Redox titration of gold and platinum surface oxides at porous microelectrodes

2017 ◽  
Vol 19 (34) ◽  
pp. 22915-22925 ◽  
Author(s):  
Mareike Haensch ◽  
Julian Behnken ◽  
Luis Balboa ◽  
Alexander Dyck ◽  
Gunther Wittstock

Cavity-microelectrodes were used to investigate surface oxides on supported platinum nanoparticles and nanoporous gold with the surface interrogation mode of scanning electrochemical microscopy.

2019 ◽  
Vol 6 (12) ◽  
pp. 3160-3166 ◽  
Author(s):  
Mareike Haensch ◽  
Luis Balboa ◽  
Matthias Graf ◽  
Alex Ricardo Silva Olaya ◽  
Jörg Weissmüller ◽  
...  

2018 ◽  
Vol 185 (8) ◽  
Author(s):  
Henry Steven Catota Sáenz ◽  
Lucas Patricio Hernández-Saravia ◽  
Jéssica S. G. Selva ◽  
Anandhakumar Sukeri ◽  
Patricio Javier Espinoza-Montero ◽  
...  

Sensors ◽  
2021 ◽  
Vol 21 (4) ◽  
pp. 1132 ◽  
Author(s):  
Rejane M. P. da Silva ◽  
Javier Izquierdo ◽  
Mariana X. Milagre ◽  
Abenchara M. Betancor-Abreu ◽  
Isolda Costa ◽  
...  

Amperometric and potentiometric probes were employed for the detection and characterization of reactive sites on the 2098-T351 Al-alloy (AA2098-T351) using scanning electrochemical microscopy (SECM). Firstly, the probe of concept was performed on a model Mg-Al galvanic pair system using SECM in the amperometric and potentiometric operation modes, in order to address the responsiveness of the probes for the characterization of this galvanic pair system. Next, these sensing probes were employed to characterize the 2098-T351 alloy surface immersed in a saline aqueous solution at ambient temperature. The distribution of reactive sites and the local pH changes associated with severe localized corrosion (SLC) on the alloy surface were imaged and subsequently studied. Higher hydrogen evolution, lower oxygen depletion and acidification occurred at the SLC sites developed on the 2098-T351 Al-alloy.


2021 ◽  
Vol 4 (4) ◽  
pp. 312-321
Author(s):  
Xiongjie Jin ◽  
Rio Tsukimura ◽  
Takeshi Aihara ◽  
Hiroki Miura ◽  
Tetsuya Shishido ◽  
...  

Nanoscale ◽  
2021 ◽  
Author(s):  
Katarina A. Novčić ◽  
Christian Iffelsberger ◽  
Siowwoon Ng ◽  
Martin Pumera

MoS2 and WS2 and their heterojunctions are used to modify thermally activated 3D-printed nanocarbon structures. Herein, the local electrochemical performance for HER of the modified structures is demonstrated by scanning electrochemical microscopy.


Author(s):  
Dylan T. Jantz ◽  
Ryan J. Balla ◽  
Siao-Han Huang ◽  
Niraja Kurapati ◽  
Shigeru Amemiya ◽  
...  

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