scholarly journals Influence of High Sintering Temperature Variation on Crystal Structure and Morphology of Nd1.2FeO3 Oxide Alloy Material by Solid-State Reaction Method

Author(s):  
E. H. Sujiono ◽  
R. A. Imran ◽  
M. Y. Dahlan ◽  
A.C. M. Said ◽  
S. Samnur ◽  
...  
Author(s):  
Hongqiang Cui ◽  
Yongze Cao ◽  
Lei Zhang ◽  
Yuhang Zhang ◽  
Siying Ran ◽  
...  

Er3+ with different concentrations doped K2Yb(PO4)(MoO4) phosphors were prepared by a solid-state reaction method, and the layered orthorhombic crystal structure of the samples was confirmed by X-ray diffraction (XRD). Under...


2013 ◽  
Vol 675 ◽  
pp. 200-204
Author(s):  
Fei Shi ◽  
Peng Cheng Du ◽  
Jing Xiao Liu ◽  
Ji Wei Wu ◽  
De Qing Chen ◽  
...  

The Mg2SiO4-MgTiO3-CaTiO3 composite dielectric ceramics with different Mg2SiO4 addition amounts were prepared by solid state reaction method. The effects of Mg2SiO4 addition amounts on the microstructure and dielectric properties as well as sintering temperature of xMg2SiO4-(0.95-x)MgTiO3-0.05CaTiO3 (abbreviated as xMSTC, 0.25≦x≦0.75) composite ceramics were investigated. The results indicated that the sintering temperature of MgTiO3-CaTiO3 based ceramics with Mg2SiO4 addition could be lowered effectively to 1320~1340°C, and the dielectric constant decreased and dielectric loss increased gradually with the increase of Mg2SiO4 content. The 0.45MSTC ceramics containing 45 wt% Mg2SiO4 and sintered at 1340°C showed desirable dielectric properties with dielectric constant εr=13.3,dielectric loss tanδ=4.5×10-4 and temperature coefficient of relative permittivity τε =10 ppm/°C.


RSC Advances ◽  
2017 ◽  
Vol 7 (56) ◽  
pp. 35305-35310 ◽  
Author(s):  
Chao Xing ◽  
Jianzhu Li ◽  
Huiling Chen ◽  
Hengyang Qiao ◽  
Jun Yang ◽  
...  

Herein, a Y(Mg1/2Sn1/2)O3 (YMS) ceramic was synthesized using a conventional solid-state reaction method.


2012 ◽  
Vol 512-515 ◽  
pp. 1488-1493 ◽  
Author(s):  
Li Hong Liu ◽  
Rong Jun Xie ◽  
Xu Dong Sun ◽  
Qing Huang ◽  
Naoto Hirosaki

This paper reports the photoluminescence properties of Ca9Eu1-xSmx(VO4)7 (x=0.2-0.4) synthesized at 1250 oC in air for 12 h using traditional solid-state reaction method. With the increase of Sm3+ substitution amount, purity Ca9Eu1-xSmx(VO4)7 phase was obtained even when the Eu3+ ions were totally substituted by Sm3+. The experimental results showed that when Sm3+ was codoped with Eu3+ into Ca9Eu1-xSmx(VO4)7 crystal structure, Sm3+ would act as a sensitizer and transfer the excitation energy to Eu3+ ions and finally enhance the emission intensity of Ca9Eu1-xSmx(VO4)7 under 405 nm excitation, which leads to more favorite of this kind of phosphor used in UV LED based white LEDs.


2016 ◽  
Vol 852 ◽  
pp. 454-460 ◽  
Author(s):  
Qiu Hong Zhang ◽  
Hai Yong Ni ◽  
Ling Li Wang ◽  
Fang Ming Xiao

Deep red emitting CaAl12-xO19:xMn4+ phosphors were synthesized by solid state reaction method. Various fluxes (BaF2, H3BO3, Na2CO3 and NH4Cl) were added in preparation of the phosphors. The influences of the various fluxes on the crystal structure, morphology and luminescent properties of CaAl12O19:Mn4+ phosphors were studied. The results show that the obtained phosphors with fluxes possessed better luminescent intensity than that of the phosphors without fluxes. The maximum luminescent intensities were found with the following order: H3BO3 (2.0 wt%) > Na2CO3 (0.5 wt%) > NH4Cl (0.3 wt%) > BaF2 (0.1 wt%) > no flux. The H3BO3 flux can decrease the single phase forming temperature of CaAl12O19:Mn4+ phosphors by about 150°C.


2016 ◽  
Vol 851 ◽  
pp. 42-45
Author(s):  
Rattanasuda Supadanaison ◽  
Theerathawan Panklang ◽  
Chalit Wanichayanan ◽  
Warayut Srithongsuk ◽  
Jaturong Junrear ◽  
...  

We investigated some properties of Y134 superconductor doped Ti superconductor. The series of samples of Y134 doped Titanium (YBa3Cu4TixO9-δ) which x=0, 0.05, 0.10, 0.15, 0.20, 0.25 were prepared by solid state reaction method with calcinations and sintering temperature at 980 °C. The porosity was reduced and the melting area were found for all Ti-doped samples. There was a little effect of Ti-doped on Tc onset but the lower of Tc offset were found that agree with the melting found on surface of sample with Ti-doped. The peritectic temperature of Y134 powder, and Y134 + 0.10Ti were on the same range about with more peak area of pure Y134 than Y134 with Ti-doping.


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