Size Control of Titanium Oxide Sheets by Regulating Catalysis in a Catalytic Sol−Gel Process and Their UV Absorption Properties

2000 ◽  
Vol 104 (9) ◽  
pp. 1916-1920 ◽  
Author(s):  
Taki Matsumoto ◽  
Yasushi Murakami ◽  
Yoshio Takasu
2015 ◽  
Vol 50 (13) ◽  
pp. 4698-4706 ◽  
Author(s):  
Maoqiao Xiang ◽  
Yingchun Zhang ◽  
Ming Hong ◽  
Shuyan Liu ◽  
Yun Zhang ◽  
...  

2010 ◽  
Vol 5 (6) ◽  
pp. 361 ◽  
Author(s):  
R.-J. Tan ◽  
Y.-H. Tseng ◽  
C.-H. Kuo

2011 ◽  
Vol 38 (3-5) ◽  
pp. 685-692
Author(s):  
Tae Kyu Kim ◽  
Euh Duck Jeong ◽  
Mee Sung Lee ◽  
Jong-Pil Kim ◽  
Myung Ho Hyun ◽  
...  

2013 ◽  
Vol 787 ◽  
pp. 52-57
Author(s):  
Ying Qiu ◽  
Shu Chun Hu ◽  
Jing Zhai ◽  
Zhi Jian Lin ◽  
Wen Feng Liu ◽  
...  

Silica sphere has wide applications not only in the field of physical chemistry dealing with dynamic behavior and stability of particulate systems, but also in industries including catalysts, ceramics, pigments, pharmacy, etc. However, the control on the particle size is a key factor in the preparation process of silica sphere. In this paper, silica sphere with uniform sphere morphology and amorphous structure was prepared by a sol-gel method, and the control of particle size was emphatically studied. The results showed that the particle size of the as-prepared silica sphere was obviously influenced by the raw materials concentration. The average size of the product increased from 0.66 μm to 0.90 μm when ethanol concentration increased from 7.14M to 9.55M, increased from 0.50 μm to 0.90 μm with the increase of ammonia concentration in the range of 1.88M to 2.36M, and increased from 0.47 to 0.90 μm while tetraethoxysilane concentration increased from 0.08M to 0.11M. Further study indicated that the silica particle size was also influenced by reaction temperature, it increased with the increase of temperature from 26°C to 28°C, and decreased with the further increase of temperature in the scope of 28°C to 32°C.


2005 ◽  
Vol 900 ◽  
Author(s):  
A. Deptuła ◽  
Kenneth C Goretta ◽  
Tadeusz Olczak ◽  
Wieslawa Lada ◽  
Andrzej G. Chmielewski ◽  
...  

ABSTRACTTitanium oxide and titanates based on Ba, Sr and Ca were prepared from commercial solutions of TiCl4 and HNO3. The main preparation steps for the sols consisted of elimination of chloride anions by distillation with nitric acid and addition of metal hydroxides for the titanates. Resulting sols were gelled and used to (1) prepare irregularly shaped powders by evaporation; (2) produce by a dipping technique thin films on glass, Ag, or Ti substrates; and (3) produce spherical powders (diameters <100 μm) by solvent extraction. Results of thermal and X-ray-diffraction analyses indicated that the temperatures required to form the various compounds were lower than those necessary to form the compounds by conventional solid-state reactions and comparable to those required with use of organometallic based sol-gel methods. Temperatures of formation could be further reduced by addition of ascorbic acid to the sols.


RSC Advances ◽  
2014 ◽  
Vol 4 (106) ◽  
pp. 61727-61735 ◽  
Author(s):  
Venu Sreekala Smitha ◽  
Saju Pillai ◽  
Unnikrishnan Nair Saraswathy Hareesh ◽  
Balagopal N. Nair ◽  
Krishna Gopakumar Warrier

Novel multifunctional luminescent and self-cleaning nanocomposites and coatings of Eu doped TiO2–SiO2–LaPO4 (Eu-TSL) were synthesized from an aqueous sol–gel process which possess photoactivity, low wettability and photoluminescent properties.


2004 ◽  
Vol 398 (1-3) ◽  
pp. 157-162 ◽  
Author(s):  
M. Rivallin ◽  
M. Benmami ◽  
A. Gaunand ◽  
A. Kanaev

Holzforschung ◽  
2017 ◽  
Vol 71 (7-8) ◽  
pp. 645-648 ◽  
Author(s):  
Edgars Kirilovs ◽  
Silvija Kukle ◽  
Janis Gravitis ◽  
Hans-Jörg Gusovius

Abstract A new invisible nanolevel coating has been developed based on the sol-gel process for veneer finishes. The sol synthesis and its application as a protective agent is described. It could be demonstrated that a combination of organic light stabilizers and sol-gel deposits is feasible and that the resulting hybrid inorganic-organic thin films decrease moisture uptake of hardwood veneers.


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