Influence of ion species of AuSi liquid metal alloy source-focused ion beam on SiO2/Si nanopatterning

2019 ◽  
Vol 669 ◽  
pp. 215-219
Author(s):  
A. Aissat ◽  
F. Benyettou ◽  
I. Berbezier ◽  
J.P. Vilcot
2020 ◽  
Vol 11 ◽  
pp. 1742-1749
Author(s):  
Nico Klingner ◽  
Gregor Hlawacek ◽  
Paul Mazarov ◽  
Wolfgang Pilz ◽  
Fabian Meyer ◽  
...  

While the application of focused ion beam (FIB) techniques has become a well-established technique in research and development for patterning and prototyping on the nanometer scale, there is still a large underused potential with respect to the usage of ion species other than gallium. Light ions in the range of m = 1–28 u (hydrogen to silicon) are of increasing interest due to the available high beam resolution in the nanometer range and their special chemical and physical behavior in the substrate. In this work, helium and neon ion beams from a helium ion microscope are compared with ion beams such as lithium, beryllium, boron, and silicon, obtained from a mass-separated FIB using a liquid metal alloy ion source (LMAIS) with respect to the imaging and milling resolution, as well as the current stability. Simulations were carried out to investigate whether the experimentally smallest ion-milled trenches are limited by the size of the collision cascade. While He+ offers, experimentally and in simulations, the smallest minimum trench width, light ion species such as Li+ or Be+ from a LMAIS offer higher milling rates and ion currents while outperforming the milling resolution of Ne+ from a gas field ion source. The comparison allows one to select the best possible ion species for the specific demands in terms of resolution, beam current, and volume to be drilled.


2013 ◽  
Vol 543 ◽  
pp. 69-73 ◽  
Author(s):  
A. Benkouider ◽  
I. Berbezier ◽  
A. Ronda ◽  
L. Favre ◽  
E. Ruiz Gomes ◽  
...  

2016 ◽  
Vol 3 (2) ◽  
pp. 021101 ◽  
Author(s):  
Lothar Bischoff ◽  
Paul Mazarov ◽  
Lars Bruchhaus ◽  
Jacques Gierak

Author(s):  
P. D. Lobanov ◽  
O. N. Kashinsky ◽  
A. S. Kurdyumov ◽  
N. A. Pribaturin

An experimental study of dynamic processes during pulsed gas injection into quiescent liquids was performed. Both water and low melting temperature metal alloy were used as test liquids. Air and argon were used as gas phase. The test sections were vertical cylindrical columns 25 and 68 mm inner diameter. Measurements of flow parameters during gas injection were performed. Water – air experiments were performed at room temperature, the temperature of liquid metal alloy was 135 deg C. Time records of pressure in the liquid and in gas phase above the liquid were obtained. Measurements of liquid temperature and level of liquid surface were performed. It was shown that at pulse gas injection into liquid metal high amplitude pressure fluctuation may arise. Also the fluctuation variation of the free surface of the liquid may appear which are connected with the oscillations of the gas volume. Experimental data obtained may be used for verification & validation of modern CFD codes.


Author(s):  
Qi Chen ◽  
W. D. Griffiths

AbstractIn this work, Mo was added into Al melt to reduce the detrimental effect of double-oxide film defect. An air bubble was trapped in a liquid metal (2L99), served as an analogy for double-oxide film defect in aluminum alloy castings. It was found that the addition of Mo significantly accelerated the consumption of the entrapped bubble by 60 pct after holding for 1 hour. 2 sets of testbar molds were then cast, with 2L99 and 2L99+Mo alloy, with a badly designed running system, intended to deliberately introduce double oxide film defects into the liquid metal. Tensile testing showed that, with the addition of Mo, the Weibull modulus of the Ultimate Tensile Strength and pct Elongation was increased by a factor of 2.5 (from 9 to 23) and 2 (from 2.5 to 4.5), respectively. The fracture surface of 2L99+Mo alloy testbars revealed areas of nitrides contained within bi-film defects. Cross-sections through those defects by Focused Ion Beam milling suggested that the surface layer were permeable, which could be as thick as 30 μm, compared to around 500 nm for the typical oxide film thickness. Transmission Electron Microscopy analysis suggested that the nitride-containing layer consisted of nitride particles as well as spinel phase of various form. The hypothesis was raised that the permeability of the nitride layers promote the reaction between the entrapped atmosphere in the defect and the surrounding liquid metal, reducing the defect size and decreasing their impact on mechanical properties.


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