SYNTHESIS AND CHARACTERIZATION OF 5- AND 6-COORDINATED MONOORGANOTIN(IV) COMPLEXES OF 2- AMINOCYCLOPENTENE-1-CARBODITHIOIC ACID AND ITS N-/S-ALKYL DERIVATIVE HAVING NS AND SS DONOR SYSTEM

2000 ◽  
Vol 166 (1) ◽  
pp. 221-230 ◽  
Author(s):  
Rajnish K. Sharma ◽  
Yashpal Singh ◽  
Audhesh K. Rai
Keyword(s):  
Alkyl Derivative ◽  
Synthesis And Characterization ◽  
Donor System

scholarly journals Synthesis and Characterization of New Oxovanadium(IV) Coordination Compounds with Pyrazol-5-one Azo Derivatives

1998 ◽  
Vol 6 (7) ◽  
pp. 91-99
Author(s):  
Anca EMANDI
Keyword(s):  
Electronic Spectra ◽  
Coordination Compounds ◽  
Synthesis And Characterization ◽  
Type I ◽  
Molecular Weights ◽  
Elementary Analysis ◽  
Visible Spectra ◽  
Azo Derivatives ◽  
Donor System

A new series of oxovanadium(IV) chelates containing bi-and tridentate pyrazol-5-one azo derivatives ligands of the type (I) [VO(L)2] and (2) [VO(L)(H2O)] have been prepared and characterized by elementary analysis, IR, electronic spectra, conductance measurements, and molecular weights. The ligands coordinate through (O-N) donor system as monobasic and bidentate (HL) for the first type and through (0-N-O) donor system as dibasic and tridentate (H2L) for the second type of complexes. The molecular weights, the presence of the (V=O) stretching band around 950 cm -1, and the visible spectra suggest a monomeric penta-coordinated structure for these complexes.

Synthesis and Characterization of the Three Dicyclopentapyrenes

1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula
Keyword(s):  
Synthesis And Characterization

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

Synthesis and characterization of zeolite-encapsulated porphyrins

2009 ◽  
Author(s):  
Marziye Javaheri Kachousangi ◽  
Rahmatollah Rahimi ◽  
Mohamad Mehdi Kashani-Motlagh
Keyword(s):  
Synthesis And Characterization
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