Improvement of the QuEChERS extraction step by matrix-dispersion effect and application on beta-lactams analysis in wastewater sludge by LC-MS/MS

Talanta ◽  
2022 ◽  
Vol 237 ◽  
pp. 122923
Author(s):  
Alexandre Guironnet ◽  
Laure Wiest ◽  
Emmanuelle Vulliet
2019 ◽  
Vol 2 (1) ◽  
pp. 59-64
Author(s):  
Vincentius Vincentius ◽  
Evita H. Legowo ◽  
Irvan S. Kartawiria

Natural gas is a source of energy that comes from the earth which is depleting every day, an alternative source of energy is needed and one of the sources comes from biogas. There is an abundance of empty fruit bunch (EFB) that comes from palm oil plantation that can become a substrate for biogas production. A methodology of fermentation based on Verein Deutscher Ingenieure was used to utilize EFB as a substrate to produce biogas using biogas sludge and wastewater sludge as inoculum in wet fermentation process under mesophilic condition. Another optimization was done by adding a different water ratio to the inoculum mixture. In 20 days, an average of 6gr from 150gr of total EFB used in each sample was consumed by the microbes. The best result from 20 days of experiment with both biogas sludge and wastewater sludge as inoculum were the one added with 150gr of water that produced 2910ml and 2185ml of gas respectively. The highest CH 4 produced achieved from biogas sludge and wastewater sludge with an addition of 150gr of water to the inoculum were 27% and 22% CH 4 respectively. This shows that biogas sludge is better in term of volume of gas that is produced and CH percentage.


2013 ◽  
Vol 8 (0) ◽  
pp. 1403010-1403010 ◽  
Author(s):  
Makoto SASAKI ◽  
Kimitaka ITOH ◽  
Naohiro KASUYA ◽  
Klaus HALLATSCHEK ◽  
Sanae-I. ITOH

2017 ◽  
Vol 16 (1) ◽  
pp. 149-155
Author(s):  
Sandor Beszedes ◽  
Lajos Ludanyi ◽  
Gabor Szabo ◽  
Cecilia Hodur

Author(s):  
N. Shakhrai ◽  
N. Dobrynina ◽  
T. Priimak

Организации водопроводно-канализационного хозяйства в рамках технологических процессов водоотведения должны обеспечивать дезинвазию очищенных сточных вод и осадков, образующихся в результате их очистки. В соответствии с пунктом 1.2 СанПиН 3.2.3215-14 Профилактика паразитарных болезней на территории РФ , санитарные правила устанавливают требования к комплексу организационных, санитарно-противоэпидемических (профилактических) мероприятий, проведение которых направлено на предупреждение возникновения и распространения паразитарных заболеваний. Проведена оценка нормативных документов по дезинвазии объектов окружающей среды, а также решений по судебным делам в части ее проведения. Выявлены разногласия в документах по проведению дезинвазии, в связи с чем направлены обращения в различные организации с предложением гармонизировать правила с целью исключения разночтений. Изучены индустриальные методы дезинвазии осадка сточных вод. Показано, что происходит необоснованное навязывание препарата Бингсти .Within the frames of the wastewater disposal processes water and wastewater utilities shall provide for the disinvasion of effluents and wastewater sludge generated in the process of wastewater treatment. In accordance with paragraph 1.2 of SanPiN 3.2.3215-14 Prevention of parasitic diseases in the territory of the Russian Federation , the sanitary rules set out the requirements for a comprehensive set of organizational, sanitary and anti-epidemic (preventive) measures, that are aimed at preventing the occurrence and spread of parasitic diseases. The assessment of regulatory documents on the disinvasion of environmental objects, as well as judicial decisions regarding its implementation, was carried out. Controversies were revealed in the regulatory documents, and appeals were sent to various organizations with a proposal to harmonize the rules in order to exclude discrepancies. Industrial methods for disinvasion of wastewater sludge were studied. It is shown that there is an unreasonable aggressive selling of Bingsti ineffective product.


Vsyo o myase ◽  
2020 ◽  
pp. 56-60
Author(s):  
Zayko E.V. ◽  
◽  
Kuznetsova O.A. ◽  
Bataeva D.S. ◽  
Grudistova M.A. ◽  
...  

The problem of the uncontrolled use of antibiotics currently remains unresolved. Step-by-step monitoring of meat using modern methods will reduce the risk of using contaminated meat raw materials for food production. Qualitative monitoring will identify samples containing residual antimicrobial substances. The use of methods for identifying groups of antibiotics will help narrow the search for antibiotics by expensive chromatographic methods. A study was carried out of beef, pork and poultry meat, which is used in meat processing plants in the production of raw smoked sausages, using two methods. At the first stage, using a qualitative microbiological method, the raw meat was evaluated for the presence of antimicrobial substances, then their group was determined using a NovoCyte flow cytometer. According to the results of a study on a flow cytometer, it was found that out of 10 groups of antibiotics that can be determined by the tested method, the group of lincosamides was not found in all meat samples. The most common groups of chemotherapy drugs in pork were sulfonamides – 29.6 %, tetracycline group – 18.5 % and beta-lactams – 14.8 %, and in beef aminoglycosides – 36.7 %, phenicols – 30 % and beta-lactams – 13.3 %. In poultry meat samples, the most common were sulfonamides – 23.2 %, fenicols – 23.2 %, and beta-lactams – 16 %. Five groups of antibiotics were found in all studied types of meat: fenicols, β-lactams, macrolides, polypeptide antibiotics, and quinolones. This indicates their widespread use in animal husbandry and poultry farming.


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