increase in the build rate of 2.74 times (build time reduction: 63%) has been demonstrated when compared to that of L-PBF, with little to no compromises in specimen mechanical properties. The observed tensile properties exceed the American Society for Testing Materials (ASTM) requirements for IN625 (by a margin of 22 to 26% in the 0.2% offset yield strength). Average specimen hardness and grain size are in the same order as that reported in literatures. The study has demonstrated that a multi-laser AM system opens up opportunities to tackle the impasse of low build rate in L-PBF in an industrial setting and that at least when operating in single mode there is no detectable degradation in the mechanical and crystallographic characteristics of the components produced.

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