Surface analysis of DC oxygen plasma treated or chromium evaporated poly(ethylene terephthalate) foils by soft X-ray absorption spectroscopy (NEXAFS)

Polymer ◽  
1997 ◽  
Vol 38 (8) ◽  
pp. 2005-2010 ◽  
Author(s):  
I. Koprinarov ◽  
A. Lippitz ◽  
J.F. Friedrich ◽  
W.E.S. Unger ◽  
Ch. Wöll
2006 ◽  
Vol 21 (4) ◽  
pp. 323-325 ◽  
Author(s):  
Joseph H. Reibenspies ◽  
Nattamai Bhuvanesh

Thin-walled heat-shrink poly(ethylene terephthalate) (PET) tubing is reported for use as an alternative for glass and Kapton® capillaries. PET tubing displays properties such as low X-ray absorption and smooth diffraction profiles. The 2.0 mm thin-walled (0.05 mm thick) and 0.5 mm thin-walled (0.02 mm thick) heat-shrink PET capillaries are 86% and 96% transparent to 1.54 Å X-rays. The low X-ray absorption and relatively smooth X-ray scattering profile of PET make it an ideal material for the home laboratory where the long wavelength, low flux, and low brilliance X-ray sources are employed. PET capillaries can be easily cut and manipulated and fixed to copper pins, which in turn can be employed in low-temperature and automated data collection routines.


Author(s):  
E. G. Rightor ◽  
A. P. Hitchcock ◽  
S. G. Urquhart ◽  
A. T. Wen

The near-edge region of core ionization edges can be used as a probe of the local bonding and structure of atoms excited by incident radiation, such as in electron energy loss spectroscopy (EELS) or x-ray absorption techniques. Recent installation of efficient parallel EELS spectrometers in ATEMs promotes study of these transitions in radiation sensitive materials such as polymers. To study relationships between poly(ethylene terephthalate) [PET] structure and EELS transitions, we compared polymer spectra with molecular analogues.The PET examined (from Scientific Polymer Products) was cut using a diamond knife and a Reichert-Jung Ultracut E ultramicrotome with FC4E cryoattachment. A JEOL 2000FX TEM with a LaB6 filament and a Gatan parallel-EELS system was used to examine PET sections on holey carbon. The gas phase EELS of molecules (from Aldrich, Matheson) was performed under inelastic scattering conditions as described previously.


2011 ◽  
Vol 44 (1) ◽  
pp. 56-61 ◽  
Author(s):  
Aleš Doliška ◽  
Alenka Vesel ◽  
Metod Kolar ◽  
Karin Stana-Kleinschek ◽  
Miran Mozetič

1991 ◽  
Vol 31 (11) ◽  
pp. 812-817 ◽  
Author(s):  
Y. Nakayama ◽  
F. Soeda ◽  
A. Ishitani ◽  
T. Ikegami

1975 ◽  
Vol 17 (4) ◽  
pp. 990-995 ◽  
Author(s):  
L.L. Razumova ◽  
T.Ye. Rudakova ◽  
Yu.V. Moiseyev ◽  
L.A. Mel'nikov ◽  
G.Ye. Zaikov

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