CH3SH-sensing characteristics of LaFeO3 thick-film prepared by co-precipitation method

2003 ◽  
Vol 94 (2) ◽  
pp. 197-200 ◽  
Author(s):  
Chu Xiangfeng ◽  
Pietro Siciliano
2006 ◽  
Vol 05 (02n03) ◽  
pp. 265-271
Author(s):  
MENG KUI WANG ◽  
YU QIANG YANG

The preparing process and the properties of thick-film double-based thermo-sensitive material were studied. The preparing steps were as follows: (i) preparing Ba 1-x Sr x TiO 3 micro-powders with chemical co-precipitation method; (ii) adding dispersants and surface active agents into crushing medium powders to prepare Ba 1-x Sr x TiO 3 nanopowders; (iii) preparing V 2 O 3-based micro-powders; (iv) mixing Ba 1-x Sr x TiO 3 nanopowders, V 2 O 3-based micro-powders, donor impurities, acceptor impurities and micro additives according to a certain ratio to make thick-film thermo-sensitive ceramic material. The presintering and sintering temperature of the prepared PTC ceramics were both reduced, which is very meaningful in using cheaper SiC instead of more expensive MoSi 2, prolonging the kiln's life, and lowering the production cost. The samples we prepared did not contain PbO , so they are safe to the environment.


2016 ◽  
Author(s):  
Prashant R. Chaudhari ◽  
S. S. Darunkar ◽  
S. M. Bansod ◽  
V. M. Gaikwad ◽  
S. A. Acharya

2015 ◽  
Vol 7 (2) ◽  
pp. 1393-1403
Author(s):  
Dr R.P VIJAYALAKSHMI ◽  
N. Manjula ◽  
S. Ramu ◽  
Amaranatha Reddy

Single crystalline nano-sized multiferroic BiFeO3 (BFO) powders were synthesized through simple chemical co-precipitation method using polyethylene glycol (PEG) as capping agent. We obtained pure phase BiFeO3 powder by controlling pHand calcination temperature. From X-ray diffraction studies the nanoparticles were unambiguously identified to have a rhombohedrally distorted perovskite structure belonging to the space group of R3c. No secondary phases were detected. It indicates single phase structure. EDX spectra indicated the appearance of three elements Bi, Fe, O in 1:1:3. From the UV-Vis diffuse reflectance spectrum, the absorption cut-off wavelength of the BFO sample is around 558nm corresponding to the energy band gap of 2.2 eV. The size (60-70 nm) and morphology of the nanoparticles have been analyzed using transmission electron microscopy (TEM).   Linear M−H behaviour and slight hysteresis at lower magnetic field is observed for BiFeO3 nanoparticles from Vibrating sample magnetometer studies. It indicates weak ferromagnetic behaviour at room temperature. From dielectric studies, the conductivity value is calculated from the relation s = L/RbA Sm-1 and it is around 7.2 x 10-9 S/m.


2020 ◽  
Vol 3 (1) ◽  
pp. 30-33
Author(s):  
Muthulakshmi M ◽  
Madhumitha G

Nanotechnology is a field of applied science focused on design, synthesis and characterization of nanomaterials. The nickel and magnesium have improved their applications in transparent electrodes and nano electronics. In addition, magnesium oxide has moisture resistance and high melting point properties. In the present work has been carried out in the development of green crystalline powder of nickel doped magnesium oxide nanoparticles by Co-precipitation method, from the mixture of nickel chloride and magnesium chloride with KOH as solvent. From the XRD results, crystalline size of the particle can be observed. Spherical structure of Ni doped MgO nanoparticles were indicated by SEM results and powdered composition of samples were obtained from FTIR. EDAX represents the peak composition of the nanoparticle. The above analytical techniques have confirmed that the Ni doped MgO nanoparticles obtained from the mixture of NiCl2 and MgCl2.


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