Rapid Determination of Active Components Inradix Isatidis Based on Near Infrared Spectroscopy and Chemometrics

2021 ◽  
Vol 11 (02) ◽  
pp. 63-68
Author(s):  
铭 贾
2013 ◽  
Vol 5 (23) ◽  
pp. 6715 ◽  
Author(s):  
Bu Haibo ◽  
Nie Lixing ◽  
Wang Dan ◽  
Yuan Shaoxiong ◽  
Li Shan ◽  
...  

2020 ◽  
Vol 110 ◽  
pp. 103138
Author(s):  
Muhammad Bilal ◽  
Zou Xiaobo ◽  
Muhmmad Arslan ◽  
Haroon Elrasheid Tahir ◽  
Muhammad Azam ◽  
...  

2019 ◽  
Vol 28 (1) ◽  
pp. 10-17
Author(s):  
Xuesong Liu ◽  
Siyu Zhang ◽  
Leting Si ◽  
Zhonglin Lin ◽  
Chunyan Wu ◽  
...  

Radix Astragali is a popular herbal medicine in the pharmaceutical industry, and many studies have confirmed its significant medical value. The objective of this study was to achieve rapid determination of the main active components (astragaloside IV and total astragalosides) in Radix Astragali using near infrared spectroscopy, mid-infrared spectroscopy, and a combination of them. Partial least squares regression was applied to establish quantitative calibration analysis models. According to the prediction results, the combined near infrared and mid-infrared spectroscopy performed better than near infrared and mid-infrared models individually. The determination coefficient and root mean square error of prediction of astragaloside IV and total astragalosides were 0.998, 0.025 and 0.998, 0.098, respectively. It can be concluded that quantitative analysis models constructed by combined near infrared and mid-infrared spectroscopy had superior performance and could be used for rapid determination of main active components in Radix Astragali.


2005 ◽  
Vol 13 (3) ◽  
pp. 169-175 ◽  
Author(s):  
Innapa Saranwong ◽  
Sumio Kawano

A system for rapid fungicide determination using near infrared spectroscopy was developed using the dry-extract system for infrared (DESIR) technique. Glass microfibre filter paper was used as the substrate. Fungicide solutions were prepared by dissolving the commercial dichlofluanid-carrying fungicide, Euparen, into acetone at concentrations of 2 ppm to 90 ppm of the active ingredient. Some techniques for adding the fungicide solutions onto the filter paper were examined. It was found that by adding 2 mL of the fungicide solution to the filter paper held in an identical size Petri dish made of polysyrene, a sufficiently accurate calibration result with SEP of 6.58 ppm could be obtained. In the following step, the technique was applied to the determination of fungicide on tomato surfaces. The fungicide was extracted from the fruit by washing with acetone. Then, the acetone solution was used for the DESIR embedding instead of the fungicide solution in the first experiment. A satisfactory result, with an SEP of 7.89 ppm for the washed solution that was equivalent to approximately 1.58 ppm per gram fruit weight, could be obtained.


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