Practical Linear Regression-Based Method for Detection and Quantification of Stiction in Control Valves

Author(s):  
Seshu K. Damarla ◽  
Xi Sun ◽  
Fangwei Xu ◽  
Ashish Shah ◽  
Joseph Amalraj ◽  
...  
2014 ◽  
Vol 22 (4) ◽  
pp. 407-412 ◽  
Author(s):  
Rafidah Ismail ◽  
Hai Yen Lee ◽  
Nor Ainy Mahyudin ◽  
Fatimah Abu Bakar

2017 ◽  
Vol 9 (1) ◽  
pp. 58 ◽  
Author(s):  
Isam Eldin Hussein Elgailani ◽  
Tofeeg Haseen Alghamdi

This research aimed to develop inexpensive, safe, rapid, efficent spectrophotometric method for the assay of atenolol in some antihypertensive drugs namely Normoten in its pharmaceutical formulation. The studied method is depend on the reaction of the drug with phenol red in acidic medium, at pH 3.0. The analytical parameters have been investigated. The maximum absorbance was obtained at 429 nm and the molar absorptivity of 0.054 L mol-1 cm-1. Beer’s law is linear in the concentration range of 0.5-100 μg/mL for atenolol in Normoten. The detection and quantification limits were found to be 0.038 and 0.113μg/mL for the atenolol in Normoten respectively, and with a linear regression correlation coefficient of 0.997. The recovery was found to be 98.94 to 100.31%. The studied method is can be applied for the determination of atenolol (active ingredient) of the antihypertensive drugs in their pharmaceutical formulations.


2006 ◽  
Vol 14 (12) ◽  
pp. 1395-1412 ◽  
Author(s):  
M.A.A. Shoukat Choudhury ◽  
S.L. Shah ◽  
N.F. Thornhill ◽  
David S. Shook

2009 ◽  
Vol 92 (6) ◽  
pp. 1833-1838 ◽  
Author(s):  
M Marsin Sanagi ◽  
Susie L Ling ◽  
Zalilah Nasir ◽  
Dadan Hermawan ◽  
Wan Aini Wan Ibrahim ◽  
...  

Abstract LOD and LOQ are two important performance characteristics in method validation. This work compares three methods based on the International Conference on Harmonization and EURACHEM guidelines, namely, signal-to-noise, blank determination, and linear regression, to estimate the LOD and LOQ for volatile organic compounds (VOCs) by experimental methodology using GC. Five VOCs, toluene, ethylbenzene, isopropylbenzene, n-propylbenzene, and styrene, were chosen for the experimental study. The results indicated that the estimated LODs and LOQs were not equivalent and could vary by a factor of 5 to 6 for the different methods. It is, therefore, essential to have a clearly described procedure for estimating the LOD and LOQ during method validation to allow interlaboratory comparisons.


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