Étude structurale d'une imidazolylcétone l'isopropyl-1-phényl-2-diaza-1,3-one-6-bicyclo[3,3,0]octène-2

The solid state configuration of 1-isopropyl-2-phenyl-1,3-diaza-6-one-bicyclo[3.3.0]oct-2-ene was determined from X-ray diffraction data (a = 10.039(3) Å; b = 8.683(3) Å; c = 15.505(6) Å; β = 90.72(9)°; P21/c;R = 0.047). This structure is compared to those of three other related (Δ-2)-imidazolines. Molecular structure in solution was investigated by 1H nuclear magnetic resonance spectroscopy. Results clearly indicate that the title compound has the same structure in the solid state as in solution. On the contrary, this configuration differs appreciably from those of other (Δ-2)-imidazolines considered in this report. Keywords: (Δ-2)-imidazolines, crystal structure, NMR, conformations.

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Structure and composition of gas hydrate in sediment recovered from the JAPEX/JNOC/GSC et al. Mallik 5L-38 gas hydrate production research well, determined by X-ray diffraction and Raman and solid-state nuclear magnetic resonance spectroscopy

10.4095/220808 ◽

2005 ◽

Cited By ~ 1

Author(s):

J A Ripmeester ◽

H Lu ◽

I L Moudrakovski ◽

R Dutrisac ◽

L D Wilson ◽

...

Keyword(s):

Nuclear Magnetic Resonance ◽

Solid State ◽

Magnetic Resonance ◽

Magnetic Resonance Spectroscopy ◽

Nuclear Magnetic Resonance Spectroscopy ◽

Gas Hydrate ◽

Resonance Spectroscopy ◽

X Ray Diffraction ◽

X Ray ◽

Production Research

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Combined Use of Solid-State Nuclear Magnetic Resonance Spectroscopy, Small-Angle X-Ray Diffraction, and Differential Scanning Calorimetry in Studies of Cannabinoid: Membrane Interactions

PsycEXTRA Dataset ◽

10.1037/e496242006-008 ◽

1991 ◽

Author(s):

Alexandros Makriyannis ◽

◽

De-Ping Yang ◽

Thomas Mavromoustakos

Keyword(s):

Nuclear Magnetic Resonance ◽

Differential Scanning Calorimetry ◽

Solid State ◽

Magnetic Resonance ◽

Magnetic Resonance Spectroscopy ◽

Resonance Spectroscopy ◽

X Ray Diffraction ◽

Scanning Calorimetry ◽

X Ray ◽

Combined Use

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CO2 Behavior in a Highly Selective Ultramicroporous Framework: Insights from Single-Crystal X-ray Diffraction and Solid-State Nuclear Magnetic Resonance Spectroscopy

The Journal of Physical Chemistry C ◽

10.1021/acs.jpcc.9b03221 ◽

2019 ◽

Vol 123 (29) ◽

pp. 17798-17807 ◽

Cited By ~ 4

Author(s):

Bligh E. Desveaux ◽

Y. T. Angel Wong ◽

Bryan E. G. Lucier ◽

Victor V. Terskikh ◽

Paul D. Boyle ◽

...

Keyword(s):

Nuclear Magnetic Resonance ◽

Solid State ◽

Magnetic Resonance ◽

Magnetic Resonance Spectroscopy ◽

Single Crystal ◽

Nuclear Magnetic Resonance Spectroscopy ◽

Resonance Spectroscopy ◽

X Ray Diffraction ◽

X Ray ◽

Nuclear Magnetic

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Molecular structure in the solid state (X-ray crystallography) and in solution (1H and13C nuclear magnetic resonance spectroscopy) of 1,3-diazetidines and pentasubstituted biguanides. X-Ray molecular structure of 2,4-bis-(6-methyl-3-methylthio-5-oxo-4,5-dihydro-1,2,4-triazin-4-yl)-5,5-pentamethylene-1,3-diphenylbig anide and 1,3-bis-(p-chlorophenyl)-5-dimethylamino-2,4-bis-(6-methyl-3-methylthio-5-oxo-4,5-dihydro-1,2,4-triazin-4-yl)biguanide

Journal of the Chemical Society Perkin Transactions 2 ◽

10.1039/p29900001859 ◽

1990 ◽

pp. 1859-1869 ◽

Cited By ~ 9

Author(s):

Rosa Ma Claramunt ◽

María de la Concepción Foces-Foces ◽

Félix Hernández Cano ◽

Alain Fruchier ◽

Pedro Molina ◽

...

Keyword(s):

Molecular Structure ◽

Nuclear Magnetic Resonance ◽

Solid State ◽

Magnetic Resonance ◽

Magnetic Resonance Spectroscopy ◽

Nuclear Magnetic Resonance Spectroscopy ◽

Resonance Spectroscopy ◽

X Ray ◽

X Ray Crystallography ◽

Nuclear Magnetic

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Structural investigations of natural and synthetic chlorite minerals by X-ray diffraction, mössbauer spectroscopy and solid-state nuclear magnetic resonance

Clays and Clay Minerals ◽

10.1346/ccmn.2006.0540210 ◽

2006 ◽

Vol 54 (2) ◽

pp. 252-265 ◽

Cited By ~ 20

Author(s):

Åsa Zazzi ◽

Tomas K. Hirsch ◽

Ekaterina Leonova ◽

Andrei Kaikkonen ◽

Jekabs Grins ◽

...

Keyword(s):

Nuclear Magnetic Resonance ◽

Mössbauer Spectroscopy ◽

Solid State ◽

Magnetic Resonance ◽

Mossbauer Spectroscopy ◽

X Ray Diffraction ◽

Structural Investigations ◽

X Ray ◽

Nuclear Magnetic ◽

Natural And Synthetic

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A Combined Solid-State Nuclear Magnetic Resonance and in Situ X-Ray Diffraction Study of the Lithium Deintercalation Mechanism for LiFexCo1-XPO4 (0 ≤ x ≤ 1)

ECS Meeting Abstracts ◽

10.1149/ma2013-02/12/833 ◽

2013 ◽

Keyword(s):

Nuclear Magnetic Resonance ◽

Solid State ◽

Magnetic Resonance ◽

Diffraction Study ◽

X Ray Diffraction ◽

X Ray ◽

Nuclear Magnetic

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Solid-state and solution 117Sn NMR study of C2O4(SnPh3)2: a revision

Main Group Metal Chemistry ◽

10.1515/mgmc-2012-0901 ◽

2011 ◽

Vol 34 (5-6) ◽

pp. 153-153

Author(s):

Libasse Diop

Keyword(s):

Nuclear Magnetic Resonance ◽

Solid State ◽

Magnetic Resonance ◽

State Structure ◽

X Ray Diffraction ◽

Magnetic Resonance Studies ◽

X Ray ◽

Nmr Study ◽

Tetrahedral Environment ◽

Good Agreement

Abstract Solid-state and solution 117Sn nuclear magnetic resonance studies of C2O4(SnPh3)2 have been carried out and found to be in good agreement with the tetrahedral environment of the tin (IV) atom as found from the solid state structure, previously determined by a single crystal X-ray diffraction analysis.

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