Synthesis of Single-Phase Gd-Doped Ceria Nanopowders by Radio Frequency Thermal Plasma Treatment

2014 ◽  
Vol 97 (5) ◽  
pp. 1379-1382 ◽  
Author(s):  
Mi-Yeon Lee ◽  
Min-Kyung Song ◽  
Jeong-Soo Kim ◽  
Jun-Ho Seo ◽  
Min-Ho Kim
2007 ◽  
Vol 90 (6) ◽  
pp. 1717-1722 ◽  
Author(s):  
Jun Ho Seo ◽  
Dong Uk Kim ◽  
Jun Seok Nam ◽  
Sang Hee Hong ◽  
Sung Bum Sohn ◽  
...  

2020 ◽  
Vol 58 (11) ◽  
pp. 798-807
Author(s):  
Dongyoon Shin ◽  
Hyun-Woo Shim ◽  
Basudev Swain ◽  
Kyung-Soo Park ◽  
Chan-Gi Lee

Facile, economic methods of preparing tungsten (W) nanopowder are critically needed to meet industrial demand. Herein, we report a method of preparing single-phase alpha-W (α-W) nanopowders using ammonium paratungstate (APT) as a starting material and the optimum synthesis conditions. The process involves two stages: i) the radio-frequency (RF) induction thermal plasma treatment of APT, followed by ii) thermochemical reduction at 600-900 <sup>o</sup>C. The crystallographic phase and morphological evolution of all products were systematically investigated using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and transmission electron microscopy (TEM), and the effects of the annealing temperature on the phase and particle size of the obtained powders were also evaluated. When the RF induction thermal plasma treatment was conducted with and without H<sub>2</sub>, the XRD and FESEM results showed the formation of mixed-phase α- and beta-W (β-W) nanopowder and WO<sub>3</sub> nanopowder, respectively. Single-phase α-W nanopowder was achieved by annealing the WO<sub>3</sub> nanopowder in an H<sub>2</sub> reductive atmosphere at 700 <sup>o</sup>C for 10 min, resulting in homogenous nanoparticles with a small particle size (d50) of 21.16 nm without any aggregation.


Author(s):  
V. V. Azharonok ◽  
I. I. Filatova ◽  
A. P. Dostanko ◽  
S. V. Bordusov ◽  
Yu. S. Shynkevich

PLoS ONE ◽  
2012 ◽  
Vol 7 (12) ◽  
pp. e52653 ◽  
Author(s):  
Laura Brullé ◽  
Marc Vandamme ◽  
Delphine Riès ◽  
Eric Martel ◽  
Eric Robert ◽  
...  

2017 ◽  
Vol 789 ◽  
pp. 012033
Author(s):  
I S Miftakhov ◽  
A V Trofimov ◽  
A I Nagmutdinova ◽  
E F Voznesensky ◽  
F S Sharifullin ◽  
...  

2020 ◽  
Vol 992 ◽  
pp. 658-662
Author(s):  
M.A. Mokeev ◽  
L.A. Urkhanova ◽  
A.N. Khagleev ◽  
Denis B. Solovev

Mechanical, chemical and plasma treatment are the main kind of treatment of polytetrafluoroethylene (PTFE) films. Each method is different from each other by the adhesive force: the value of the wetting angle. Mechanical treatment allows different particles to permeate into the structure of the polymer. Chemical treatment creates new functional groups on the polymer surface, but this method is toxic and dangerous. Plasma treatment, in a glow discharge non-thermal plasma, is a more ecological and practical method. The experiment showed that the plasma treatment successfully increases the adhesion, this has been proven by infrared spectroscopy and scanning electron microscopy. According to the obtained data of the wetting angle, the regression equation was derived. A graphical model is constructed by regression equations allows you to determine the main processing factor and choose the optimal values of treatment.


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