A Condensable Amphiphile with a Cleavable Tail as a “Lizard” Template for the Sol−Gel Synthesis of Functionalized Mesoporous Silica

2004 ◽  
Vol 126 (4) ◽  
pp. 988-989 ◽  
Author(s):  
Qingmin Zhang ◽  
Katsuhiko Ariga ◽  
Akihiro Okabe ◽  
Takuzo Aida
Keyword(s):  
Mesoporous Silica ◽  
Sol Gel ◽  
Functionalized Mesoporous Silica ◽  
Sol Gel Synthesis

ELECTROCHEMICAL PREPARATION OF NEW ORGANOSILICONE COMPOUNDS FOR FUNCTIONALIZING OF MESOPOROUS SILICA

2013 ◽  
Vol 06 (03) ◽  
pp. 1350031
Author(s):  
HABIBEH HADAD DABAGHI ◽  
MAHMOOD KAZEMZAD ◽  
YADOLAH GANJKHANLOU ◽  
AMIR ALI YUZBASHI
Keyword(s):  
Mesoporous Silica ◽  
Sol Gel ◽  
Area Measurement ◽  
Bet Surface Area ◽  
Electrochemical Preparation ◽  
Organometallic Reagents ◽  
Functionalized Mesoporous Silica ◽  
Ft Ir ◽  
Voltammetric Studies ◽  
Adsorption Desorption

Electrochemistry has been introduced as a powerful tool in order to prepare new organometallic reagents for functionalizing of mesoporous silica. Preparation of the reagents was based on electrochemical oxidation of dihydroxybenzene derivatives in the presence of 3-(trimethoxysilyl)-1-propanethiol as a nucleophile. The mechanisms of electrochemical reactions were studied by voltammetric studies. Mesoporous silica SBA-15 was also synthesized in this work through sol-gel hydrothermal method using Genapol PF-10 as structure directing compound. The prepared mesoporous silica was characterized by FT-IR analysis and Barrett–Joiner–Halenda (BJH) pore size and Brunauer–Emmett–Teller (BET) surface area measurement methods using N2 adsorption–desorption isotherm. Finally, the organometallic reagent was covalently grafted on the surface of mesoporous silica. Functionalizing of this material with the new reagent was confirmed by Fourier transform infrared (FT-IR) spectroscopy. The functionalized mesoporous silica by new reagent can be utilized in biological applications.

A new method for loading mesoporous silica nanoparticles with drugs: Sol–gel synthesis using drug micelles as a template

2016 ◽  
Vol 78 (5) ◽  
pp. 586-595 ◽  
Author(s):  
O. V. Dement’eva ◽  
I. N. Senchikhin ◽  
M. E. Kartseva ◽  
V. A. Ogarev ◽  
A. V. Zaitseva ◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Silica Nanoparticles ◽  
Mesoporous Silica Nanoparticles ◽  
Sol Gel ◽  
New Method ◽  
Sol Gel Synthesis

Template Sol-Gel Synthesis of Phosphorescent Mesoporous Silica Film Nanocomposites Using an Amphiphilic Gold (I) Pyrazolate Complex

2011 ◽  
Vol 364 ◽  
pp. 55-59 ◽  
Author(s):  
Hendrik O. Lintang ◽  
Kazushi Kinbara ◽  
Takuzo Aida
Keyword(s):  
Mesoporous Silica ◽  
Sol Gel ◽  
Silica Film ◽  
Aqueous Alcohol ◽  
Molar Ratios ◽  
Silica Source ◽  
Aqueous Alcohol Solution ◽  
Mesoporous Silica Film ◽  
Sol Gel Synthesis ◽  
Film Nanocomposites

Herein novel mesoporous silica film nanocomposites are successfully synthesized by using phosphorescent columnar assembly of an amphiphilic trinuclear gold (I) pyrazolate complex [Au3Pz3] as a functional template in the sol-gel synthesis. By controlling the molar ratios of silica source tetrabutylorthosilicate (TBOS) to [Au3Pz3] in an acidic aqueous alcohol solution from 60:1 to 20:1, highly ordered phosphorescent nanocomposites can be fabricated with hexagonal [Au3Pz3]/silicahexand lamellar [Au3Pz3]/silicalamsilicates.

scholarly journals Sol‐Gel Synthesis of Mesoporous Silica Using a Protein Crystal Template

ChemNanoMat ◽  
2021 ◽  
Author(s):  
Antti Korpi ◽  
Mauri Aleksi Kostiainen
Keyword(s):  
Mesoporous Silica ◽  
Sol Gel ◽  
Protein Crystal ◽  
Sol Gel Synthesis

Smart organic/inorganic sol-gel nanocomposite containing functionalized mesoporous silica for corrosion protection

2019 ◽  
Vol 133 ◽  
pp. 44-54 ◽  
Author(s):  
S.M. Ashrafi-Shahri ◽  
F. Ravari ◽  
D. Seifzadeh
Keyword(s):  
Mesoporous Silica ◽  
Corrosion Protection ◽  
Sol Gel ◽  
Functionalized Mesoporous Silica

scholarly journals Sol-Gel Synthesis and Adsorption Properties of Mesoporous Silica with Mercapto Groups

2018 ◽  
Vol 11 (4) ◽  
pp. 518-530
Author(s):  
Novikova Svetlana A. ◽  
◽  
Parfenov Vladimir A. ◽  
Zaitseva Julia N. ◽  
◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Sol Gel ◽  
Adsorption Properties ◽  
Sol Gel Synthesis ◽  
Mercapto Groups

scholarly journals Template-free sol–gel synthesis of high surface area mesoporous silica based catalysts for esterification of di-carboxylic acids

2016 ◽  
Vol 19 (10) ◽  
pp. 1247-1253 ◽  
Author(s):  
Pavan M. More ◽  
Shubhangi B. Umbarkar ◽  
Mohan K. Dongare
Keyword(s):  
Mesoporous Silica ◽  
Surface Area ◽  
Carboxylic Acids ◽  
High Surface ◽  
Sol Gel ◽  
High Surface Area ◽  
Template Free ◽  
Sol Gel Synthesis
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