scholarly journals Mechanical and Tribological Properties of Carbon Thin Film with Tungsten Interlayer Prepared by Ion Beam Assisted Deposition

2013 ◽  
Vol 2013 ◽  
pp. 1-4 ◽  
Author(s):  
Petr Vlcak ◽  
Frantisek Cerny ◽  
Zdenek Tolde ◽  
Josef Sepitka ◽  
Ivan Gregora ◽  
...  

Mechanical and tribological properties of the thin carbon film with tungsten interlayer were investigated. The carbon film (130 nm) and the tungsten interlayer (20 nm) were prepared by ion beam assisted deposition (IBAD) method. Both layers were electron beam evaporated and were simultaneously irradiated by the beam of argon (Ar) or nitrogen (N) ions with energy of 700 eV. Mechanical properties of the thin carbon film with tungsten interlayer were investigated by the nanoindentation method. Concerning tribological properties the coefficient of friction was investigated by means of pin on disc tribometer. Phase composition was investigated by X-ray diffraction method (XRD), and bonding characterization of carbon thin film was characterized by Raman spectroscopy.

1994 ◽  
Vol 66 (1-3) ◽  
pp. 514-518 ◽  
Author(s):  
Yoshinori Funada ◽  
Kaoru Awazu ◽  
Kisaburo Shimamura ◽  
Hiroshi Watanabe ◽  
Masaya Iwaki

1996 ◽  
Vol 438 ◽  
Author(s):  
E. J. Tobin ◽  
F. Namavar ◽  
H. F. Karimy ◽  
C. Colerico-Stenstrom ◽  
R. J. Bricault ◽  
...  

AbstractMechanical and tribological properties of chromium-nitrogen films deposited by ion beam assisted deposition (IBAD) were investigated. The films were deposited reactively, i.e., via chromium evaporation with concurrent nitrogen ion beam bombardment, on stainless steel substrates at low deposition temperatures (<200°C). Two primary deposition regimes, with differing Cr/N atom-to-ion arrival ratios, were investigated: approximately 0.8–1.0 and 2.5–3.0. Rutherford Backscattering Spectroscopic analysis showed the lower arrival ratio films to be essentially stoichiometric CrN, whereas films deposited at higher arrival ratios were Cr-rich with Cr/N ratios of about 3:1. Both films were fine grained polycrystalline (typically 5–20 nanometer crystal dimension). The stoichiometric films were approximately two times harder than the Cr-rich films., based on nanohardness indentation measurements, and possessed higher residual stress levels. Both film types substantially improved the wear resistance of stainless steel disks, based on the results of ball-ondisk wear tests against ruby balls. The best performance was obtained with Cr-rich films, which exhibited a very low wear rate and lower friction than either the stoichiometric film or the uncoated steel.


Author(s):  
N. Kohyama ◽  
K. Fukushima ◽  
A. Fukami

Since the interlayer or adsorbed water of some clay minerals are quite easily dehydrated in dried air, in vacuum, or at moderate temperatures even in the atmosphere, the hydrated forms have not been observed by a conventional electron microscope(TEM). Recently, specific specimen chambers, “environmental cells(E.C.),” have been developed and confirmed to be effective for electron microscopic observation of wet specimen without dehydration. we observed hydrated forms of some clay minerals and their morphological changes by dehydration using a TEM equipped with an E.C..The E.C., equipped with a single hole copper-microgrid sealed by thin carbon-film, attaches to a TEM(JEM 7A) with an accelerating voltage 100KV and both gas pressure (from 760 Torr to vacuum) and relative humidity can be controlled. The samples collected from various localities in Japan were; tubular halloysite (l0Å) from Gumma Prefecture, sperical halloysite (l0Å) from Tochigi Pref., and intermediate halloysite containing both tubular and spherical types from Fukushima Pref..


Author(s):  
O. H. Kapp ◽  
M. Ohtsuki ◽  
N. Robin ◽  
S. N. Vinogradov ◽  
A. V. Crewe

Annelid extracellular hemoglobins are among the largest known proteins (M.W = 3.9 x 106), and together with the hemocyanins are the largest known oxygen carriers. They display oxygen affinities generally higher than those o vertebrate hemoglobins with Hill coefficients ranging from slightly higher than unity to values as high as 5-6. These complex molecules are composed of multiple copies of as many as six different polypeptides and posse: approximately 150 hemes per molecule.The samples were diluted to 100-200 μg/ml with distilled water just before application to a thin carbon film (∽15 Å thick). One percent (w/v) uranyl acetate solution was used for negative staining for 2 minutes and dried in air. The specimens were examined with the high resolution STEM. Their general appearance is that of a hexagonal bilayer (Fig. 1), each layer consisting of six spheroidal subunits. The corner to corner hexagonal dimensic is approximately 300 Å and the bilayer thickness approximately 200 Å.


2011 ◽  
Vol 519 (21) ◽  
pp. 7317-7320 ◽  
Author(s):  
H. Zachmann ◽  
S. Puttnins ◽  
F. Daume ◽  
A. Rahm ◽  
K. Otte

2004 ◽  
Vol 447-448 ◽  
pp. 388-391 ◽  
Author(s):  
Ari Ide-Ektessabi ◽  
Hiroki Uehara ◽  
Susumu Kamitani

1997 ◽  
Vol 226 (3-4) ◽  
pp. 212-216 ◽  
Author(s):  
Chhaya R. Kant ◽  
M.P. Srivastava ◽  
R.S. Rawat

2000 ◽  
Vol 15 (11) ◽  
pp. 2292-2295 ◽  
Author(s):  
Young-Joon Park ◽  
Young-Joon Baik ◽  
Jae Hyoung Choi ◽  
Jeong Yong Lee ◽  
Jun-Hee Hahn

BN films consisting of c-BN and h-BN phases were synthesized using an ion-beam-assisted deposition process. In contrast to conventional observations, the c-BN and h-BN phases did not form separate layers, but were distributed in the form of nano-sized grains throughout the film thickness. No distinctly aligned h-BN layer was observed before the c-BN phase. Such a mixed character of the film was attributed to a localized ion bombardment effect instead of the macro-stress. Possibly because of the presence of scattered h-BN phases, the thin film described here possessed a low hardness of about 20 GPa and a low stress of about 5 GPa, compared with other reported c-BN-containing films.


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