scholarly journals A facile one-pot synthesis of CaO/CuO hollow microspheres featuring highly porous shells for enhanced CO2 capture in a combined Ca–Cu looping process via a template-free synthesis approach

2019 ◽  
Vol 7 (37) ◽  
pp. 21096-21105 ◽  
Author(s):  
Jian Chen ◽  
Lunbo Duan ◽  
Tian Shi ◽  
Ruoyu Bian ◽  
Yuxiao Lu ◽  
...  
Keyword(s):  
Co2 Capture ◽  
High Performance ◽  
Hollow Microspheres ◽  
One Pot ◽  
One Pot Synthesis ◽  
Template Free ◽  
Synthesis Approach ◽  
Highly Porous

The preparation of CaO/CuO composites with high performance is essential for combined Ca–Cu looping process, where the exothermic reduction of CuO with methane is used in situ to calcine CaCO3.

Dielectric Nanowire Composites: One-Pot Synthesis of Gold Nanoparticles Encapsulated in Polyaniline Fibers

2013 ◽  
Vol 1453 ◽  
Author(s):  
Eliud K. Mushibe ◽  
Steven C. Murphy ◽  
Kate Raiti-Palazzolo ◽  
Danielle L Mccarthy ◽  
Emilly A. Obuya ◽  
...  
Keyword(s):  
Electrical Conductivity ◽  
Gold Nanoparticles ◽  
Dielectric Constant ◽  
High Electrical Conductivity ◽  
One Pot ◽  
One Pot Synthesis ◽  
Inorganic Acids ◽  
Vis Spectroscopy ◽  
Synthesis Approach

ABSTRACTNanocomposites of gold nanoparticles (AuNPs) embedded in polyaniline fibers have been fabricated using a one-pot synthesis approach and in-situ polymerization. By using a combination of inorganic acids (e.g. HCl) and camphorsulfonic acid, polyaniline nanostructured fibers of high aspect ratio with diameters of 150 ± 50 nm and several micrometers in length were obtained. These fibers afforded high electrical conductivity of 4.2 ± 0.5 S/cm. Encapsulation of the AuNPs in the polyaniline fibers afforded nanocomposites with high electrical conductivity and dielectric constant of 34.0 ± 0.5 S/cm and 65.3 ± 5 respectively. The morphology of these materials was analyzed using SEM and HRTEM and electronic properties were analyzed using UV-Vis spectroscopy.

Indium Bromide-catalyzed Unprecedented Hydrogenolysis: A Novel One-Pot Synthesis of Per-O-Acetylated β-carboxymethyl O and S-glycosides

2020 ◽  
Vol 24 (8) ◽  
pp. 900-908
Author(s):  
Ram Naresh Yadav ◽  
Amrendra K Singh ◽  
Bimal Banik
Keyword(s):  
Asymmetric Synthesis ◽  
Chiral Auxiliary ◽  
Bioactive Molecules ◽  
One Pot ◽  
Enantiomerically Pure ◽  
Stereoselective Glycosylation ◽  
One Pot Synthesis ◽  
Wide Range

Numerous O (oxa)- and S (thia)-glycosyl esters and their analogous glycosyl acids have been accomplished through stereoselective glycosylation of various peracetylated bromo sugar with benzyl glycolate using InBr3 as a glycosyl promotor followed by in situ hydrogenolysis of resulting glycosyl ester. A tandem glycosylating and hydrogenolytic activity of InBr3 has been successfully investigated in a one-pot procedure. The resulting synthetically valuable and virtually unexplored class of β-CMGL (glycosyl acids) could serve as an excellent potential chiral auxiliary in the asymmetric synthesis of a wide range of enantiomerically pure medicinally prevalent β-lactams and other bioactive molecules of diverse medicinal interest.

Thermally stable amine-functionalized silica sorbents using one-pot synthesis method for CO2 capture at low temperature

2020 ◽  
Vol 37 (12) ◽  
pp. 2317-2325
Author(s):  
Seong Bin Jo ◽  
Ho Jin Chae ◽  
Tae Young Kim ◽  
Jeom-In Baek ◽  
Dhanusuraman Ragupathy ◽  
...  
Keyword(s):  
Low Temperature ◽  
Co2 Capture ◽  
Synthesis Method ◽  
Functionalized Silica ◽  
Thermally Stable ◽  
One Pot ◽  
One Pot Synthesis ◽  
Amine Functionalized
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