scholarly journals Hydrothermal synthesis of high surface area CuCrO2 for H2 production by methanol steam reforming

RSC Advances ◽  
2021 ◽  
Vol 11 (21) ◽  
pp. 12607-12613
Author(s):  
Rong-Jun Huang ◽  
Subramanian Sakthinathan ◽  
Te-Wei Chiu ◽  
Chaofang Dong

Hydrothermal synthesis of CuCrO2 nanopowder for H2 production by methanol steam reforming.

RSC Advances ◽  
2012 ◽  
Vol 2 (21) ◽  
pp. 8145 ◽  
Author(s):  
Mohamed A. Ebiad ◽  
Dalia R. Abd El-Hafiz ◽  
Radwa A. Elsalamony ◽  
Lamia. S. Mohamed

2012 ◽  
Vol 531-532 ◽  
pp. 508-511 ◽  
Author(s):  
Yan Juan Li ◽  
Nan Li ◽  
Xiao Yan ◽  
Yue Chi ◽  
Qing Yuan ◽  
...  

One-step and controlled pH hydrothermal synthesis of transition metal disulfide using double molybdenum sources to synthesize MoS2 nano-flowers at low temperature was first reported. Anhydrous molybdenum pentachloride (MoCl5) and four sulfur ammonium molybdate ((NH4) 6Mo7O24•4H2O) were the molybdenum source and CS (NH2) 2 was the sulfur source. Through hydrothermal method, MoS2 was obtained at 180 °C. The pH value of system was controlled by adjusting the molar ratio of MoCl5 and (NH4) 6Mo7O24•4H2O. The products were characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), surface area (BET) and transmission electron microscopy (TEM). The results show that the products were hexagonal MoS2 with a high crystalline and flower-like structure consisted of small particles. The thickness of petals is a few to tens of nanometers. By changing the molar ratio of molybdenum sources, the resultant phase from the mixed phase transited to the pure phase and the purity of synthetic MoS2 crystal increaseed.


2017 ◽  
Vol 69 ◽  
pp. 13-21 ◽  
Author(s):  
V.V. Butova ◽  
A.P. Budnyk ◽  
E.A. Bulanova ◽  
C. Lamberti ◽  
A.V. Soldatov

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