Three-dimensional characterization of ODS ferritic steel using by FIB-SEM serial sectioning method

Microscopy ◽  
2014 ◽  
Vol 63 (suppl 1) ◽  
pp. i23.1-i23 ◽  
Author(s):  
T. Endo ◽  
Y. Sugino ◽  
N. Ohono ◽  
S. Ukai ◽  
N. Miyazaki ◽  
...  

2020 ◽  
Vol 49 (9) ◽  
pp. 5190-5195
Author(s):  
Kenichi Ogawa ◽  
Naoya Ogawa ◽  
Ryo Kosaka ◽  
Toshiyuki Isshiki ◽  
Yongzhao Yao ◽  
...  


2019 ◽  
Vol 261 ◽  
pp. 105265 ◽  
Author(s):  
Tingting Wei ◽  
Wen Fan ◽  
Ningyu Yu ◽  
Ya-ni Wei




2019 ◽  
Vol 116 (1) ◽  
pp. 117
Author(s):  
Wang Wei ◽  
Heng Zheng ◽  
Runsheng Xu ◽  
Fenglou Wu ◽  
Weilin Chen ◽  
...  

A new analysis method based on serial sectioning and three-dimensional (3D) reconstruction was developed for the quantification of minerals in an iron ore pellet. The morphology and spatial distribution of the minerals in 3D space were analysed via 3D reconstructed images of an iron ore pellet. The volume fraction of the minerals in the 3D image was also calculated based on the pixel points. The results showed that the morphology and spatial distributions of hematite, magnetite and silicate varied among different pellets as well as among different positions within the same pellet. Thick plate and interconnected hematite was observed in the outer area of the pellets, whereas the inner area of the pellets mainly contained small granular and independent hematite. The hematite grains in pellet 1 were small, whereas those in pellet 2 were relatively dense. Some of the magnetite in pellet 1 was in the form of dense blocks, whereas fewer blocks were found in pellet 2, where magnetite occurred mainly in chain form scattered within the large particles of hematite. The silicate in pellet 2 was dense, granular and smaller than that in pellet 1. The quantitative analysis results for the two kinds of pellets showed that pellet 2 contained more hematite. Moreover, pellet 2 contained less unoxidized magnetite than pellet 1. These results indicate that the main bonding phase in pellet 1 was magnetite, whereas the main binding phase in pellet 2 was hematite. The greater compressive strength of pellet 2 was strongly related to higher amount of hematite interconnections.



2018 ◽  
Author(s):  
Seyedeh Mastooreh Seyedi Ghezghapan

We developed a three-dimensional microstructure analysis system based on the manual serial sectioning method to evaluate the heat treatment effects on chromium carbide size and morphology in AISI D2 tool steel. Two heat treatment factors, austenitizing and tempering temperature were investigated. The results show that increasing in austenitizing temperature leads to further carbide precipitation after the tempering process and increasing in the tempering temperature causes precipitate smaller secondary carbides even more than the primary carbides.



2004 ◽  
Vol 35 (7) ◽  
pp. 1927-1933 ◽  
Author(s):  
C. Zhang ◽  
M. Enomoto ◽  
A. Suzuki ◽  
T. Ishimaru


2007 ◽  
Vol 558-559 ◽  
pp. 751-756 ◽  
Author(s):  
Kristofer Hannesson ◽  
Dorte Juul Jensen

Grain structures in polycrystalline materials are typically three dimensional (3D) structures, but by far the most characterizations of grain structures are done by microscopy and are thus limited to 2D. In the present work 3D grain structures in a well-annealed cylindrical aluminium (AA1050) sample is characterized and analyzed. The characterization is done by 2 methods i) by non-destructive 3-dimensional x-ray diffraction (3DXRD) ii) by serial sectioning and subsequent EBSP mapping of entire circular 2D sample sections; 50 sections are mapped In total 333 grains are reconstructed. It is found that the 3D grain morphologies can be quite complex in particular for the larger grains, the number of neighbours varies significantly and values above 20 are not unusual. When the results from the 2 methods are compared, it is found that the crystallographic agreement is very good and within experimental uncertainties. Slightly more significant differences are found when the reconstructed grain morphologies are compared. Reasons for this are discussed.



2018 ◽  
Vol 144 ◽  
pp. 235-244 ◽  
Author(s):  
Waldemar Krieger ◽  
Sergiy V. Merzlikin ◽  
Asif Bashir ◽  
Agnieszka Szczepaniak ◽  
Hauke Springer ◽  
...  


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