Three-dimensional lattice connectivities from two-dimensional high-resolution solid-state NMR. Silicon-29 magic angle spinning NMR investigation of the silicate lattice of zeolite ZSM-39 (Dodecasil 3C)

1989 ◽  
Vol 111 (20) ◽  
pp. 7702-7707 ◽  
Author(s):  
C. A. Fyfe ◽  
H. Gies ◽  
Y. Feng
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Three Dimensional ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Two Dimensional ◽  
Dimensional Lattice ◽  
Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

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