Development of a stochastic detection efficiency calibration procedure for studying collimation effects on a broad energy germanium detector

Author(s):  
Massimo Altavilla ◽  
Romolo Remetti
2021 ◽  
Vol 16 (12) ◽  
pp. C12017
Author(s):  
G. Kim ◽  
I. Lim ◽  
B. Kim ◽  
K. Song ◽  
J.-G. Kim

Abstract An alpha imaging detector acquires a two-dimensional distribution of a sample that emits alpha particles. For the quantitative analysis of the image of an alpha-emitting sample, the individual energies of the alpha particles must be identified, which can be achieved using the spectrometric method after detector calibration. In this study, an energy and efficiency calibration method was investigated to assess an alpha imaging detector. The calibration was performed using a single standard source of Am-241 based on the energy loss characteristic of an alpha particle. The feasibility of the calibration method was evaluated using another source, Ac-225. The calibrated alpha imaging detector was evaluated in terms of energy resolution and detection efficiency, and the alpha imaging detector was found to be efficiently calibrated using a single standard source. The calibrated alpha imaging detector appears promising for the quantitative analysis of samples that emit alpha particles.


2019 ◽  
Vol 322 (3) ◽  
pp. 1311-1321
Author(s):  
Krzysztof Gorzkiewicz ◽  
Jerzy Wojciech Mietelski ◽  
Renata Kierepko ◽  
Kamil Brudecki

Abstract This paper presents results of the development process of low-background, digital gamma-rays spectrometer equipped with Broad Energy Germanium detector (CANBERRA BE5030), multi-layer passive shield and cosmic veto system that consists of five plastic scintillators (SCIONIX EJ-200). Data acquisition is performed using digitizer CAEN DT5725 with CoMPASS software. Output data analysis is carried out with purposely written and developed code VETO. On the basis of conducted tests, acquisition parameters were set up and tuned as well as time delays between all detectors were established. As a result of the configuration process, the mean background counts reduction of 64% in the whole spectrum and 65% in annihilation peak were achieved. This procedure allowed diminishing detection limits of selected isotopes 37% on average.


2006 ◽  
Vol 12 (5) ◽  
pp. 406-415 ◽  
Author(s):  
Marco Alvisi ◽  
Markus Blome ◽  
Michael Griepentrog ◽  
Vasile-Dan Hodoroaba ◽  
Peter Karduck ◽  
...  

A calibration procedure for the detection efficiency of energy dispersive X-ray spectrometers (EDS) used in combination with scanning electron microscopy (SEM) for standardless electron probe microanalysis (EPMA) is presented. The procedure is based on the comparison of X-ray spectra from a reference material (RM) measured with the EDS to be calibrated and a reference EDS. The RM is certified by the line intensities in the X-ray spectrum recorded with a reference EDS and by its composition. The calibration of the reference EDS is performed using synchrotron radiation at the radiometry laboratory of the Physikalisch-Technische Bundesanstalt. Measurement of RM spectra and comparison of the specified line intensities enables a rapid efficiency calibration on most SEMs. The article reports on studies to prepare such a RM and on EDS calibration and proposes a methodology that could be implemented in current spectrometer software to enable the calibration with a minimum of operator assistance.


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