scholarly journals Effect of Immerse Temperature and Time on Solvent Debinding Process of Stainless Steel 316L Metal Injection Molding

Author(s):  
Nur Hafizah Kamarudin ◽  
Mohd Halim Irwan Ibrahim
2014 ◽  
Vol 607 ◽  
pp. 83-86 ◽  
Author(s):  
Rosli Asmawi ◽  
Mohd Halim Irwan Ibrahim ◽  
Azriszul Mohd Amin

This paper describes the mixing process and homogeneity analysis of a newly developed binder system based on waste polystyrene (PS) and palm kernel oil (PKO) to produce feedstock for metal injection molding (MIM). Since mixing is a critical step in MIM process, hence the mixture of powder and binder should be homogeneous and injectable. In this study, water atomised Stainless Steel powder was mixed with a new binder system consisting of waste polystyrene and palm kernel oil in a Brabender Plastograph EC rotary mixer. Several tests were performed to assess the homogeneity of the feedstock that was produced at 60 vol.% powder loadings. The 60 vol.% was chosen because the Critical Powder Volume Concentration (CPVC) of the SS316L powder was found to be 64.8 vol.%. The tests conducted were density, binder burn-out and SEM morphology observation. It was found that the feedstock shows good homogeneity and suitable for further processing in MIM.


2007 ◽  
Vol 534-536 ◽  
pp. 369-372 ◽  
Author(s):  
Kazuaki Nishiyabu ◽  
Yasuhiro Kanoko ◽  
Shigeo Tanaka

The production method of micro sacrificial plastic mold insert metal injection molding, namely μ-SPiMIM process has been proposed to solve specific problems involving the miniaturization of MIM. The sacrificial plastic mold (SP-mold) with fine structures was prepared by injection-molding polymethylmethacrylate (PMMA) into Ni-electroform, which is a typical LIGA (Lithographie-Galvanoformung-Abformung) process. Stainless steel 316L feedstock was injectionmolded into the SP-mold which had micro structures with multi-pillars. The green compact was demolded as one component with the SP-mold, which was decomposed along with binder constituent of feedstock in debinding process. This study focused on the effects of metal particle size and processing conditions on the shrinkage, transcription and surface roughness of sintered parts, which were evaluated by SEM (Scanning Electron Microscope) observation.


2021 ◽  
Vol 1028 ◽  
pp. 403-408
Author(s):  
Apang Djafar Shieddieque ◽  
Shinta Virdhian ◽  
Moch Iqbal Zaelana Muttahar ◽  
Muhammad Rafi Muttaqin

Metal injection molding (MIM) is a near net shape manufacturing technique for producing small, complex, precision parts in mass production. MIM process is manufacturing method that combines traditional shape-making capability of plastic injection molding and the materials flexibility of powder metallurgy. The process consists of the following four steps: mixing of metal powder and binder, injection molding to shape the component, debinding to remove the binder in the component, sintering to consolidate the debound parts. In this research, the physical and mechanical properties of metal injection molded 17-4 PH stainless steel were investigated with the variation of sintering temperatures (1300 °C - 1360 °C) and atmosphere conditions (argon and vacuum conditions). The relative density, microstructure, distortion, and hardness are measured and analyzed in this study. The results show that highest relative density of 87%, relative homogeneous shrinkage and high hardness are achieved by sintering at 1360 °C for 1.5 hours and argon atmosphere. At the same sintering temperature and time, sintering in vacuum shows lower relative density (81%) than that in argon condition due to pores growth. The pore growths were not observed in the argon atmosphere. It can be concluded that sintering stages more rapidly under vacuum condition. The hardness measurements result also showed that high hardness is obtained by high density parts. The optimum average hardness obtained in this study is 239 HV. However, the hardness properties results are still lower than 280 HV according to MPIF Standard 35 for MIM parts.


2010 ◽  
Vol 44-47 ◽  
pp. 2872-2876
Author(s):  
Pei Li Haw ◽  
Norhamidi Muhamad ◽  
Hadi Murthadha

The rheological behaviors of the Micro Metal Injection Molding feedstock are important for the stability of the feedstock during micro injection molding process and quality of the final micro-components. Homogeneous feedstocks are preferable for MIM process to ensure the dimensional consistency of molded components and prevent the defects of powder-binder separation or particle segregation. In this work, feedstocks with various formulations of 316L stainless steel and binder system were prepared by using Brabender Plastograph EC Plus mixer. The binder system comprises of palm stearin, polyethelene (PE) and stearic acid. In order to obtain the viscosity, activation energy, flow behavior and mold ability index, the rheological characterization of the feedstocks were investigated in numerous conditions by using Shimadzu 500-D capillary rheometer The study showed that all of the 316L stainless steel feedstocks are homogenous with pseudo-plastic behaviors.


2013 ◽  
Vol 465-466 ◽  
pp. 709-714 ◽  
Author(s):  
N.H. Mohamad Nor ◽  
Muhammad Hussain Ismail ◽  
Nur Atikah Abu Kasim ◽  
N. Muhamad ◽  
M.A. Taib

Current trend for manufacturers associated to MIM industry try to enhance the feedstock in term of its characteristics, since it is the most crucial part of the MIM process. This paper covered the characterization and rheological studies on a ready-made feedstock of stainless steel 316L which is vital to determine the availability and suit the needs of many advanced applications. There are three different experiments involved which are Scanning Electron Microscope (SEM), Differential Scanning Calorimeter (DSC), Thermogravimetric (TGA) and Capillary Rheometer. Observation through SEM gives an insight of the bonding microstructure matrices of the feedstock and also determines the homogeneity of the feedstock. DSC testing defines the melting temperature of the 3 binders used which are 62.07°C for surfactant, 178.72°C for filler and 236.61°C for backbone binder. From TGA result, it showed that the total weight loss of feedstock was 39%. Throughout the capillary rheometer testing, the feedstocks viscosity was decreasing as the shear rate increasing. The feedstock exhibits pseudoplastic behaviour since its flow behaviour index was less than 1. It is founded that at the temperature of 190°C, the feedstock exhibits the best characteristics for injection.


2013 ◽  
Vol 372 ◽  
pp. 398-401
Author(s):  
Hee Jin Jeong ◽  
Hwan Kyun Yeo ◽  
Dae Yeol Bae ◽  
Je Hyun Kim ◽  
Dong Woo Kim ◽  
...  

This study proposes the research method to examine through experiment the mechanical properties of final products based on the size and sintering temperature of powder particle during STS630 powder based metal injection molding and heat treatment processing condition after the sintering. The feedstock for the injection was manufactured based on STS630 powder with the diameter of 7.0±1.0μm and 8.0±1.0μm and the sintering was carried at 2 temperature conditions of 1300°C and 1355°C after the injection and debinding process. Heat treatment conditions of sample after the sintering were divided into 2 types thus final samples of total 8 cases were manufactured. Then, the 5 types of mechanical properties test were conducted. Optimal processing conditions for MIM molding and heat treatment of STS630 powder could be established based on it.


2001 ◽  
Vol I.01.1 (0) ◽  
pp. 509-510
Author(s):  
Yutaka KAWAMORI ◽  
Takashi MATSUOKA ◽  
Kazuhiko SAKAGUCHI ◽  
Hideki KYOGOKU

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