scholarly journals In Vitro Evaluation of Physical and Mechanical Properties of Light-Curing Resin Cement: A Comparative Study

2020 ◽  
Vol 14 (01) ◽  
pp. 152-156
Author(s):  
Luís Felipe Espíndola-Castro ◽  
Oscar Felipe Fonseca de Brito ◽  
Larissa Gabrielle Assis Araújo ◽  
Izabella Luiza Aragão Santos ◽  
Gabriela Queiroz De Melo Monteiro

Abstract Objective The aim of study was to evaluate in vitro the surface hardness, sorption, solubility, and color stability of three light-cured resin cements, namely RelyX Veneer (RLX), Variolink Veneer (VLK), and All Cem Veneer (ACV). Materials and Methods Cylindrical samples (15 × 1 mm) were made for each group using a metallic mold (n = 10). Vickers microhardness test was performed, and average hardness was calculated from three indentations (300 gf/15s) per sample. The sorption and solubility of the materials were evaluated according to ISO 4049:2009 based on three samples weighing: initial (m 1), after immersion in distilled water for 7 days (m 2), and final (after removal of all moisture [m 3]). The color change was observed using a digital spectrophotometer, at three different time points, baseline, 1 day, and 1 week of immersion in coffee and distilled water (control). Statistical Analysis Shapiro–Wilk test was used to analyze the normality of the data, and groups were compared using Kruskal–Wallis and Mann–Whitney tests. A significance level of 5% was used. Results RLX showed the highest microhardness mean values (36.96 VHN), but higher sorption (23.2 µg/mm3) and solubility (2.40 µg/mm3), with statistically significant differences with the other groups. For color stability, higher ∆E was observed for the samples immersed in coffee (p = 0.009). The VLK resin cement presented statistically significant differences from the other groups, with higher color changes in coffee at 1 day (15.14) and after 1 week (23.65). Conclusion RLX resin cement showed better hardness results. All materials tested performed satisfactorily for sorption and solubility according to ISO 4049:2009. All materials showed high-staining values after 1 week of immersion in coffee.

2019 ◽  
Vol 18 ◽  
pp. e191647
Author(s):  
Catharina e Silva Monteiro Barros ◽  
Jose Guilherme Neves ◽  
Ana Paula Terossi de Godoi ◽  
Ana Rosa Costa ◽  
Mario Vedovello Filho ◽  
...  

Aim: The present study aimed to assess, in vitro, the effect of chlorhexidine on the potentiation of polycrystalline ceramic bracket staining. Methods: Seventy-two polycrystalline ceramic brackets of upper right central incisors were divided into six groups (n=12) according to immersion solution. The groups were G1 - distilled water (control); G2 - chlorhexidine; G3 - coffee; G4 - red wine; G5 - chlorhexidine associated with coffee; and G6 - chlorhexidine associated with red wine. The samples were analyzed by means of a spectrophotometer according to the CIEL*a*b* system, and color change (ΔE*) was calculated. The readings were performed at the following times: T0 - After package removal and T1 - After staining. The data were analyzed by Kruskal Wallis and t tests (p<0.05) at 5% significance level. Results: The total color variation (ΔE*) was greater in the group that received chlorhexidine associated with red wine (p<0.05) and lower in the groups that received distilled water. All other groups showed greater value variations when compared to G1 and G2. Group G6 showed a greater color change due to the potentiation of chlorhexidine with the dye substance. Conclusion: It is concluded that chlorhexidine potentiates the staining caused by red wine in polycrystalline ceramic brackets.


2018 ◽  
Vol 47 (5) ◽  
pp. 333-339
Author(s):  
Tatiane Cristina DOTTA ◽  
Vinicius Cappo BIANCO ◽  
Alma Blásida Concepción Elizaur Benitez CATIRSE ◽  
Mayara Manfrin ARNEZ ◽  
Raisa CASTELO ◽  
...  

