scholarly journals Effect of decontamination methods on shear bond strength of resin cement to translucent monolithic zirconia

2020 ◽  
Vol 23 (4) ◽  
pp. 9p
Author(s):  
Mazen Ahmed Attia ◽  
Kamal Khaled Ebeid
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Strength Test ◽  
Resin Cement ◽  
Adhesive Resin ◽  
Tukey Test ◽  
Significant Difference ◽  
Monolithic Zirconia ◽  
Adhesive Resin Cement ◽  
Saliva Contamination

Objective. The aim of this study was to evaluate the effect of decontamination methods on shear bond strength of resin cement to translucent monolithic zirconia. Material and Methods. Eighty 4-mol yttria-stabilized tetragonal zirconia polycrystal specimens were fabricated. All specimens were subjected to saliva contamination and divided into four groups (n=20) according to the decontamination methods: 70% isopropanol (AL); zirclean (ZC); 5.25% sodium  ypochlorite (NaOCL); and no cleaning (NC). All specimens were bonded by using self-adhesive resin cement. Half of the specimens in each group (n=10) were subjected to thermocycling. All specimens were subjected to shear bond strength test in a universal testing machine. Failure modes were evaluated by using a scanning electron microscope (SEM). The data obtained were statistically analyzed by using one-way ANOVA followed by the HSD Tukey test (P < 0.05). Results. ANOVA test revealed a significant difference among the different decontamination methods (P < 0.05). No significant differences were found among NaOCL, ZC, and AL groups as revealed by the HSD Tukey test (P > 0.05). The effect of thermocycling was significantly different in all groups (P < 0.05); whereas, no significant difference was found in group ZC (P > 0.05). (SEM) analysis showed mixed failures in all groups except in group NC where only adhesive failure was observed. Conclusion. Saliva contamination during clinical evaluation significantly decreases the shear bond strength between self-adhesive resin cement and translucent monolithic zirconia. The cleaning gel has an impact on improving the bond strength between resin cement and translucent monolithic zirconia.   KEYWORDS Monolithic zirconia; Resin cement; Shear bond strength test; Translucent zirconia; Zirclean.

scholarly journals Influence of Different Surface Pretreatments on Shear Bond Strength of an Adhesive Resin Cement to Various Zirconia Ceramics

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 652 ◽  
Author(s):  
Marco Colombo ◽  
Simone Gallo ◽  
Sara Padovan ◽  
Marco Chiesa ◽  
Claudio Poggio ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Adhesive Resin ◽  
Surface Pretreatment ◽  
Significant Difference ◽  
Computer Aided ◽  
Adhesive Resin Cement

The aim of this in vitro study was to assess the influence of surface pretreatment on shear bond strength (SBS) of an adhesive resin cement (G-CEM Link Force TM, GC Corporation, Tokyo, Japan) to three different yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramics: (1) Copran Zirconia Monolith HT, COP; (2) Katana ML Zirconia, KAT; and (3) Metoxit Z-CAD HTL Zirconia, MET. In total, 45 cylinders (5 mm in diameter, 1 mm height) for each type of zirconia ceramic were prepared used a computer-aided design and computer-aided manufacturing (CAD/CAM) machine (software CEREC 4.2). Each type of zirconia was subdivided into three groups and each group received a different surface pretreatment; 15 samples were not conditioned as control (groups COP 1, KAT 1, MET 1), 15 samples were air-borne particle abraded with aluminum dioxide particles of 50-μm size at 0.3 MPa for 20 s (groups COP 2, KAT 2, MET 2), and 15 samples were hot-etched with a solution of hydrochloric acid and ferric chloride (groups COP 3, KAT 3, MET 3). After specimen fabrication, the adhesive cement–ceramic interface was analyzed using an SBS test. Subsequently, the adhesive remnant index (ARI) was measured. Data were submitted to statistical analysis. Air-borne particle abraded specimens showed the highest SBS values for COP and KAT groups. For MET, no significant difference was reported between air-borne particle abraded specimens and untreated controls. The lowest values were detected for acid-etched groups. A higher frequency of ARI = “1” and ARI = “2” was reported in control and air-borne particle abraded groups, whereas ARI = “3” was detected in hot-etched groups. No correlation was found between ARI score and shear bond strength. Air-borne particle abrasion is considered the best treatment for Zirconia Copran and Zirconia Katana ML, if it is followed by using dual-curing resin cement.

Development of a Cavity Disinfectant Containing Antibacterial Monomer MDPB

2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  
Keyword(s):  
Antibacterial Activity ◽  
Bond Strength ◽  
Bacterial Species ◽  
Oral Bacteria ◽  
Resin Cement ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Adhesive Resin Cement

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.

Shear bond strength of a self-adhesive resin cement to resin-coated dentin

2013 ◽  
Vol 51 (1) ◽  
pp. 27
Author(s):  
Jee-Youn Hong ◽  
Cheol-Woo Park ◽  
Jeong-Uk Heo ◽  
Min-Ki Bang ◽  
Jae-Jun Ryu
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Cement ◽  
Adhesive Resin ◽  
Adhesive Resin Cement

scholarly journals Influence of Non-Thermal Atmospheric Pressure Plasma Treatment on Shear Bond Strength between Y-TZP and Self-Adhesive Resin Cement

Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3321 ◽  
Author(s):  
Dae-Sung Kim ◽  
Jong-Ju Ahn ◽  
Eun-Bin Bae ◽  
Gyoo-Cheon Kim ◽  
Chang-Mo Jeong ◽  
...  
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Atmospheric Pressure ◽  
Shear Bond Strength ◽  
Atmospheric Pressure Plasma ◽  
Resin Cement ◽  
Control Group ◽  
Adhesive Resin ◽  
Pressure Plasma ◽  
Adhesive Resin Cement

The purpose of this study was to evaluate the effect of non-thermal atmospheric pressure plasma (NTP) on shear bond strength (SBS) between yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) and self-adhesive resin cement. For this study, surface energy (SE) was calculated with cube-shaped Y-TZP specimens, and SBS was measured on disc-shaped Y-TZP specimens bonded with G-CEM LinkAce or RelyX U200 resin cylinder. The Y-TZP specimens were classified into four groups according to the surface treatment as follows: Control (no surface treatment), NTP, Sb (Sandblasting), and Sb + NTP. The results showed that the SE was significantly higher in the NTP group than in the Control group (p < 0.05). For the SBS test, in non-thermocycling, the NTP group of both self-adhesive resin cements showed significantly higher SBS than the Control group (p < 0.05). However, regardless of the cement type in thermocycling, there was no significant increase in the SBS between the Control and NTP groups. Comparing the two cements, regardless of thermocycling, the NTP group of G-CEM LinkAce showed significantly higher SBS than that of RelyX U200 (p < 0.05). Our study suggests that NTP increases the SE. Furthermore, NTP increases the initial SBS, which is higher when using G-CEM LinkAce than when using RelyX U200.

Evaluation of the Microshear Bond Strength of MDP-containing and Non–MDP-containing Self-adhesive Resin Cement on Zirconia Restoration

2019 ◽  
Vol 44 (4) ◽  
pp. 379-385 ◽  
Author(s):  
EJ Go ◽  
Y Shin ◽  
JW Park
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Exact Test ◽  
Tukey Test ◽  
Significant Difference ◽  
Post Hoc ◽  
Microshear Bond Strength

SUMMARY Objectives: The purpose of this study was to measure the microshear bond strength (μSBS) of four different self-adhesive resin cements with/without 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing primer to zirconium ceramics and to evaluate the effect of zirconia primers on these self-adhesive resin cements (SARCs). Methods and Materials: Zirconia blocks (20 × 20 × 8 mm3) were prepared and divided into eight groups (n=20). They were sandblasted (50 μm Al2O3) and treated as follows: no primer or primer (Z-Primer Plus). Four self-adhesive resin cements (MDP-containing: Permacem 2.0 [PC], Clearfil SA luting [CS]; non–MDP-containing: Rely-X U200 [RU], Maxcem Elite [ME]) were bonded to the zirconia surface. After thermocycling, a μSBS test was performed. The failure mode was analyzed using light microscopy. Statistical analysis of μSBS was performed using one-way analysis of variance and two-sample t-test with post hoc Tukey test. The loss rate was evaluated using the Fisher's exact test and χ2 test with post hoc Tukey test (p&lt;0.05). Results: Within the no primer groups, the PC and CS groups showed higher bond strength than the RU and ME groups. Comparing the μSBS of the no primer and primer groups in the same SARCs, the RU/P group was higher than the RU group, and the ME/P group was higher than the ME group. No significant difference was observed between the PC and PC/P groups and between the CS and CS/P groups. Conclusions: Non–MDP-containing SARC showed the increased bonding value with MDP-containing primer to zirconia ceramics. The bond strength of MDP-containing SARCs was not affected significantly by the use of zirconia primer.

The Effect of Aging and Surface treatments on Micro-shear Bond Strength of Resin Nano-Ceramic Material Using Two Resin Cements

2020 ◽  
Author(s):  
Ayman Mohammed Said
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Surface Treatments ◽  
Resin Cement ◽  
Acid Etching ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Mean Values ◽  
Adhesive Resin Cement

Purpose: To evaluate the effect of aging and different surface treatments on micro-shear bond strength of two resin cements to resin nano-ceramic composite blocks using an in-vitro study. Materials and methods: Blocks of resin nano-ceramic (Lava Ultimate, 3M, St Paul, Minnesota, USA) were used to prepare eight plates having the following dimensions: (14mm × 12mm × 2mm). After plates preparation they were assigned to two main groups according to the surface treatment applied, either hydrofluoric acid etching and silane or sandblasting and silane. Scanning electron microscope (SEM) was used to analyze the surface topography of the Lava-Ultimate plates before and after application of surface treatments. Two resin cements were used; dual cured adhesive resin cement (Bifix QM, VOCO, Cuxhafen, Germany) and dual cured self-adhesive resin cement (Bifix SE, VOCO, Cuxhafen, Germany) to create a five resin micro-cylinders received on each lava ultimate plate. Ten specimens from each subgroup were tested after 24 hours and the other ten specimens were tested after aging in saline for 6 months. Micro-shear bond strength test was applied until failure. . Multi-factorial ANOVA test and One-way ANOVA followed by pair-wise Tukey’s post-hoc tests were used to analyze the data. Results: Both resin cements showed statistically significant decrease on bond strength after aging. Before aging, both surface treatments with adhesive resin cement showed statistically significant higher micro-shear bond strength mean values than with self-adhesive resin cement. After aging sandblasting showed a statistically significant higher micro-shear bond strength mean values with adhesive resin cement, while hydrofluoric acid etching revealed a statistically non-significant higher values with adhesive resin cement than self-adhesive resin cement. Conclusion: For both surface treatments and resin cements aging had a detrimental effect on micro- shear bond strength.

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