Determination of 4-Hexylresorcinol in Shrimp by Liquid Chromatography with Fluorescence Detection
2000 ◽
Vol 83
(1)
◽
pp. 241-244
◽
Keyword(s):
Abstract A method was developed to determine 4-hexylresorcinol in shrimp meat. The procedure is based on extraction of test portions with methanol followed by liquid chromatographic analysis of the extracts, using a reversed-phase column and fluorimetric detection (excitation: 280 nm, and emission: 310 nm). The confidence interval of the recovery in working range of 1.5–2.5 mg/kg was 81.6 ± 0.8%. The relative standard deviation in the working range was 2.1%. Limits of quantitation and detection were 6.59 and 1.98 ng/mL extract, respectively, corresponding to 0.26 and 0.08 mg/kg in shrimp.
1996 ◽
Vol 319
(1-2)
◽
pp. 187-190
◽
1980 ◽
Vol 26
(10)
◽
pp. 1499-1503
◽
1993 ◽
Vol 76
(1)
◽
pp. 92-94
◽
1998 ◽
Vol 708
(1-2)
◽
pp. 27-38
◽
2008 ◽
Vol 91
(3)
◽
pp. 589-597
◽
1990 ◽
Vol 526
◽
pp. 139-150
◽
Keyword(s):
1996 ◽
Vol 79
(1)
◽
pp. 43-49
◽