scholarly journals Determination of n-alkane profile through developmental state of sunflower leaves

2012 ◽  
Vol 30 (1) ◽  
pp. 72 ◽  
Author(s):  
Nayan Roy ◽  
Subrata Laskar ◽  
Anandamay Barik

The n-hexane extracts of young, mature and senescent sunflower leaves containing a thin layer of epicuticular waxes was analysed by TLC and GC using standard hydrocarbons. The Scanning Electron Microscopy study indicated changes in the deposition of epicuticular wax throughout the developmental stage of the sunflower leaves. The young, mature and senescent leaves contained nine, nine and five long-chain nalkanes accounting for 86.22%, 99.76% and 92.07% of the hydrocarbons, respectively. The predominant nalkane was n-C29 for young and mature leaves, and n-C23 for senescent leaves representing 35.85%, 45.37% and 68.54% of the hydrocarbons, respectively; whilst n-C24, n-C32 and n-C19 were present in least amounts in young, mature and senescent leaves indicating 0.59%, 0.83% and 0.53% of the hydrocarbons, respectively.

Author(s):  
Julie A. Martini ◽  
Robert H. Doremus

Tracy and Doremus have demonstrated chemical bonding between bone and hydroxylapatite with transmission electron microscopy. Now researchers ponder how to improve upon this bond in turn improving the life expectancy and biocompatibility of implantable orthopedic devices.This report focuses on a study of the- chemical influences on the interfacial integrity and strength. Pure hydroxylapatite (HAP), magnesium doped HAP, strontium doped HAP, bioglass and medical grade titanium cylinders were implanted into the tibial cortices of New Zealand white rabbits. After 12 weeks, the implants were retrieved for a scanning electron microscopy study coupled with energy dispersive spectroscopy.Following sacrifice and careful retrieval, the samples were dehydrated through a graduated series starting with 50% ethanol and continuing through 60, 70, 80, 90, 95, and 100% ethanol over a period of two days. The samples were embedded in LR White. Again a graduated series was used with solutions of 50, 75 and 100% LR White diluted in ethanol.


2014 ◽  
Vol 48 ◽  
pp. 57-65 ◽  
Author(s):  
S. I. Genkal ◽  
M. I. Jarushina

A rare species Sellaphora hustedtii, which is also new for the flora of Russia, has been found in waterbodies of the Messoyakha River basin (south-western part of the Gydan Peninsula, Western Siberia). The scanning electron microscopy study revealed variability of the main quantitative and qualitative diagnostic features of the species (length and width of the valve, number of striae and areolae in 10 μm, shape of the valve and structure of the raphe). New data on the ecology and distribution of the species allowed us to specify its diagnosis.


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