Abstract Introduction The color stability of resin cements, whether dual-pre-cured or photopolymerizable, as well as the color of the dental substrate, are fundamental for the aesthetic success of ceramic restorations, since the ceramic presents a high level of translucency due to its small thickness. Objective The aim of this in vitro study was to evaluate the color of a resin cement light polymerized by different light sources and immersed in potentially staining beverages. Material and method Were made 42 specimens of resin cement Variolink-Esthetic (2×6mm) (n=7), being half polymerized with LED light (F1) and half with Halogen light (F2). The specimens were stored in artificial saliva at 37 °C±1 °C. After 24 hours, they were polished with abrasive discs, and divided for the purpose of being submitted to the different solutions for 2 minutes per day, for 28 days, as follows: S1 – Coca-Cola; S2 – Red Wine; and S3 – Distilled Water (Control). Five color readouts were taken: T0 – initial; T1 – 7 days; T2 – 14 days; T3 – 21 days; and T4 – 28 days; with a spectrophotometer (Model SP62S). The color change data (ΔE*) were submitted to statistical analysis, ANOVA and Tukey (p≤0.05). Result Analyzing the factor solution, S2 (5.89 (±0.02)), produced a higher ΔE* value than S1 (3.79 (±0.02)) and (S1), a higher value than S3 (1.41 (±0.02)). Analyzing the factor light source, F2 (4.05 (±0.12)), produced a higher ΔE* value than F1 (3.33 (±0.12)). When analyzing the factor time, ΔE* values were found to increase gradually over the course of time: T1(2.36 (±0.08)); T2(3.27 (±0.08)); T3(4.06 (±0.08)); and T4(5.09 (±0.08)). Conclusion It was concluded that red wine produced a greater color change; Halogen light promoted highest degree of pigmentation; and the longer the time of immersion, the greater the color change of the material.


2013 ◽  
Vol 14 (4) ◽  
pp. 681-690 ◽  
Author(s):  
Khalid H Al-Samadani

ABSTRACT Objective To evaluate the effect of Arabic coffee, Turkish coffee and Nescafe on the color stability of four different composite resins after a period of aging time 1, 7 and 30 days. Materials and methods Twenty specimens from each type of tested composite resin material were prepared. Five specimens from each tested material (Z350 XT, Artist, GC and Z250) was evaluated after storage in Arabic coffee, Turkish coffee, Nescafe and distil water (control) at 37°C in a dark container for 1, 7 and 30 days. Color measurement was done using colorimeter based on the CIE L* a* b* color scale. Color differences ΔE*ab, Δb* and Δa* among specimens immersed in distil water and staining coffee beverages were evaluated overtime. Mean values were statistically analyzed with one-way analysis of variance (ANOVA), followed by Tukey test with p < 0.05 as significance level. Results All tested composite resins showed increase color change after a period of 1, 7 and 30 days. The color change ΔE*ab, Δb* and Δa* exhibited by Arabic coffee, in Turkish coffee and Nescafe except Δa*. The highest total color difference ΔE*ab after 30 days was in group A Arabic coffee (ΔE > 1.5 perceivable) and not perceivable in group B Turkish coffee and group C Nescafe. For Δb* all materials discolored toward yellowness after 30 days except Arabic coffee group which shifted from yellowness toward blueness (Δb*> 1.5 perceivable). Conclusion The effect of staining beverages on the resin composite materials increases with time of aging toward yellowness and not perceivable in all groups except with Arabic coffee which had highest effect after 30 days and the discoloration shifted from yellowness to blueness perceivable. How to cite this article Al-Samadani KH. Color Stability of Restorative Materials in Response to Arabic Coffee, Turkish Coffee and Nescafe. J Contemp Dent Pract 2013;14(4):681-690.


2016 ◽  
Vol 10 (1) ◽  
pp. 516-521 ◽  
Author(s):  
Vanessa Dias da Silva ◽  
Eduardo Martinelli S de Lima ◽  
Caroline Dias ◽  
Leandro Berni Osório

Proposition: The purpose of this study was to evaluate in vitro the color changes of esthetic orthodontic elastomeric ligatures of different shades when exposed to four food colorings commonly found in the diet of patients. Materials and Methods: The sample consisted of esthetic orthodontic elastomeric ligatures in the colors pearl, pearl blue, pearl white and colorless, which were immersed for 72 hours in five different solutions: distilled water (control group), coffee, tea, Coca-Cola ® and wine. The color changes of the esthetic orthodontic elastomeric ligatures were measured with the aid of a spectrophotometer, at T1 - as provided by the manufacturer; and T2 - after colorings process. Results: The results indicated that the esthetic orthodontic elastomeric ligatures of all initial hues are susceptible to pigmentation. Among the evaluated colors, all changed the finished look and the color of the samples tested. In ascending order, the color of the samples was as follows: distilled water, Coca-Cola®, black tea, wine and coffee. Conclusion: The substances that have a greater potential for pigmentation in esthetic orthodontic elastomeric ligatures were black tea, wine and coffee, respectively. All shades of esthetic orthodontic elastomeric ligatures are susceptible to color change.


