Evaluating Clay Microfabric Using Scanning Electron Microscopy and Digital Information Processing

Author(s):  
Dayakar Penumadu

Several aspects related to the qualitative and quantitative evaluation of clay microfabric are presented. A digital image processing technique called “intensity gradient analysis” is used in evaluating clay microfabric from scanning electron micrographs. Details are given of three computer programs (histogram.c, average.c and ellipse.c) that provide for the quantitative analysis of the orientation of clay particles. The important aspects related to sample and surface preparation, digital image acquisition, and analysis are explained. Two natural clays, Pennsylvanian fire clay and Pleistocene varved glacial lake clay, considered in the analysis show well-defined preferred and random fabric. The polar histograms of the intensity gradient analysis for the two clays are compared at varying magnifications, and conclusions were drawn. The output data was conveniently reduced to a few parameters that indicate the strength and magnitude of a given orientation. The concept of fabric index is used to quantitatively describe the preferential or randomness of clay microfabric. A simple scheme is proposed by which clay microfabric is classified as preferred when the fabric index is less than a value of 0.75 and random otherwise. The advantages of the signal intensity gradient method are that it is based on intensity changes rather than absolute values, the rosette diagrams of several micrographs can simply be added to get an overall idea, and it provides a common frame of reference for description of microfabric. The disadvantages are that it requires careful surface preparation, and the technique is valid for linear features. With the advent of inexpensive and powerful image processing tools, the technique has the potential to become a routine tool for the orientation analysis of clay micrographs seen in scanning electron microscopy.

Author(s):  
Yasushi Kokubo ◽  
Hirotami Koike ◽  
Teruo Someya

One of the advantages of scanning electron microscopy is the capability for processing the image contrast, i.e., the image processing technique. Crewe et al were the first to apply this technique to a field emission scanning microscope and show images of individual atoms. They obtained a contrast which depended exclusively on the atomic numbers of specimen elements (Zcontrast), by displaying the images treated with the intensity ratio of elastically scattered to inelastically scattered electrons. The elastic scattering electrons were extracted by a solid detector and inelastic scattering electrons by an energy analyzer. We noted, however, that there is a possibility of the same contrast being obtained only by using an annular-type solid detector consisting of multiple concentric detector elements.


Scanning ◽  
2020 ◽  
Vol 2020 ◽  
pp. 1-9
Author(s):  
Eisaku Oho ◽  
Kazuhiko Suzuki ◽  
Sadao Yamazaki

This study proposes an efficient and fast method of scanning (e.g., television (TV) scan) coupled with digital image processing technology to replace the conventional slow-scan mode as a standard model of acquisition for general-purpose scanning electron microscopy (SEM). SEM images obtained using the proposed method had the same quality in terms of sharpness and noise as slow-scan images, and it was able to suppress the adverse effects of charging in a full-vacuum condition, which is a challenging problem in this area. Two problems needed to be solved in designing the proposed method. One was suitable compensation in image quality using the inverse filter based on characteristics of the frequency of a TV-scan image, and the other to devise an accurate technique of image integration (noise suppression), the position alignment of which is robust against noise. This involved using the image montage technique and estimating the number of images needed for the integration. The final result of our TV-scan mode was compared with the slow-scan image as well as the conventional TV-scan image.


2019 ◽  
Vol 29 (1) ◽  
pp. 1226-1234
Author(s):  
Safa Jida ◽  
Hassan Ouallal ◽  
Brahim Aksasse ◽  
Mohammed Ouanan ◽  
Mohamed El Amraoui ◽  
...  

Abstract This work intends to apprehend and emphasize the contribution of image-processing techniques and computer vision in the treatment of clay-based material known in Meknes region. One of the various characteristics used to describe clay in a qualitative manner is porosity, as it is considered one of the properties that with “kill or cure” effectiveness. For this purpose, we use scanning electron microscopy images, as they are considered the most powerful tool for characterising the quality of the microscopic pore structure of porous materials. We present various existing methods of segmentation, as we are interested only in pore regions. The results show good matching between physical estimation and Voronoi diagram-based porosity estimation.


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