Non-destructive measurement of grinding-induced deformation-depth using grazing incidence X-ray diffraction technique

2021 ◽  
pp. 102592
Author(s):  
Anirban Naskar ◽  
S. Paul
2020 ◽  
Vol 60 (4) ◽  
pp. 475-480
Author(s):  
V. A. N. Righetti ◽  
T. M. B. Campos ◽  
L. B. Robatto ◽  
R. R. Rego ◽  
G. P. Thim

2005 ◽  
Vol 490-491 ◽  
pp. 143-148
Author(s):  
Chedly Braham ◽  
Andrzej Baczmanski ◽  
Wilfrid Seiler ◽  
N. Shiraki

The X-ray diffraction measurements based on the grazing incident geometry were applied to determine lattice strains in polycrystalline materials. This method enables a non-destructive measurement at chosen depth below the sample surface. The volume, for which the stress is measured, is well defined and it does not vary during experiment. The multireflection method was used for analysis of the experimental results since the interplanar spacings were measured for various orientation of the scattering vector as well as for various crystallographic planes {hkl}. Applying two different wavelengths of X- ray radiation and various incident angles non-destructive measurements of the residual stresses in function of penetration depth were performed. The variation of stresses in plastically deformed surface layers of steel samples was successfully determined and the values of the stresses were confirmed by standard diffraction measurement.


2013 ◽  
Vol 772 ◽  
pp. 143-147
Author(s):  
Marianna Marciszko ◽  
Andrzej Stanisławczyk ◽  
Andrzej Baczmanski ◽  
Krzysztof Wierzbanowski ◽  
Wilfrid Seiler ◽  
...  

The geometry based on the multireflection grazing incidence X-ray diffraction (called the MGIXD method) can be applied to measure residual stresses. Using this method, it is possible to perform a non-destructive analysis of the heterogeneous stresses for different and well defined volumes below the surface of the sample (range of several mm). As the result the average values of stresses weighted by absorption of X-ray radiation are measured. In this work the stress profile as a function of depth for mechanically polished Ti and Al samples were calculated from MGIXD data using inverse Laplace transform.


The Analyst ◽  
2018 ◽  
Vol 143 (18) ◽  
pp. 4290-4297 ◽  
Author(s):  
Elena Possenti ◽  
Chiara Colombo ◽  
Claudia Conti ◽  
Lara Gigli ◽  
Marco Merlini ◽  
...  

Underlying layers of polychrome stratigraphies revealed using a non-destructive approach by synchrotron radiation grazing incidence X-ray diffraction.


2011 ◽  
Vol 1 (SRMS-7) ◽  
Author(s):  
M. Sato ◽  
T. Doi ◽  
Y. Hidaka ◽  
Y. Higashida ◽  
Y. Masaki ◽  
...  

The depth profiles of the constituent in iron oxide scales were investigated by X-ray diffraction measurement with controlling X-ray penetration depth at SPring-8. We successfully observed the interface region of scales non-destructively using X-ray with energy of 28 keV. The results indicated that the volume fraction ratio of Fe3O4 to FeO around the surface of samples increased by isothermal heat treatment. This suggested that the transformation of FeO to Fe3O4 due to isothermal heat treatment proceeds from surface into the inside of scale.


2001 ◽  
Vol 34 (4) ◽  
pp. 427-435 ◽  
Author(s):  
S. J. Skrzypek ◽  
A. Baczmański ◽  
W. Ratuszek ◽  
E. Kusior

A new development in the determination of residual stresses in thin surface layers and coatings is presented. The procedure, based on the grazing-incidence X-ray diffraction geometry (referred to here as the `g-sin2 ψ' geometry), enables non-destructive measurement at a chosen depth below the sample surface. The penetration depth of the X-ray radiation is well defined and does not change during the experiment. The method is particularly useful for the analysis of non-uniform stresses in near-surface layers. The g-sin2 ψ geometry was applied for measurements of the residual stresses in TiN coatings. Anisotropic diffraction elastic constants of textured material were used to determine the stress value from the measured lattice strains. A new method of data treatment enables reference-free measurements of residual stresses.


Author(s):  
A. R. Lang

AbstractX-ray topography provides a non-destructive method of mapping point-by-point variations in orientation and reflecting power within crystals. The discovery, made by several workers independently, that in nearly perfect crystals it was possible to detect individual dislocations by X-ray diffraction contrast started an epoch of rapid exploitation of X-ray topography as a new, general method for assessing crystal perfection. Another discovery, that of X-ray Pendellösung, led to important theoretical developments in X-ray diffraction theory and to a new and precise method for measuring structure factors on an absolute scale. Other highlights picked out for mention are studies of Frank-Read dislocation sources, the discovery of long dislocation helices and lines of coaxial dislocation loops in aluminium, of internal magnetic domain structures in Fe-3 wt.% Si, and of stacking faults in silicon and natural diamonds.


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