Synthesis of VO2(A) Nanostructures by a Hydrothermal Method and their Transition to VO2(M)
2011 ◽
Vol 295-297
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pp. 368-372
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Keyword(s):
X Ray
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VO2(A) nanobelts have been synthesized using V2O5, H2O2, ethanol, H2O as the starting materials through a facile hydrothermal method. The as-obtained products were characterized by X-ray powder diffraction (XRD), X-ray photoelecton spectroscopy (XPS), transmission electron microscopy (TEM) and differential scanning calorimetry (DSC). Some parameters, such as, the reaction time, reaction temperature and the ratio of EtOH/H2O, have greatly influenced on the phases and morphologies of the final products. It was found that VO2(A) can be converted to VO2(M) at 700 °C for 2 h for the first time. Furthermore, the phase transition properties of VO2(A) and VO2(M) phases were respectively studied.
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Vol 94
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pp. 1012-1030
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2021 ◽
Vol 12
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Vol 7
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