The Chemical Polishing of Single Crystal a -Alumina Using Silicon

1966 ◽  
Vol 113 (10) ◽  
pp. 1085 ◽  
Author(s):  
J. D. Filby
1967 ◽  
Vol 6 (5) ◽  
pp. 652-652 ◽  
Author(s):  
Masao Maeda ◽  
Masanobu Doken ◽  
Hiroshi Fukui

2020 ◽  
Vol 56 (8) ◽  
pp. 785-790
Author(s):  
G. P. Malanych ◽  
V. N. Tomashyk ◽  
A. A. Korchovyi

1973 ◽  
Vol 24 (2) ◽  
pp. 91-93
Author(s):  
Eiichi SATO ◽  
Toshiyasu TAMURA ◽  
Taijiro OKABE

1984 ◽  
Vol 131 (7) ◽  
pp. 1730-1731 ◽  
Author(s):  
Radoslav R. Adzic ◽  
Michael E. Hanson ◽  
Ernest B. Yeager

Author(s):  
P.E. Batson ◽  
C.R.M. Grovenor ◽  
D.A. Smith ◽  
C. Wong

In this work As doped polysilicon was deposited onto (100) silicon wafers by APCVD at 660°C from a silane-arsine mixture, followed by a ten minute anneal at 1000°C, and in one case a further ten minute anneal at 700°C. Specimens for TEM and STEM analysis were prepared by chemical polishing. The microstructure, which is unchanged by the final 700°C anneal,is shown in Figure 1. It consists of numerous randomly oriented grains many of which contain twins.X-ray analysis was carried out in a VG HB5 STEM. As K α x-ray counts were collected from STEM scans across grain and twin boundaries, Figures 2-4. The incident beam size was about 1.5nm in diameter, and each of the 20 channels in the plots was sampled from a 1.6nm length of the approximately 30nm line scan across the boundary. The bright field image profile along the scanned line was monitored during the analysis to allow correlation between the image and the x-ray signal.


Author(s):  
Akira Tanaka ◽  
David F. Harling

In the previous paper, the author reported on a technique for preparing vapor-deposited single crystal films as high resolution standards for electron microscopy. The present paper is intended to describe the preparation of several high resolution standards for dark field microscopy and also to mention some results obtained from these studies. Three preparations were used initially: 1.) Graphitized carbon black, 2.) Epitaxially grown particles of different metals prepared by vapor deposition, and 3.) Particles grown epitaxially on the edge of micro-holes formed in a gold single crystal film.The authors successfully obtained dark field micrographs demonstrating the 3.4Å lattice spacing of graphitized carbon black and the Au single crystal (111) lattice of 2.35Å. The latter spacing is especially suitable for dark field imaging because of its preparation, as in 3.), above. After the deposited film of Au (001) orientation is prepared at 400°C the substrate temperature is raised, resulting in the formation of many square micro-holes caused by partial evaporation of the Au film.


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