Solution small-angle X-ray scattering studies on myosin with a multiwire area detector

1991 ◽  
Vol 24 (5) ◽  
pp. 852-856 ◽  
Author(s):  
A. R. Faruqi ◽  
R. A. Cross ◽  
J. Kendrick-Jones
1997 ◽  
Vol 30 (5) ◽  
pp. 765-769 ◽  
Author(s):  
P. Fratzl ◽  
H. F. Jakob ◽  
S. Rinnerthaler ◽  
P. Roschger ◽  
K. Klaushofer

Many biological materials, like bone or wood, are hierarchically organized and optimized at all levels for their specific mechanical function. At the lowest level, these materials are fiber composites, where the fiber direction as well as the size of the individual components varies considerably with position inside a given specimen. For bone or wood, some of these parameters can be readily obtained by small-angle X-ray scattering (SAXS) in a position-resolved way. A scanning-SAXS system based on a pinhole camera with rotating anode and area detector is presented, and first applications to the study of bone and wood are reported.


2009 ◽  
Vol 16 (2) ◽  
pp. 231-236 ◽  
Author(s):  
Kaori Hattori ◽  
Ken'ichi Tsuchiya ◽  
Kazuki Ito ◽  
Yoko Okada ◽  
Kotaro Fujii ◽  
...  

The application of a two-dimensional photon-counting detector based on a micro-pixel gas chamber (µ-PIC) to high-resolution small-angle X-ray scattering (SAXS), and its performance, are reported. The µ-PIC is a micro-pattern gaseous detector fabricated by printed circuit board technology. This article describes the performance of the µ-PIC in SAXS experiments at SPring-8. A dynamic range of >105 was obtained for X-ray scattering from a polystyrene sphere solution. A maximum counting rate of up to 5 MHz was observed with good linearity and without saturation. For a diffraction pattern of collagen, weak peaks were observed in the high-angle region in one accumulation of photons.


2019 ◽  
Author(s):  
Christian Prehal ◽  
Aleksej Samojlov ◽  
Manfred Nachtnebel ◽  
Manfred Kriechbaum ◽  
Heinz Amenitsch ◽  
...  

<b>Here we use in situ small and wide angle X-ray scattering to elucidate unexpected mechanistic insights of the O2 reduction mechanism in Li-O2 batteries.<br></b>


2019 ◽  
Author(s):  
Hao Wu ◽  
Jeffrey Ting ◽  
Siqi Meng ◽  
Matthew Tirrell

We have directly observed the <i>in situ</i> self-assembly kinetics of polyelectrolyte complex (PEC) micelles by synchrotron time-resolved small-angle X-ray scattering, equipped with a stopped-flow device that provides millisecond temporal resolution. This work has elucidated one general kinetic pathway for the process of PEC micelle formation, which provides useful physical insights for increasing our fundamental understanding of complexation and self-assembly dynamics driven by electrostatic interactions that occur on ultrafast timescales.


1981 ◽  
Vol 46 (7) ◽  
pp. 1675-1681 ◽  
Author(s):  
Josef Baldrian ◽  
Božena N. Kolarz ◽  
Henrik Galina

Porosity variations induced by swelling agent exchange were studied in a styrene-divinylbenzene copolymer. Standard methods were used in the characterization of copolymer porosity in the dry state and the results were compared with related structural parameters derived from small angle X-ray scattering (SAXS) measurements as developed for the characterization of two-phase systems. The SAXS method was also used for porosity determination in swollen samples. The differences in the porosity of dry samples were found to be an effect of the drying process, while in the swollen state the sample swells and deswells isotropically.


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