The determination of microgram amounts of sulphate by emission spectroscopy of barium with a nitrous oxide-acetylene flame

The macrophorous hydrophobic sorbent Amberlite XAD-2 proved to be well suited to the preconcentration of minority amounts of Al, Au, Cd, Co, Cr, Cu, Fe, Mn, Ni, Pb, Sn, Ti and V in the form of their chelates with organic reagents. From among 14 reagents tested, 8-hydroxyquinoline and diethyldithiocarbamate appeared most suitable for the quantitative sorption up to level of 1 μg l-1 of analyte. Emission spectrometry served as the analytical finish; the nitrous oxide-acetylene flame, electric arc and inductively coupled argon plasma were chosen according to the nature of the element. The procedure is convenient for the determination of the minority analytes in waters

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Mercury-204 Determination by Emission Spectroscopy

Applied Spectroscopy ◽

10.1366/000370265789619962 ◽

1965 ◽

Vol 19 (3) ◽

pp. 87-89 ◽

Cited By ~ 1

Author(s):

F. M. Smith

Keyword(s):

Coefficient Of Variation ◽

Isotope Shift ◽

Emission Spectroscopy ◽

Electrodeless Discharge ◽

Discharge Lamp ◽

Isotope Concentration ◽

Single Determination ◽

Time Required

The determination of mercury-204 was made by using the isotope shift of the 3984 A mercury line excited by electrodeless discharge. Densitometric traces were made from film recordings of the 3984 A line and the areas under the component peaks were determined. Ratios of each of these areas to the sum of the areas from all the line components are plotted against the isotope concentration to produce a working curve. The coefficient of variation for this method is approximately 11 percent The time required for a single determination (after fabrication of the discharge lamp) is about two hours.

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Based on Atomic Spectrometry for the Determination of Titanium Element in Molten Steel

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.622-623.1528 ◽

2012 ◽

Vol 622-623 ◽

pp. 1528-1531

Author(s):

Cui Hong Ma ◽

Wei Qiang Zhang

Keyword(s):

Molten Steel ◽

Emission Spectroscopy ◽

Atomic Emission ◽

Lag Time ◽

High Accuracy ◽

Atomic Spectrometry ◽

Atomic Emission Spectrometry ◽

Emission Spectrometry ◽

Important Significance

Atomic emission spectrometry with high accuracy, short lag time, and low detection limit, it has been widely applied in various fields. The application of atomic emission spectrometry in the converter steelmaking process has an important significance to improve the smelting of speed and steel quality. This article describes the principle of atomic emission spectroscopy (AES) analysis. Spectra obtained by the experimental for qualitative analysis, detected molten steel containing titanium element.

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Interferences of Major Elements in the Determination of Rare Earth Elements by Inductively Coupled Plasma Atomic Emission Spectroscopy.

Analytical Sciences ◽

10.2116/analsci.8.189 ◽

1992 ◽

Vol 8 (2) ◽

pp. 189-193 ◽

Cited By ~ 45

Author(s):

Ambrogio MAZZUCOTELLI ◽

Fabio DE PAZ ◽

Emanuele MAGI ◽

Roberto FRACHE

Keyword(s):

Rare Earth ◽

Rare Earth Elements ◽

Inductively Coupled Plasma ◽

Emission Spectroscopy ◽

Atomic Emission ◽

Major Elements ◽

Atomic Emission Spectroscopy ◽

Plasma Atomic Emission ◽

Inductively Coupled

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ANALYSIS OF SOLDERS ON TIN AND LEAD BASES BY X-RAY FLOORESCENT SPECTROSCOPY

Proceedings of VIAM ◽

10.18577/2307-6046-2021-0-4-124-131 ◽

2021 ◽

pp. 124-131

Author(s):

A.V. Alekseev ◽

◽

G.V. Orlov ◽

P.S. Petrov ◽

A.V. Slavin ◽

...

Keyword(s):

Emission Spectroscopy ◽

High Resolution Mass Spectrometry ◽

Analytical Signal ◽

Atomic Emission ◽

Standard Samples ◽

X Ray ◽

Fundamental Parameters ◽

The Matrix ◽

Resolution Mass

The determination of the elements Cu, Ni, Sb, Bi, Pb, Zn and Fe in the tin-based solder VPr35, as well as the elements Sn, Ni, Sb, Bi and In in the lead-based VPr40 solder by the method of х-ray fluorescence spectroscopy has been carried out. The calibration dependences are corrected taking into account the superposition of signals from interfering elements on the analytical signal and changes in intensity caused by inter-element influences in the matrix. The analysis was carried out by the method of fundamental parameters without using standard samples. The correctness of the results obtained was confirmed by their comparative analysis by atomic emission spectroscopy and high-resolution mass spectrometry with a glow discharge.

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