Positron trapping model for point defects and grain boundaries in polycrystalline materials

2009 ◽  
Vol 79 (18) ◽  
Author(s):  
Bernd Oberdorfer ◽  
Roland Würschum
Author(s):  
J. R. Fekete ◽  
R. Gibala

The deformation behavior of metallic materials is modified by the presence of grain boundaries. When polycrystalline materials are deformed, additional stresses over and above those externally imposed on the material are induced. These stresses result from the constraint of the grain boundaries on the deformation of incompatible grains. This incompatibility can be elastic or plastic in nature. One of the mechanisms by which these stresses can be relieved is the activation of secondary slip systems. Secondary slip systems have been shown to relieve elastic and plastic compatibility stresses. The deformation of tungsten bicrystals is interesting, due to the elastic isotropy of the material, which implies that the entire compatibility stress field will exist due to plastic incompatibility. The work described here shows TEM observations of the activation of secondary slip in tungsten bicrystals with a [110] twist boundary oriented with the plane normal parallel to the stress axis.


Author(s):  
R. W. Fonda ◽  
D. E. Luzzi

The properties of polycrystalline materials are strongly dependant upon the strength of internal boundaries. Segregation of solute to the grain boundaries can adversely affect this strength. In copper alloys, segregation of either bismuth or antimony to the grain boundary will embrittle the alloy by facilitating intergranular fracture. Very small quantities of bismuth in copper have long been known to cause severe grain boundary embrittlement of the alloy. The effect of antimony is much less pronounced and is observed primarily at lower temperatures. Even though moderate amounts of antimony are fully soluble in copper, concentrations down to 0.14% can cause grain boundary embrittlement.


2008 ◽  
Vol 16 (1) ◽  
pp. 34-37 ◽  
Author(s):  
R.A. Schwarzer

Automated Crystal Orientation Microscopy (ACOM) on a grain specific level has proved to be an invaluable new tool for characterizing polycrystalline materials. It is usually based on scanning facilities using electron diffraction , due to its high sensitivity and spatial resolution, but also attempts have been made which rely upon X-ray or hard synchrotron radiation diffraction. The grain orientations are commonly mapped in pseudo-colors on the scanning grid to construct Crystal Orientation Maps (COM), which represent “images” of the microstructure with the advantage of providing quantitative orientation contrast. In a similar way, misorientations across grain boundaries, Σ values of grain boundaries, or other microstructural characteristics are visualized by mapping the grains in the micrograph with specific colors. The principal objectives are the determination of quantitative, statistically meaningful data sets of crystal orientations, misorientations, the CSL character (Σ) of grain boundaries, local crystal texture (pole figures, ODF, MODF, OCF) and derived entities, phase discrimination and phase identification.


1986 ◽  
Vol 3 (5) ◽  
pp. 237-240 ◽  
Author(s):  
Xiong Liangyue (L Y Xiong)

2000 ◽  
Vol 6 (S2) ◽  
pp. 386-387
Author(s):  
N. Ravishankar ◽  
M.T. Johnson ◽  
C. Barry Carter

The migration of grain boundaries in polycrystalline materials can occur under a variety of driving forces. Grain growth in a single-phase material and Ostwald ripening of a second phase are two common processes involving boundary migration. The mass transport in each of these cases can be related to a chemical potential difference across the grains; due to curvature in the former case and due to a difference in the chemistry in the latter case. The mass transport across grains controls the densification process during sintering. In the case of liquid-phase sintering (LPS), a liquid film may be present at the grain boundaries which results in an enhanced mass transport between grains leading to faster densification. Hence, in LPS, it is important to understand mass transport across and along a boundary containing a liquid film. The use of bicrystals and tricrystals with glass layers in the boundary can provide a controlled geometry by which to study this phenomenon.


Author(s):  
Arman Ahmadi ◽  
Narges Shayesteh Moghaddam ◽  
Mohammad Elahinia ◽  
Haluk E. Karaca ◽  
Reza Mirzaeifar

Selective laser melting (SLM) is an additive manufacturing technique in which complex parts can be fabricated directly by melting layers of powder from a CAD model. SLM has a wide range of application in biomedicine and other engineering areas and it has a series of advantages over traditional processing techniques. A large number of variables including laser power, scanning speed, scanning line spacing, layer thickness, material based input parameters, etc. have a considerable effect on SLM process materials. The interaction between these parameters is not completely studied. Limited studies on balling effect in SLM, densifications under different processing conditions, and laser re-melting, have been conducted that involved microstructural investigation. Grain boundaries are amongst the most important microstructural properties in polycrystalline materials with a significant effect on the fracture and plastic deformation. In SLM samples, in addition to the grain boundaries, the microstructure has another set of connecting surfaces between the melt pools. In this study, a computational framework is developed to model the mechanical response of SLM processed materials by considering both the grain boundaries and melt pool boundaries in the material. To this end, a 3D finite element model is developed to investigate the effect of various microstructural properties including the grains size, melt pools size, and pool connectivity on the macroscopic mechanical response of the SLM manufactured materials. A conventional microstructural model for studying polycrystalline materials is modified to incorporate the effect of connecting melt pools beside the grain boundaries. In this model, individual melt pools are approximated as overlapped cylinders each containing several grains and grain boundaries, which are modeled to be attached together by the cohesive zone method. This method has been used in modeling adhesives, bonded interfaces, gaskets, and rock fracture. A traction-separation description of the interface is used as the constitutive response of this model. Anisotropic elasticity and crystal plasticity are used as constitutive laws for the material inside the grains. For the experimental verification, stainless steel 316L flat dog bone samples are fabricated by SLM and tested in tension. During fabrication, the power of laser is constant, and the scan speed is changed to study the effect of fabrication parameters on the mechanical properties of the parts and to compare the result with the finite element model.


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