Reaction-sintering method for microwave dielectric Li2CoTi3O8 ceramic

2016 ◽  
Vol 505 (1) ◽  
pp. 4-9 ◽  
Author(s):  
Pei Cui-Jin ◽  
Hu Xu-Sheng ◽  
Yao Guo-Guang ◽  
Yang He-qing
2015 ◽  
Vol 655 ◽  
pp. 164-167 ◽  
Author(s):  
Xu Sheng Hu ◽  
Guo Guang Yao ◽  
Xiu Lao Tian

Li2ZnTi3O8ceramics were prepared by reaction-sintering process (calcination free). The crystal phase and microstructure were investigated using X-ray diffraction (XRD) and scanning electron microscopy (SEM). A pure phase of Li2ZnTi3O8ceramics sintered at 1075 °C-1150 °C with cubic spinel structure was confirmed by XRD. The microwave dielectric properties (εr,Qxf) of Li2ZnTi3O8ceramics were strongly dependent on the densification and grain size. The τfof Li2ZnTi3O8ceramics was almost independent with the sintering temperatures. In particular, Li2ZnTi3O8ceramics by reaction-sintering method sintered at 1125 °C for 5 h exhibited good combination microwave dielectric properties of εr=21.7, Q×f=70 500 GHz (at 7.5 GHz) and τf=-13 ppm/°C.


2007 ◽  
Vol 546-549 ◽  
pp. 1661-1664
Author(s):  
Xiao Yan Wang ◽  
Fa Luo ◽  
Dong Mei Zhu ◽  
Wan Cheng Zhou ◽  
Hong Huan Wu

Csf/Si3N4 composites were prepared by hot-press sintering method using α-Si3N4 power, short chopping carbon-fiber and sintering additives. XRD analysis showed that the α-Si3N4 was almost completely transferred into β-Si3N4. The SEM micrographs of fractured surfaces showed that special network developed by rod-like β- Si3N4 grains. The flexure strength of 590±10MPa, and fracture toughness of 7.94±0.1MPa·m1/2 were achieved for the samples incorporated with 0.5wt% the carbon fibers .The microwave dielectric property of Csf/Si3N4 composites was measured at a frequency range of 8.2~18GHz by E8362B PNA series network analyzer. The real part (ε ′ ) of the permittivity of the Csf/Si3N4 composites increases from 10 to 58 with the rise of the content of carbon fibers in the composites, as well as the imaginary part increases from 0.03 to 98 at frequency of 9.375GHz. A strong frequency dependence of the real part was observed both in X and Ku bands.


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