Effective and diastereoselective preparation of dispiro[cyclopent-3′-ene]bisoxindoles via novel [3 + 2] annulation of isoindigos and MBH carbonates

2018 ◽  
Vol 16 (8) ◽  
pp. 1297-1304 ◽  
Author(s):  
Hong-Xia Ren ◽  
Lin Peng ◽  
Xiang-Jia Song ◽  
Li-Guo Liao ◽  
Ying Zou ◽  
...  

Efficient, one-step preparation of highly steric dispiro[cyclopent-3′-ene]bisoxindoles with two all-carbon quaternary spirocenters and three adjacent cycles in excellent yields and diastereoselectivities under mild conditions.

2021 ◽  
Author(s):  
Zhigang Ren ◽  
peng zhao ◽  
Ye Zhang ◽  
Yang Yu ◽  
xiaoxuan lv ◽  
...  

Micron-sized carbon spheres synthesized via pickering emulsions has attracted much attention in recent two years. In present paper, we prepared palladium (Pd) and nitrogen co-embedded carbon microspheres for formaldehyde (HCHO)...


RSC Advances ◽  
2020 ◽  
Vol 10 (45) ◽  
pp. 27183-27193
Author(s):  
Rose Fadzilah Abdullah ◽  
Umer Rashid ◽  
Yun Hin Taufiq-Yap ◽  
Mohd Lokman Ibrahim ◽  
Chawalit Ngamcharussrivichai ◽  
...  

The potential of bifunctional nanocatalysts obtained from waste palm kernel shell (PKS) was investigated for one-step transesterification–esterification under mild conditions.


2021 ◽  
Author(s):  
Züleyha Kudaş ◽  
Emir Çepni ◽  
Emre Gür ◽  
Duygu Ekinci

Here, new carbon-based nanostructures were prepared by the one-step electrochemical method using hexagonal and pentagonal polychlorinated organic rings as carbon source. The electrochemical growth of carbon nanostructures on substrates was...


2016 ◽  
Vol 12 ◽  
pp. 1772-1777 ◽  
Author(s):  
Lena Huck ◽  
Juan F González ◽  
Elena de la Cuesta ◽  
J Carlos Menéndez

A sequential three-component process is described, starting from 3-arylmethylene-2,5-piperazinediones and involving a one-pot sequence of reactions achieving regioselective opening of the 2,5-diketopiperazine ring and diastereoselective generation of an aziridine ring. This method allows the preparation of N-unprotected, trisubstituted aziridines bearing a peptide side chain under mild conditions. Their transformation into β-trifluoroacetamido-α-ketoamide and α,β-diketoamide frameworks was also achieved in a single step.


2018 ◽  
Vol 47 (9) ◽  
pp. 2925-2932 ◽  
Author(s):  
J. Brendlé

The sol–gel process involving hydrolysis and condensation reactions is an attractive way to form siloxane based hybrid materials since it is a one-step method performed under mild conditions.


2017 ◽  
Vol 1 (2) ◽  
Author(s):  
Braja Gopal Bag ◽  
Shib Shankar Dash ◽  
Anup Mandal

The antioxidant efficacy of the rhizome extract of Polygonatum cirrhifolium (Mahameda) has been studied against a stable 2, 2-diphenylpicrylhydrazyl (DPPH) radical at room temperature. The chemical constituents present in the rhizome extract have been utilized for the one step synthesis of stable gold nanoparticles at room temperature under very mild conditions.


Synlett ◽  
2019 ◽  
Vol 30 (19) ◽  
pp. 2153-2156
Author(s):  
Andrea Renzetti ◽  
Ryan N. Rutherford ◽  
Kozo Fukumoto ◽  
Dominique Kunciw ◽  
Hannah F. Sore ◽  
...  

N-Substituted dipropargylamines that are suitable as functionalized linkers for peptide stapling can be synthesized in one step under mild conditions from commercially available starting materials (41% to quantitative yield).


2018 ◽  
Vol 5 (11) ◽  
pp. 2893-2897 ◽  
Author(s):  
Liangbiao Wang ◽  
Weicheng Dai ◽  
Kailong Zhang ◽  
Tao Mei ◽  
Haoyun Zhuang ◽  
...  

Carbides (Cr3C2 and Cr2AlC) have been synthesized by using waste PE as a carbon source in an autoclave under mild conditions.


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