A facile hydrothermal method to synthesize Sb2S3/Sb4O5Cl2 composites with three-dimensional spherical structures

RSC Advances ◽  
2015 ◽  
Vol 5 (65) ◽  
pp. 53019-53024 ◽  
Author(s):  
Qian Jiang ◽  
Xingzhong Yuan ◽  
Hou Wang ◽  
Xiaohong Chen ◽  
Shansi Gu ◽  
...  

Three-dimensional spherical Sb2S3/Sb4O5Cl2 microcrystallines were synthesized for the first time via a facile hydrothermal process without any oxychlorides at 100 °C.

Nanoscale ◽  
2015 ◽  
Vol 7 (17) ◽  
pp. 8149-8158 ◽  
Author(s):  
Wen-Da Oh ◽  
Shun-Kuang Lua ◽  
Zhili Dong ◽  
Teik-Thye Lim

A novel CuBi2O4 consisting of self-assembled spherical nanocolumn arrays (CuB-H) was synthesized via a facile hydrothermal method.


2016 ◽  
Vol 52 (75) ◽  
pp. 11274-11276 ◽  
Author(s):  
Jin Han ◽  
Maowen Xu ◽  
Yubin Niu ◽  
Guan-Nan Li ◽  
Minqiang Wang ◽  
...  

Novel K2Ti8O17 is successfully fabricated via a facile hydrothermal method combined with a subsequent annealing treatment and further evaluated as an anode material for potassium-ion batteries for the first time.


NANO ◽  
2016 ◽  
Vol 11 (06) ◽  
pp. 1650066 ◽  
Author(s):  
Quangui He ◽  
Jia Zhuang ◽  
Qiuxiang Wen ◽  
Yang Deng ◽  
Jun Yu ◽  
...  

An anatase TiO2 photoanode with a novel three-dimensional nest-like structure was prepared directly on a transparent conductive glass substrate through hydrothermal cycles by three times. First, an unidirectional banded structure film was prepared by a facile hydrothermal method. And then, with the time of hydrothermal cycle increased, part of nanobelts were ruptured into a lot of small polyhedrons, but they still maintained a trend of the previous connection, and some fine nanobelts were interweaved in small polyhedrons. Finally, we successfully prepared a film with a novel 3D nest-like structure, and it had all the characteristics of the hierarchitectures. It had better photoelectric properties than the film with fewer times of hydrothermal cycle. Its photoelectric conversion efficiency reached 3.81%, which is due to a large dye adsorption amount, rapid electronic transmission, and superior light scattering and more electrons transmission paths.


2014 ◽  
Vol 50 (14) ◽  
pp. 1731-1734 ◽  
Author(s):  
Zheng Wang ◽  
Jungang Hou ◽  
Chao Yang ◽  
Shuqiang Jiao ◽  
Hongmin Zhu

Three-dimensional MoS2–CdS–γ-TaON hollow nanostructures as novel photocatalysts were firstly synthesized via a facile hydrothermal method and they exhibit a high photocatalytic hydrogen production rate without a noble metal.


Author(s):  
Khatun A Jannath ◽  
Mahmood Hassan Akhtar ◽  
NG Gurudatt ◽  
Deog-Su Park ◽  
Kwang Bok Kim ◽  
...  

Octahedral SrMoO4 nanoparticles (NPs) with a high degree of crystallinity and controlled size (250-350 nm) were synthesized for the first time by employing a facile hydrothermal method. The prepared NPs...


RSC Advances ◽  
2016 ◽  
Vol 6 (105) ◽  
pp. 103124-103131 ◽  
Author(s):  
Boyang Ruan ◽  
Haipeng Guo ◽  
Qiannan Liu ◽  
Dongqi Shi ◽  
Shulei Chou ◽  
...  

SnO2-coated polypyrrole (PPy) with a three-dimensional (3-D) structured nanotube network has been prepared via a facile hydrothermal method and tested as an anode material for Na-ion batteries.


2008 ◽  
Vol 8 (12) ◽  
pp. 6425-6430 ◽  
Author(s):  
L. A. Diaz-Torres ◽  
P. Salas ◽  
J. S. Perez-Huerta ◽  
C. Angeles-Chavez ◽  
E. De la Rosa

Strong Blue, green, and red upconversion emission of Er3+ in nanocrystalline BaZrO3:(Yb3+Er3+) is observed. Powder samples were obtained by a facile hydrothermal process at 100 °C. The as synthesized nanocrystallites preserve a stable cubic perovskite phase under subsequent annealing treatment up to 1000 °C. No other phase or segregation of other compounds was detected. Crystallites sizes were around 115 nm and well faceted. Under IR excitation in the range between 900 and 1050 nm the Er3+ blue emission was almost not present in single Er3+ doped BaZrO3, whereas it became easily observable when Yb3+ was added as codopant. Besides, both green and red upconversion emission or upconverted signal of Er3+ are enhanced by around three orders of magnitude in comparison with the single Er3+ doped BaZrO3. The strong blue emission presents dependence on both excitation power and excitation wavelength. This is the first time that upconversion emission is observed in BaZrO3. A possible mechanism for the upconversion process that leads to the observed blue, green and red emissions under NIR excitation is suggested based on the experimental results.


2011 ◽  
Vol 295-297 ◽  
pp. 368-372 ◽  
Author(s):  
Ya Lan Zhong ◽  
Yi Fu Zhang ◽  
Xin Liu ◽  
Xing Hai Liu ◽  
Chi Huang ◽  
...  

VO2(A) nanobelts have been synthesized using V2O5, H2O2, ethanol, H2O as the starting materials through a facile hydrothermal method. The as-obtained products were characterized by X-ray powder diffraction (XRD), X-ray photoelecton spectroscopy (XPS), transmission electron microscopy (TEM) and differential scanning calorimetry (DSC). Some parameters, such as, the reaction time, reaction temperature and the ratio of EtOH/H2O, have greatly influenced on the phases and morphologies of the final products. It was found that VO2(A) can be converted to VO2(M) at 700 °C for 2 h for the first time. Furthermore, the phase transition properties of VO2(A) and VO2(M) phases were respectively studied.


RSC Advances ◽  
2015 ◽  
Vol 5 (122) ◽  
pp. 100934-100942 ◽  
Author(s):  
Yunxuan Zhao ◽  
Fei Teng ◽  
Juan Xu ◽  
Zailun Liu ◽  
Yang Yang ◽  
...  

One- and three-dimensional (1D, 3D) Cu2PO4OH hierarchical architectures have been successfully prepared by a facile hydrothermal method, mainly through adjusting the precursor concentrations.


Sign in / Sign up

Export Citation Format

Share Document