Changes in particle-size distribution influenced by organic matter and mechanical or ultrasonic dispersion techniques

2002 ◽  
Vol 33 (7-8) ◽  
pp. 1351-1362 ◽  
Author(s):  
Agnès Hereter ◽  
Ramon Josa ◽  
Xavier Candela
1984 ◽  
Vol 40 ◽  
Author(s):  
J. B. Blum ◽  
W. R. Cannon

AbstractFor the past two years we have been investigating the tape casting of BaTiO3 Specifically we have been interested in developing a useful tape casting formulation and procedure and in studying the effects of powder particle size distribution and dispersion processes on the forming of BaTiO3 tapes.The formulation we have developed is non-aqueous. An MEKethanol mixture is the solvent and an acrylic binder is used. Two dispersants are being used, a phosphate ester and Menhaden fish oil. Ultrasonic dispersion was found to be effective in breaking up weak powder agglomerates. We have found it important to add the dispersant before adding other organic components to obtain the best dispersion and strongest tapes. The drying method is also important to tape strength. The strongest tapes resulted when the tape was removed from the glass plate soon after casting. We have also demonstrated that for forming purposes a wide particle size distribution is preferred.


2020 ◽  
Author(s):  
Cristina Contreras ◽  
Sara Acevedo ◽  
Sofía Martínez ◽  
Carlos Bonilla

<p>Typical information in soil databases is the soil texture and particle size distribution. These properties are used for soil description or predicting other soil properties such as bulk density or hydraulic conductivity. Measuring particle size distribution with standards methods such as the pipette or hydrometer is time-consuming because of the sample pre-treatment used to remove organic matter or iron and the sample post-treatment. Nowadays, there are new methodologies for determining soil particle size distribution, such as the Integral Suspension Pressure (ISP) method, which measures the silt content in a semi-automatized process. Thus, the main objective of this study was to evaluate the suitability of the ISP method compared to standard techniques used in soil analysis and evaluate the effect of organic matter content in the ISP measurements. The main results showed that the ISP method is equivalent in accuracy to the pipette, especially for soils rich in silt or sand content. Also, the results demonstrate the convenience of removing the soil organic matter when using the ISP for soils with more than 1.5% organic matter.</p>


1982 ◽  
Vol 62 (4) ◽  
pp. 631-639 ◽  
Author(s):  
G. T. PATTERSON ◽  
G. J. WALL

Replicate soil samples (2–20) from the A, B and C horizons of 41 pedons were collected to measure within-pedon variability of particle size distribution, organic matter content, calcium carbonate equivalent and pH. Variability in soil properties was examined in relation to the mode of origin of the soil material, soil horizonation and soil drainage. Variance in particle size distribution was significantly influenced by mode of deposition as well as by soil horizons, while soil drainage had no significant influence on the variation in particle size distribution. Variance in calcium carbonate equivalent and organic matter content was not influenced by soil drainage or mode of deposition. The number of replicate samples required for statistically reliable evaluation of a pedon at given confidence limits was determined for the soil properties studied. The results of these calculations indicate the need for up to five replicate samples to achieve satisfactory levels of accuracy at the 95% confidence level for some of the soil properties studied.


2013 ◽  
Vol 37 (2) ◽  
pp. 379-391 ◽  
Author(s):  
Alexandre Hugo Cezar Barros ◽  
Quirijn de Jong van Lier ◽  
Aline de Holanda Nunes Maia ◽  
Fábio Vale Scarpare

Pedotransfer functions (PTF) were developed to estimate the parameters (α, n, θr and θs) of the van Genuchten model (1980) to describe soil water retention curves. The data came from various sources, mainly from studies conducted by universities in Northeast Brazil, by the Brazilian Agricultural Research Corporation (Embrapa) and by a corporation for the development of the São Francisco and Parnaíba river basins (Codevasf), totaling 786 retention curves, which were divided into two data sets: 85 % for the development of PTFs, and 15 % for testing and validation, considered independent data. Aside from the development of general PTFs for all soils together, specific PTFs were developed for the soil classes Ultisols, Oxisols, Entisols, and Alfisols by multiple regression techniques, using a stepwise procedure (forward and backward) to select the best predictors. Two types of PTFs were developed: the first included all predictors (soil density, proportions of sand, silt, clay, and organic matter), and the second only the proportions of sand, silt and clay. The evaluation of adequacy of the PTFs was based on the correlation coefficient (R) and Willmott index (d). To evaluate the PTF for the moisture content at specific pressure heads, we used the root mean square error (RMSE). The PTF-predicted retention curve is relatively poor, except for the residual water content. The inclusion of organic matter as a PTF predictor improved the prediction of parameter a of van Genuchten. The performance of soil-class-specific PTFs was not better than of the general PTF. Except for the water content of saturated soil estimated by particle size distribution, the tested models for water content prediction at specific pressure heads proved satisfactory. Predictions of water content at pressure heads more negative than -0.6 m, using a PTF considering particle size distribution, are only slightly lower than those obtained by PTFs including bulk density and organic matter content.


Soil Research ◽  
1979 ◽  
Vol 17 (1) ◽  
pp. 29 ◽  
Author(s):  
R Brewer

Soil fabrics at the level of related distribution of f-matrix (usually finer material) to f-members (usually coarser units) are considered in relation to particle size distribution for a number of randomly selected Australian profiles. Three major fabric continua are recognized: the chlamydic iunctic and matrigranic sequences. The majority of samples in the first two sequences have ratios of clay to silt greater and less than one, respectively, and successive stages correlate with increasing proportions of silt plus clay; fabrics of samples that fall out of sequence in relation to percentage of silt plus clay are explained on the basis of composition and/or specific processes, especially fine-grained carbonates, organic matter, faunal activity, and illuviation. The matrigranic sequence does not correlate with particle size distribution, but seems to be related to composition and/or specific processes such as faunal activity. The usefulness of the results lies in the possibility of using the conclusions to reduce the number of thin sections required to characterize areas of soil, particularly within restricted areas.


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