microstructural analysis
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Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 581
Author(s):  
Se-Beom Oh ◽  
Jongbeom Kim ◽  
Soon-Woo Han ◽  
Kyung-Mo Kim ◽  
Dong-Seok Yun ◽  
...  

Coal-fired power plants operating under Korea’s standard supercritical pressure operate in a high-temperature environment, with steam temperatures reaching 540 °C. A standard coal-fired power plant has a 30-year design life, and lifespan diagnosis is performed on facilities that have operated for more than 100,000 h or 20 years. Visual inspection, thickness measurements, and hardness measurements in the field are used to assess the degree of material degradation at the time of diagnosis. In this study, aging degradation was assessed using an electromagnetic acoustic transducer to measure the change in transverse ultrasonic propagation speed, and the results were compared to microstructural analysis and tensile test results. Based on the experimental results, it was found that the boiler tube exposed to a high-temperature environment during long-term boiler operation was degraded and damaged, the ultrasonic wave velocity was reduced, and the microstructural grains were coarsened. It was also confirmed through tensile testing that the tensile and yield strengths increased with degradation. Our findings prove that the degree of change in mechanical properties as a function of the material’s degradation state is proportional to the change in ultrasonic wave velocity.


CORROSION ◽  
10.5006/3961 ◽  
2022 ◽  
Author(s):  
Lisa Blanchard ◽  
Kasra Sotoudeh ◽  
James Hesketh ◽  
Gareth Hinds ◽  
Hongbiao Dong

The quantified microstructural analysis carried out on a wrought and a hot isostatically-pressed (HIP) UNS S31803 duplex stainless steel (DSS) in the Part 1 publication of this study 1, established the significance of the three-dimensional (3D) distribution and morphology/geometry of the ferrite and austenite phases on hydrogen transport through two DSS product forms. This paper is a follow-on to Part 1, and focuses on the role of the other two key, interrelated components of hydrogen-induced stress cracking (HISC): stress/strain, and hydrogen. For this purpose, experimental hydrogen permeation measurements, and environmental fracture toughness testing (i.e. J R-curve testing) using conventional and non-standard single-edge notched bend test specimens were used. These particularly enabled interpretation of the hydrogen permeation and transport test data, and evaluation of suitability of environmental fracture toughness test methods for the assessment of resistance to HISC in DSSs. The latter is discussed, both from laboratory and component integrity perspectives, in the context of the findings from the 3D microstructural characterisation of the two phases, the role of stress raisers and their severity, and hydrogen transport through the bulk and from the surface.


Geofluids ◽  
2022 ◽  
Vol 2022 ◽  
pp. 1-14
Author(s):  
Xiao Feng ◽  
Chong Xia ◽  
Sifeng Zhang ◽  
Chuangui Li ◽  
Hongkui Zhao ◽  
...  

In the treatment of goafs in traffic engineering, technical problems such as those related to large-volume grouting and the precise control of material properties are often encountered. To address these issues, we developed a new composite material comprising cement-fly ash-modified sodium silicate (C-FA-MS). The setting time, fluidity, unconfined compressive strength, and microstructure were varied for different proportions of cement-sodium silicate (C-S) slurry, cement-fly ash-sodium silicate (C-FA-S) slurry, and C-FA-MS slurry, and their performances were compared and analysed. The experimental results showed that the initial setting time of the slurry was the shortest when both the original sodium silicate volume ratio ( V S ) and modified sodium silicate volume ratio ( V MS ) were 0.2. The final setting time of the C-S and C-FA-S slurries tended to decrease but then increased with decrease in V S , while that of the C-FA-MS slurry increased with lower V MS . The fluidity of the C-FA-S and C-FA-MS slurries decreased with decrease in V S or V MS at different fly ash admixture ratios. The consolidation compressive strength of C-S increased with decreasing V S , while that of C-FA-S showed a considerable increase only when V S decreased from 0.4 to 0.2. Meanwhile, the compressive strength of the C-FA-MS concretions first increased and then decreased with decrease in V MS . Microstructural analysis revealed that there were more cracks in the C-S agglomerate, the fly ash in the C-FA-S agglomerate reduced the relative density of the skeletal structure, and the stronger cross-linking in the C-FA-MS agglomerate improved the strength of the agglomerate. Under the condition of unit grouting volume, the cost of the C-FA-MS slurry was approximately 44.7% and 31.3% lower than that of the C-S and C-FA-S slurries, respectively. The new C-FA-MS material was applied for the treatment of the goaf in the Wu Sizhuang coal mine. Core drilling detection and audiofrequency magnetotelluric survey revealed that the goaf was sufficiently filled.


2022 ◽  
Vol 327 ◽  
pp. 197-206
Author(s):  
Pietro Tonolini ◽  
Annalisa Pola ◽  
Lorenzo Montesano ◽  
Marialaura Tocci ◽  
Marcello Gelfi ◽  
...  

In this paper, wear properties of samples manufactured using thixocasting were compared with those of components obtained using low-pressure die-casting and additive manufacturing in order to assess the relationship between material performance and production technologies, both conventional and innovative. The investigated items were made with AlSi7Mg alloy. First, microstructural analysis and hardness measurements were carried out. Subsequently, pin-on-disk wear tests were performed. Wear behavior of the samples was studied considering both coefficient of friction and wear rate, while the damage mechanism was analyzed by observation of the worn paths using scanning electron microscope, correlating the behavior to the specific microstructure. In addition, the effect of selected heat-treated conditions, relevant for real applications, on wear properties was also evaluated.


