scholarly journals Charge of clustered microparticles measured in spatial plasma afterglows follows the smallest enclosing sphere model

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
B. van Minderhout ◽  
J. C. A. van Huijstee ◽  
R. M. H. Rompelberg ◽  
A. Post ◽  
A. T. A. Peijnenburg ◽  
...  

AbstractThe plasma-induced charge of non-spherical microparticles is a crucial parameter in complex plasma physics, aerosol science and astrophysics. Yet, the literature describes this charge by two competing models, neither of which has been experimentally verified or refuted. Here we offer experimental proof that the charge on a two-particle cluster (doublet) in the spatial afterglow of a low-pressure plasma equals the charge that would be obtained by the smallest enclosing sphere and that it should therefore not be based on its geometrical capacitance but rather on the capacitance of its smallest enclosing sphere. To support this conclusion, the size, mass and charge of single particles (singlets) and doublets are measured with high precision. The measured ratio between the plasma-afterglow-induced charges on doublets and singlets is compared to both models and shows perfect agreement with the predicted ratio using the capacitance of the smallest enclosing sphere, while being significantly dissimilar to the predicted ratio based on the particle’s geometrical capacitance.

2008 ◽  
Vol 36 (4) ◽  
pp. 1014-1015 ◽  
Author(s):  
L. Couedel ◽  
A.A. Samarian ◽  
M. Mikikian ◽  
L. Boufendi

2008 ◽  
Vol 84 (3) ◽  
pp. 35002 ◽  
Author(s):  
L. Couëdel ◽  
A. A. Samarian ◽  
M. Mikikian ◽  
L. Boufendi

2008 ◽  
Vol 15 (6) ◽  
pp. 063705 ◽  
Author(s):  
L. Couëdel ◽  
A. A. Samarian ◽  
M. Mikikian ◽  
L. Boufendi

2008 ◽  
Author(s):  
B. Layden ◽  
L. Couëdel ◽  
A. A. Samarian ◽  
M. Mikikian ◽  
S. V. Vladimirov ◽  
...  

2011 ◽  
Vol 39 (11) ◽  
pp. 2764-2765 ◽  
Author(s):  
Brett Layden ◽  
Lénaïc Couedel ◽  
Alexander A. Samarian ◽  
Laïfa Boufendi

2009 ◽  
Vol 49 (4-5) ◽  
pp. 235-259 ◽  
Author(s):  
L. Couëdel ◽  
A. Mezeghrane ◽  
A.A. Samarian ◽  
M. Mikikian ◽  
Y. Tessier ◽  
...  

Author(s):  
S. Cusack ◽  
J.-C. Jésior

Three-dimensional reconstruction techniques using electron microscopy have been principally developed for application to 2-D arrays (i.e. monolayers) of biological molecules and symmetrical single particles (e.g. helical viruses). However many biological molecules that crystallise form multilayered microcrystals which are unsuitable for study by either the standard methods of 3-D reconstruction or, because of their size, by X-ray crystallography. The grid sectioning technique enables a number of different projections of such microcrystals to be obtained in well defined directions (e.g. parallel to crystal axes) and poses the problem of how best these projections can be used to reconstruct the packing and shape of the molecules forming the microcrystal.Given sufficient projections there may be enough information to do a crystallographic reconstruction in Fourier space. We however have considered the situation where only a limited number of projections are available, as for example in the case of catalase platelets where three orthogonal and two diagonal projections have been obtained (Fig. 1).


Author(s):  
A.M. Jones ◽  
A. Max Fiskin

If the tilt of a specimen can be varied either by the strategy of observing identical particles orientated randomly or by use of a eucentric goniometer stage, three dimensional reconstruction procedures are available (l). If the specimens, such as small protein aggregates, lack periodicity, direct space methods compete favorably in ease of implementation with reconstruction by the Fourier (transform) space approach (2). Regardless of method, reconstruction is possible because useful specimen thicknesses are always much less than the depth of field in an electron microscope. Thus electron images record the amount of stain in columns of the object normal to the recording plates. For single particles, practical considerations dictate that the specimen be tilted precisely about a single axis. In so doing a reconstructed image is achieved serially from two-dimensional sections which in turn are generated by a series of back-to-front lines of projection data.


Author(s):  
Joachim Frank

Compared with images of negatively stained single particle specimens, those obtained by cryo-electron microscopy have the following new features: (a) higher “signal” variability due to a higher variability of particle orientation; (b) reduced signal/noise ratio (S/N); (c) virtual absence of low-spatial-frequency information related to elastic scattering, due to the properties of the phase contrast transfer function (PCTF); and (d) reduced resolution due to the efforts of the microscopist to boost the PCTF at low spatial frequencies, in his attempt to obtain recognizable particle images.


Author(s):  
L.D. Schmidt ◽  
K. R. Krause ◽  
J. M. Schwartz ◽  
X. Chu

The evolution of microstructures of 10- to 100-Å diameter particles of Rh and Pt on SiO2 and Al2O3 following treatment in reducing, oxidizing, and reacting conditions have been characterized by TEM. We are able to transfer particles repeatedly between microscope and a reactor furnace so that the structural evolution of single particles can be examined following treatments in gases at atmospheric pressure. We are especially interested in the role of Ce additives on noble metals such as Pt and Rh. These systems are crucial in the automotive catalytic converter, and rare earths can significantly modify catalytic properties in many reactions. In particular, we are concerned with the oxidation state of Ce and its role in formation of mixed oxides with metals or with the support. For this we employ EELS in TEM, a technique uniquely suited to detect chemical shifts with ∼30Å resolution.


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