scholarly journals New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team

2015 ◽  
Vol 86 (7) ◽  
pp. 072201 ◽  
Author(s):  
Yue Meng ◽  
Rostislav Hrubiak ◽  
Eric Rod ◽  
Reinhard Boehler ◽  
Guoyin Shen
2001 ◽  
Vol 15 (18) ◽  
pp. 2491-2497 ◽  
Author(s):  
J. L. ZHU ◽  
L. C. CHEN ◽  
R. C. YU ◽  
F. Y. LI ◽  
J. LIU ◽  
...  

In situ high pressure energy dispersive X-ray diffraction measurements on layered perovskite-like manganate Ca 3 Mn 2 O 7 under pressures up to 35 GPa have been performed by using diamond anvil cell with synchrotron radiation. The results show that the structure of layered perovskite-like manganate Ca 3 Mn 2 O 7 is unstable under pressure due to the easy compression of NaCl-type blocks. The structure of Ca 3 Mn 2 O 7 underwent two phase transitions under pressures in the range of 0~35 GPa. One was at about 1.3 GPa with the crystal structure changing from tetragonal to orthorhombic. The other was at about 9.5 GPa with the crystal structure changing from orthorhombic back to another tetragonal.


2001 ◽  
Vol 72 (2) ◽  
pp. 1289 ◽  
Author(s):  
Tetsu Watanuki ◽  
Osamu Shimomura ◽  
Takehiko Yagi ◽  
Tadashi Kondo ◽  
Maiko Isshiki

2010 ◽  
Vol 12 (12) ◽  
pp. 2059-2064 ◽  
Author(s):  
Björn Winkler ◽  
Erick A. Juarez-Arellano ◽  
Alexandra Friedrich ◽  
Lkhamsuren Bayarjargal ◽  
Florian Schröder ◽  
...  

2006 ◽  
Vol 21 (4) ◽  
pp. 320-322 ◽  
Author(s):  
P. Ch. Sahu ◽  
N. R. Sanjay Kumar ◽  
N. V. Chandra Shekar ◽  
N. Subramanian

An incident beam X-ray collimator for Mao-Bell type diamond anvil cell (DAC) has been developed. Alignment of the collimator is carried out in situ while viewing the image of the collimated X-ray spot formed on a thin layer of fluorescent material spread on the diamond anvil culets with the help of a microscope. Special precaution has been taken to meet the radiation safety requirements during alignment and routine use. This collimator is of immense help for laboratory based high pressure X-ray diffraction experiments.


2005 ◽  
Vol 19 (06) ◽  
pp. 313-316
Author(s):  
X. M. QIN ◽  
Y. YU ◽  
G. M. ZHANG ◽  
F. Y. LI ◽  
J. LIU ◽  
...  

In-situ high-pressure energy dispersive X-ray diffraction measurements on CuBa 2- Ca 3 Cu 4 O 10 + δ (Cu-1234) have been performed by using diamond anvil cell (DAC) device with synchrotron radiation. The results suggest that the crystal structure of Cu-1234 superconductor is stable under pressures up to 34 GPa at room temperature. According to the Birch–Murnaghan equation of state, the bulk modulus is obtained to be ~ 150 GPa.


2014 ◽  
Vol 277-278 ◽  
pp. 15-30 ◽  
Author(s):  
Ashkan Salamat ◽  
Rebecca A. Fischer ◽  
Richard Briggs ◽  
Malcolm I. McMahon ◽  
Sylvain Petitgirard

1997 ◽  
Vol 499 ◽  
Author(s):  
C. S. Yoo ◽  
H. Cynn ◽  
A. Campbell ◽  
J.-Z. Hu

ABSTRACTAn integrated technique of diamond-anvil cell, laser-heating and synchrotron x-ray diffraction technologies is capable of structural investigation of condensed matter in an extended region of high pressures and temperatures above 100 GPa and 3000 K. The feasibility of this technique to obtain reliable data, however, strongly depends on several experimental issues, including optical and x-ray setups, thermal gradients, pressure homogeneity, preferred orientation, and chemical reaction. In this paper, we discuss about these experimental issues together with future perspectives of this technique for obtaining accurate data.


2020 ◽  
Vol 5 (1) ◽  
pp. 018403 ◽  
Author(s):  
N. Hirao ◽  
S. I. Kawaguchi ◽  
K. Hirose ◽  
K. Shimizu ◽  
E. Ohtani ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document