2022 ◽  
Author(s):  
Tuhin Biswas ◽  
Narayan Bose ◽  
Dripta Dutta ◽  
Soumyajit Mukherjee

Interest in hydrocarbon exploration from the the Lesser Himalayan Sequence (LHS) has recently been revived amongst petroleum geoscientists. Understanding the paleostress regime and the deformation processes are the two important steps to understand the structural geology of any (petroliferous) terrane. Arc-parallel shear is an integral deformation process in orogeny. The scale of the consequent deformation features can range from micro-mm up to regional scale. Unlike orogen-perpendicular shear, different driving forces can produce orogen-parallel shears. We review these mechanisms/theories from several orogens including the Himalaya and compile 44 locations worldwide with reported orogen-parallel shear. Due to continuous crustal shortening by the India-Eurasia collision, the squeezed rock mass at the plate interface has produced the Himalayan Mountain chain. In addition, the rock mass also escapes laterally along the orogenic trend. Tectonic stress-field governs this mass flow. Field study and microstructural analysis in the northwest LHS (India) reveals orogen-parallel brittle and ductile shear movement. Y- and P- brittle shear planes, and the S- and C- ductile shear planes reveal the following shears documented on the ~ NW-SE trending natural rock selections: (i) top-to-NW up, (ii) top-to-SE up, (iii) top-to-NW down, and (iv) top-to-SE down. Our paleostress analysis indicates top-to-SE down and top-to-NW down shears occurred due to stretching along ~ 131°-311° (Dext), whereas top-to-SE up and top-to-NW up shear fabric originated due to shortening along ~133.5°-313.5° (Dcompr). Previous authors considered that the orogen-parallel extension generated ~ 15-5 Ma due to vertical thinning of the Himalaya. The NE-trending Delhi-Haridwar Ridge below the LHS plausibly acted as a barrier to the flowing mass and piled up the rock mass in the form of NW-SE/orogen-parallel compression. The NW-SE compression can be correlated with the D3 of Hintersberger et al. (2011) during ~ 4-7 Ma.


2022 ◽  
Vol 12 (2) ◽  
pp. 613
Author(s):  
Alexey N. Beskopylny ◽  
Evgenii M. Shcherban’ ◽  
Sergey A. Stel’makh ◽  
Levon R. Mailyan ◽  
Besarion Meskhi ◽  
...  

Currently, considering global trends and challenges, as well as the UN sustainable development goals and the ESG plan, the development of geopolymer binders for the production of geopolymer concrete has become an urgent area of construction science. This study aimed to reveal the influence of the component composition and recipe dosage on the characteristics of fine-grained geopolymer concrete with the use of stone flour. Eleven compositions of geopolymer fine-grained concrete were made from which samples of the mixture were obtained for testing at the beginning and end of setting and models in the form of beams and cubes for testing the compressive strength tensile strength in bending. It was found that the considered types of stone flour can be successfully used as an additive in the manufacture of geopolymer concrete. An analysis of the setting time measurements showed that stone flour could accelerate the hardening of the geopolymer composite. It was found that the addition of stone waste significantly improves the compressive strength of geopolymers in comparison with a geopolymer composite containing only quartz sand. The maximum compressive strength of 52.2 MPa and the tensile strength in bending of 6.7 MPa provide the introduction of potassium feldspar in an amount of 15% of the binder mass. Microstructural analysis of the geopolymer composite was carried out, confirming the effectiveness of the recipe techniques implemented in this study.


2022 ◽  
Author(s):  
SERAFINO CARUSO ◽  
DOMENICO UMBRELLO

Abstract Residual stresses and strains, distortion, heat affected zone (HAZ), grain size changes and hardness variation during gas metal arc welding (GMAW), are fundamental aspects to study and control during welding processes. For this reason, numerical simulations of the welding processes represent the more frequently used tool to better analyse the several aspects characterizing this joining process with the aim to reduce lead time and production costs. In the present study an uncoupled 3D thermo-mechanical analysis was carried out by two commercial finite element method (FEM) software to model an experimental single bead GMAW of AISI 441 at different process set-up. The experimental HAZ and measured temperatures were used to calibrate the heat source of both the used numerical codes, then a validation procedure was done to test the robustness of the two developed analytical procedures. One software was used to predict the residual stresses and strains and the distortions of the welded components, while in the second software a user routine was implemented, including a physical based model and the Hall-Petch (H-P) equation, to predict grain size change and hardness evolution respectively. The results demonstrate that the predicted mechanical and microstructural aspects agree with those experimentally found showing the reliability of the two codes in predicting the thermal phenomena characterizing the HAZ during the analysed welding process.


2022 ◽  
Vol 1048 ◽  
pp. 121-129
Author(s):  
Samit Karmakar ◽  
Soumik Kumar Kundu ◽  
Aditya Mukherjee ◽  
Sujit Kumar Bandyopadhyay ◽  
Satyaranjan Bhattacharyya ◽  
...  

Microstructural analysis of commercially available cold-rolled polycrystalline copper foil, etched and annealed in an in-house developed Electron Cyclotron Resonance (ECR) Plasma Enhanced Chemical Vapour Deposition (PE-CVD) reactor, have been carried out using x-ray diffraction (XRD) studies. The annealing experiments were carried out under a vacuum environment, keeping the working pressure of the reactor at 50×10-3 mbar, for three different time spans of 30 mins, 45 mins and 1 hour at 823 K (550 °C) and 923 K (650 °C) respectively in presence of hydrogen plasma. The XRD studies reveal the significance of annealing time at two different temperatures for the determination of physical and microstructural parameters such as the average grain size and micro-strain in copper lattice by Williamson-Hall (W-H) method.


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