2019 ◽  
Vol 44 (1) ◽  
pp. 65-75 ◽  
Author(s):  
JW Reinhardt ◽  
MM Balbierz ◽  
CM Schultz ◽  
B Simetich ◽  
MW Beatty

SUMMARY In this laboratory study, a composite resin was stained to a visibly discernible level using both coffee and red wine over 14 days (change was considered clinically noticeable and significant when ΔEab*≥2.7). Color change was measured at one, three, seven, and 14 days of staining. Although the nature of color change was different for the two staining solutions, the overall degree of staining (ΔEab*) rendered by either coffee or wine at each time interval was not significantly different (p≥0.05). Four whitening protocols were applied to stained composites. Treatment included applications of distilled water (control), Crest Pro-Health [HD] toothpaste, Crest Whitestrips, Opalescence PF bleach (15%), and application of a fine pumice polishing (Preppies). HD toothpaste and Whitestrips were applied daily for 21 days, Opalescence was applied daily for 10 days, and polishing was applied once. Each of the whitening products, applied in a manner simulating at-home or in-office treatment, was effective in producing color improvements (lightening) over controls (p&lt;0.05), but none of the four treatments produced lightening that was significantly different from the other treatments (p≥0.05). A comparison of final composite color with that measured at baseline showed that Opalescence returned composite color to an acceptable level following exposure to both staining solutions (ΔEab*&lt;2.7), Whitestrips returned color close to baseline for wine-stained composites, and HD paste and polishing permitted residual stain to remain (ΔEab*≥2.7).


2021 ◽  
Vol 3 (1) ◽  
pp. 61-65
Author(s):  
Wael Abdul Alrazzaq Alwaeli ◽  
Mohammed Abdul Sattar Alsegar

Heat-polymerized resins are common substances utilized for construction of removable dental prostheses (i.e. Orthodontic appliances). Such materials should have appropriate physical properties. The use of disinfectant solutions might influence the physical characteristics of the acrylic materials.  This study was conducted to assess the influence of different disinfectants on heat polymerized resins in terms of surface hardness. Forty specimens were made from heat-polymerized acrylic resins in total. The investigation comprised 4 groups according to the disinfectants utilized and each group had ten specimens. The 1st group was immersed in distilled water (control); the 2nd group was disinfected in Efferdent; the 3rd group was disinfected in 4 % Chlorhexidine; and the 4th group was disinfected in 1% hypochlorite. All specimens were tested via a hardness tester three times and the average reading was measured for all specimens. The statistical results indicated a slight decline in the mean values of surface hardness of acrylic specimens following immersion in disinfectants. The greatest value of mean was for distilled water specimens whereas the lowest value of mean was for 4% Chlorhexidine specimens. Furthermore, no significant differences were found among all groups (P>0.05). The study concluded that the use of disinfectants solutions slightly decreases the hardness of heat polymerized resins. It is recommended to evaluate the chemical interaction between the acrylic resins and disinfectants.


2007 ◽  
Vol 18 (2) ◽  
pp. 119-123 ◽  
Author(s):  
Fernanda de Carvalho Panzeri Pires-de-Souza ◽  
Lucas da Fonseca Roberti Garcia ◽  
Hisham Mohamad Hamida ◽  
Luciana Assirati Casemiro

The purpose of this study was to evaluate, in vitro, the color stability of three composite resins of two different shades (A3 and C3) cured with either a quartz tungsten halogen (QTH) or a light emitting diode (LED) source. Forty specimens (20 x 2 mm) were prepared for each composite (Tetric Ceram®, Heliomolar® and Esthet-X®), being 20 for each shade. In each group, 10 specimens were light-cured using the QTH unit and 10 with the LED source. The shade of the materials was evaluated before and after submitting the specimens to artificial accelerated aging (4 h UV-B/4 h condensing vapor), using a reflection spectrophotometer. deltaE means were calculated and analyzed statistically by 2-way ANOVA and Tukey's test at 5% significance level. Both A3 and C3 shades of Esthet-X composite resin showed the lowest color change when cured with the QTH light, while Tetric C3 cured with the QTH light showed the highest color change.


