Study of Annealing Conditions on Particle Size of Nickel Ferrite Nanoparticles Synthesized by Wet Chemical Route

2015 ◽  
Vol 46 (3) ◽  
pp. 405-408 ◽  
Author(s):  
Israf Ud Din ◽  
S. Tasleem ◽  
A. Naeem ◽  
Maizatul S. Shaharun ◽  
Qazi Nasir
Keyword(s):  
Particle Size ◽  
Nickel Ferrite ◽  
Ferrite Nanoparticles ◽  
Chemical Route ◽  
Annealing Conditions ◽  
Nickel Ferrite Nanoparticles ◽  
Wet Chemical ◽  
Wet Chemical Route

Thiol-Capped CdSe and CdTe Nanoclusters: Synthesis by a Wet Chemical Route, Structural and Optical Properties

1998 ◽  
Vol 536 ◽  
Author(s):  
A. L. Rogach ◽  
A Eychmüller ◽  
J. Rockenberger ◽  
A. Kornowski ◽  
H. Weller ◽  
...  
Keyword(s):  
Particle Size ◽  
X Ray Diffraction ◽  
Structural And Optical Properties ◽  
Chemical Route ◽  
X Ray ◽  
Stabilizing Agents ◽  
Transmission Electron ◽  
Wet Chemical ◽  
Wet Chemical Route ◽  
X Ray Absorption

AbstractCdSe and CdTe nanoclusters were formed in aqueous solutions at moderate temperatures by a wet chemical route in the presence of thiols as effective stabilizing agents. The nature of the stabilizing agent (thioalcohols or thioacids) had an important influence on the particle size and largely determined the photoluminescence properties. The nanoclusters were characterized by means of UV-vis absorption and photoluminescence spectroscopy, powder X-ray diffraction, high resolution transmission electron microscopy, and extended X-ray absorption fine structure measurements. CdSe and CdTe nanoclusters were crystalline, in the cubic zincblende phase, with mean sizes in the range of 2 to 5 nm depending on the preparative conditions and the postpreparative size-selective fractionation, and showed pronounced electronic transitions in the absorption spectra. Thioglycerol-stabilized CdTe nanoclusters possessed sharp band-egde photoluminescence being tunable with particle size.

scholarly journals Synthesis of Bismuth Ferrite Nanoparticles via a Wet Chemical Route at Low Temperature

2011 ◽  
Vol 2011 ◽  
pp. 1-6 ◽  
Author(s):  
Yongming Hu ◽  
Linfeng Fei ◽  
Yiling Zhang ◽  
Jikang Yuan ◽  
Yu Wang ◽  
...  
Keyword(s):  
Citric Acid ◽  
Chemical Process ◽  
Bismuth Ferrite ◽  
Chelating Agent ◽  
Ferrite Nanoparticles ◽  
Size Distributions ◽  
Iron Nitrate ◽  
Chemical Route ◽  
Wet Chemical ◽  
Wet Chemical Route

Nanoparticles (NPs) of multiferroic bismuth ferrite (BiFeO3) with narrow size distributions were synthesized via a wet chemical route using bismuth nitrate and iron nitrate as starting materials and excess tartaric acid and citric acid as chelating agent, respectively, followed by thermal treatment. It was found that BiFeO3NPs crystallized at∼350∘Cwhen using citric acid as chelating agent. Such crystallization temperature is much lower than that of conventional chemical process in which other types of chelating agent are used. BiFeO3NPs with different sizes distributions show obvious ferromagnetic properties, and the magnetization is increased with reducing the particle size.

Structures of chemically stabilized ceramics

1993 ◽  
Vol 51 ◽  
pp. 924-925
Author(s):  
Pratibha L. Gai ◽  
M. A. Saltzberg ◽  
L.G. Hanna ◽  
S.C. Winchester
Keyword(s):  
High Temperature ◽  
Calcium Nitrate ◽  
Nitrate Hexahydrate ◽  
Chemical Route ◽  
Cubic Form ◽  
Tetragonal Form ◽  
Wet Chemical ◽  
Wet Chemical Route ◽  
Final Composition ◽  
Aluminium Nitrate Nonahydrate

Silica based ceramics are some of the most fundamental in crystal chemistry. The cristobalite form of silica has two modifications, α (low temperature, tetragonal form) and β (high temperature, cubic form). This paper describes our structural studies of unusual chemically stabilized cristobalite (CSC) material, a room temperature silica-based ceramic containing small amounts of dopants, prepared by a wet chemical route. It displays many of the structural charatcteristics of the high temperature β-cristobalite (∼270°C), but does not undergo phase inversion to α-cristobalite upon cooling. The Structure of α-cristobalite is well established, but that of β is not yet fully understood.Compositions with varying Ca/Al ratio and substitutions in cristobalite were prepared in the series, CaO:Al2O3:SiO2 : 3-x: x : 40, with x= 0-3. For CSC, a clear sol was prepared from Du Pont colloidal silica, Ludox AS-40®, aluminium nitrate nonahydrate, and calcium nitrate hexahydrate in proportions to form a final composition 1:2:40 composition.

scholarly journals Synthesis, characterization and heavy metal removal efficiency of nickel ferrite nanoparticles (NFN’s)

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Waheed Ali Khoso ◽  
Noor Haleem ◽  
Muhammad Anwar Baig ◽  
Yousuf Jamal
Keyword(s):  
Heavy Metals ◽  
Nickel Ferrite ◽  
Contact Time ◽  
Metal Removal ◽  
Heavy Metal Removal ◽  
Ferrite Nanoparticles ◽  
Batch Adsorption ◽  
Aqueous Environment ◽  
Human Beings ◽  
Nickel Ferrite Nanoparticles

AbstractThe heavy metals, such as Cr(VI), Pb(II) and Cd(II), in aqueous solutions are toxic even at trace levels and have caused adverse health impacts on human beings. Hence the removal of these heavy metals from the aqueous environment is important to protect biodiversity, hydrosphere ecosystems, and human beings. In this study, magnetic Nickel-Ferrite Nanoparticles (NFNs) were synthesized by co-precipitation method and characterized using X-Ray Diffraction (XRD), Energy Dispersive Spectroscopy (EDS) and Field Emission Scanning Electronic Microscopy (FE-SEM) techniques in order to confirm the crystalline structure, composition and morphology of the NFN’s, these were then used as adsorbent for the removal of Cr(VI), Pb(II) and Cd(II) from wastewater. The adsorption parameters under study were pH, dose and contact time. The values for optimum removal through batch-adsorption were investigated at different parameters (pH 3–7, dose: 10, 20, 30, 40 and 50 mg and contact time: 30, 60, 90, and 120 min). Removal efficiencies of Cr(VI), Pb(II) and Cd(II) were obtained 89%, 79% and 87% respectively under optimal conditions. It was found that the kinetics followed the pseudo second order model for the removal of heavy metals using Nickel ferrite nanoparticles.

Structural, spectral, electrical and magnetic parameters evaluation of Er3+-substituted Ni0·8Zn0·2Fe2O4 nanoparticles synthesized by wet chemical route

2021 ◽  
Vol 602 ◽  
pp. 412574
Author(s):  
Tahira Akhter ◽  
Muhammad Asif Yousuf ◽  
Muhammad Asghar ◽  
Ibrahim A. Alsafari ◽  
Akmal Jamil ◽  
...  
Keyword(s):  
Chemical Route ◽  
Magnetic Parameters ◽  
Wet Chemical ◽  
Wet Chemical Route
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