Stopped-flow injection simultaneous determination of phosphate and silicate using molybdenum blue

Talanta ◽  
2002 ◽  
Vol 58 (6) ◽  
pp. 1319-1326 ◽  
Author(s):  
K Grudpan
1983 ◽  
Vol 66 (3) ◽  
pp. 718-726
Author(s):  
Jacobus F Van Staden

Abstract A 3-channel flow-injection procedure was developed, which enables the simultaneous determination of protein, phosphorus, and calcium in a wide range of animal feeds from a single digestion. Samples are digested with a block digestor, diluted, and analyzed at a rate of 82 samples/h. Protein (nitrogen) as ammonia is determined colorimetrically by the indophenol method. Phosphorus and calcium are determined by measuring the absorbances of the molybdenum blue and calcium-cresolphthalein complexes at 660 and 580 nm, respectively. Protein is determined in the range from 0 to 75%, phosphorus in the range from 0 to 6%, and calcium in the range from 0 to 6%. The results obtained do not differ significantly from those obtained by proven manual methods, and considerable time, space, and reagents are saved.


The Analyst ◽  
1990 ◽  
Vol 115 (5) ◽  
pp. 605 ◽  
Author(s):  
Jacobus F. van Staden ◽  
Ancel van Rensburg

2018 ◽  
Vol 73 (5) ◽  
pp. 216-222
Author(s):  
D. V. Vokhmyanina ◽  
E. E. Karyakina ◽  
E. A. Andreev ◽  
A. A. Karyakin

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