2020 ◽  
Vol 33 (2) ◽  
pp. 59-68
Author(s):  
Bruna Tavares ◽  
Fabiana França ◽  
Roberta Basting ◽  
Basting Turssi ◽  
Turssi Amaral

The aim of this in vitro study was to evaluate the effect of bleaching protocols on the surface roughness (Ra), color change and surface micromorphology of a low-viscosity bulk-fill composite (Filtek Bulk Fill Flow, 3M ESPE), a highviscosity bulk-fill composite (Filtek Bulk Fill, 3M ESPE) and a conventional nanoparticulate composite resin (control) (Filtek Z350 XT, 3M ESPE). Forty samples of each composite (disks 5 mm in diameter and 2 mm thick) were randomly divided into four groups (n=10), according to bleaching protocol: a) 10% carbamide peroxide gel (Opalescence, Ultradent Products) (2 h/ day, for 14 days); b) 40% hydrogen peroxide gel (Opalescence Boost, Ultradent Products) (three bleaching sessions, once a week, 45 min/session); c) whitening rinse (Listerine Whitening Extreme, Johnson & Johnson) (2 min/day, for 14 days); and d) distilled water (control). The samples were submitted to triplicate readings (Ra and color [CIELAB parameters]) before and after contact with bleaching protocols. Micromorphology was analyzed in a scanning electron microscope (SEM). Ra and color parameters (ΔL, Δa, Δb and ΔE) were analyzed by generalized linear models (α=0.05). The Ra of the high-viscosity bulk-fill was significantly higher than that of the other composites (p<0.05). Ra increased significantly (p<0.05) and surface became more irregular (SEM analysis) in all the composite resins, regardless of the bleaching protocol (p<0.05). The high-viscosity bulk-fill composite resin group had significantly lower ΔE (p<0.05) than the nanoparticulate composite resin group immersed in distilled water. It was concluded that the characteristics of each resin significantly influenced the Ra more than the bleaching protocol. The high-viscosity bulk-fill resin presented minor color change.


2017 ◽  
Vol 41 (2) ◽  
pp. 120-125 ◽  
Author(s):  
Ahmed Nour El-din Ahmed Habib ◽  
Soad Abdelmoniem Abdelmoniem ◽  
Sara Ahmed Mahmoud

Aim: To assess the effect of four different children's drinks on color stability of resin dental composites. Study design: A total of one hundred and twenty specimens were prepared from Grandio SO, Filtek Z350 XT and Filtek Z250 XT (forty specimens each). Specimens were thermocycled, then each group was further subdivided into four subgroups (n=10) according to the immersion media which were chocolate milk, mango juice, orange fizzy drink, and water (control). The initial color parameters of each specimen were recorded before immersion (baseline) and color change values were recorded three and seven days after immersion in each solution using a digital spectrophotometer. Atomic force microscope was used to measure the surface roughness in randomly selected samples after one week immersion in children's drinks. Results: All the children's drinks produced color changes in the examined resin dental composites, yet there was no statistical significant difference between the effects of tested drinks on the color changes (mean ΔE) of the three different dental composites (P&gt;0.05). Conclusions: All tested children's drinks caused clinically unacceptable color changes of the tested resin dental composites. Immersion in chocolate milk and orange fizzy led to the highest color changes in the tested resin dental composites.


2009 ◽  
Vol 39 (4) ◽  
pp. 961-968 ◽  
Author(s):  
Débora da Costa e Silva ◽  
Sanmya Beatriz da Silva Pereira Tiradentes ◽  
Rosana Cristina Pereira Parente ◽  
Maria Fulgência Costa Lima Bandeira

The purpose of this study is to evaluate in vitro the color stability of composite resins when exposed to beverages with high coloring contents from the Amazon region. 240 samples from four different composite brands (Natural Look, Z350, 4Seasons and Opallis) of hue A3 were fabricated using an acrylic matrix. The samples were stored in distilled water at 37ºC for 24 hours. The initial color (T0) was registered using a Canon EOS Rebel XTi 10 mp camera, and then the samples were divided into four groups (n=15): G1 (coffee), G2 (açaí juice), G3 (energetic guaraná) and G4 (control - distilled water). The samples were exposed to solutions of DES (6hs) and RE (18hs) and placed in a double boiler under constant agitation, at 37ºC for 30 days. The samples were immersed in the coloring solutions for 15 minutes daily. After 7, 15 and 30 days, new photographic registers were made (T1, T2 and T3). The images were analyzed using Corel PHOTO-PAINT 12 software to identify the colors through the HSB system. The Kruskal-Wallis and t tests (p<0.05) demonstrated significant differences in color (hue, saturation and brightness). The results revealed that none of the tested composites showed color stability when exposed to coloring solutions, and that the Amazon region beverages (açaí juice and energetic guaraná) showed to be less coloring than coffee.


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