scholarly journals A Novel High-Resolution and Sensitivity-Enhanced Three-Dimensional Solid-State NMR Experiment Under Ultrafast Magic Angle Spinning Conditions

2015 ◽  
Vol 5 (1) ◽  
Author(s):  
Rongchun Zhang ◽  
Manoj Kumar Pandey ◽  
Yusuke Nishiyama ◽  
Ayyalusamy Ramamoorthy
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Solid State Nmr ◽  
Three Dimensional ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

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