scholarly journals Influence of Different Surface Pretreatments on Shear Bond Strength of an Adhesive Resin Cement to Various Zirconia Ceramics

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 652 ◽  
Author(s):  
Marco Colombo ◽  
Simone Gallo ◽  
Sara Padovan ◽  
Marco Chiesa ◽  
Claudio Poggio ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Adhesive Resin ◽  
Surface Pretreatment ◽  
Significant Difference ◽  
Computer Aided ◽  
Adhesive Resin Cement

The aim of this in vitro study was to assess the influence of surface pretreatment on shear bond strength (SBS) of an adhesive resin cement (G-CEM Link Force TM, GC Corporation, Tokyo, Japan) to three different yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramics: (1) Copran Zirconia Monolith HT, COP; (2) Katana ML Zirconia, KAT; and (3) Metoxit Z-CAD HTL Zirconia, MET. In total, 45 cylinders (5 mm in diameter, 1 mm height) for each type of zirconia ceramic were prepared used a computer-aided design and computer-aided manufacturing (CAD/CAM) machine (software CEREC 4.2). Each type of zirconia was subdivided into three groups and each group received a different surface pretreatment; 15 samples were not conditioned as control (groups COP 1, KAT 1, MET 1), 15 samples were air-borne particle abraded with aluminum dioxide particles of 50-μm size at 0.3 MPa for 20 s (groups COP 2, KAT 2, MET 2), and 15 samples were hot-etched with a solution of hydrochloric acid and ferric chloride (groups COP 3, KAT 3, MET 3). After specimen fabrication, the adhesive cement–ceramic interface was analyzed using an SBS test. Subsequently, the adhesive remnant index (ARI) was measured. Data were submitted to statistical analysis. Air-borne particle abraded specimens showed the highest SBS values for COP and KAT groups. For MET, no significant difference was reported between air-borne particle abraded specimens and untreated controls. The lowest values were detected for acid-etched groups. A higher frequency of ARI = “1” and ARI = “2” was reported in control and air-borne particle abraded groups, whereas ARI = “3” was detected in hot-etched groups. No correlation was found between ARI score and shear bond strength. Air-borne particle abrasion is considered the best treatment for Zirconia Copran and Zirconia Katana ML, if it is followed by using dual-curing resin cement.

Bond Strength Stability of Self-adhesive Resin Cement to Etched Vitrified Yttria-stabilized Tetragonal Zirconia Polycrystal Ceramic After Thermomechanical Cycling

2019 ◽  
Vol 44 (5) ◽  
pp. 545-555 ◽  
Author(s):  
EV Maroun ◽  
JGA Guimarães ◽  
WG de Miranda ◽  
LRC Netto ◽  
AB Elias ◽  
...  
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Adhesive Resin ◽  
Thermomechanical Cycling ◽  
Significant Difference ◽  
Ceramic Blocks ◽  
Adhesive Resin Cement ◽  
Tetragonal Zirconia Polycrystal

SUMMARY The purpose of this study was to evaluate the influence of thermomechanical cycling on the bond strength stability of self-adhesive resin cement to vitrified yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) ceramic. Y-TZP ceramic blocks were divided into four groups according to the surface treatments: AS, as sintered; SB, sandblasted with 50-μm Al2O3 particles; LG, vitrification with a low-fusing glaze and etching with 10% hydrofluoric acid; and HC, vitrification with a ceramic liner and etching with 10% hydrofluoric acid. Lithium disilicate ceramic blocks etched with 10% hydrofluoric acid for 20 seconds (EM) were also tested. Blocks of resin composite were cemented on the ceramic block surfaces using a self-adhesive resin cement. Half of the blocks from each group were cut into beams and submitted to microtensile bond strength (μTBS) testing after immersion in water at 37°C for 24 hours and the other half after mechanical (1,200,000 cycles, 98 N, 2.5 Hz) and thermal (10,000 cycles, 5-55°C, 30-second dwell time) cycling (TMC). Data were analyzed using one-way analysis of variance, Tukey's honest significant difference post hoc test, and Student t-test (α=0.05). After 24 hours, EM and LG presented similar and the highest μTBS, whereas AS showed the lowest μTBS (p<0.05). After TMC, EM presented the highest μTBS, followed by LG (p<0.05). Only EM and LG maintained the stability of μTBS after TMC (p>0.05). The bonding to Y-TZP ceramic vitrified with a low-fusing glaze withstood thermomechanical cycling.

The Effect of Sandblasting and Different Primers on Shear Bond Strength Between Yttria-tetragonal Zirconia Polycrystal Ceramic and a Self-adhesive Resin Cement

2015 ◽  
Vol 40 (1) ◽  
pp. 63-71 ◽  
Author(s):  
Y-A Yi ◽  
J-S Ahn ◽  
Y-J Park ◽  
S-H Jun ◽  
I-B Lee ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Xrd Analysis ◽  
Resin Cement ◽  
Air Abrasion ◽  
Adhesive Resin ◽  
Multiple Comparison Test ◽  
Adhesive Resin Cement ◽  
Tetragonal Zirconia Polycrystal

SUMMARY Purpose To evaluate the effect of zirconia primers, air-abrasion, and tribochemical surface treatment methods on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramic and self-adhesive resin cement. Methods and Materials Y-TZP ceramic surfaces were ground flat with 600-grit silicon carbide paper and then divided into seven groups of 10 and treated as follows: untreated (control), Monobond Plus, Z-PRIME Plus, ESPE Sil with CoJet, air-abrasion, Monobond Plus with air-abrasion, and Z-PRIME Plus with air-abrasion. Self-adhesive resin cement was placed onto the treated Y-TZP specimens for each group. All specimens were thermocycled and subjected to a shear bond strength test. Scanning electron microscope images of the fractured areas and x-ray diffraction (XRD) analysis of the surface-treated Y-TZP specimens were performed. Data were statistically analyzed using one-way analysis of variance and the Student-Newman-Keuls multiple comparison test (p<0.05). Results The Z-PRIME Plus treatment in combination with air-abrasion produced the highest bond strength (16.50±2.26 MPa), followed by air-abrasion (10.56±3.32 MPa), and then Monobond Plus combined with air-abrasion (8.93±3.13 MPa), ESPE Sil after CoJet application (8.54±3.98 MPa), and the Z-PRIME Plus group (8.27±2.79 MPa). The control (3.91±0.72 MPa) and Monobond Plus (4.86±1.77 MPa) groups indicated the lowest results (p<0.05). The XRD results showed the peaks of the monoclinic phase for the air-abrasion and CoJet treatment groups compared with the Y-TZP control. Conclusion Z-PRIME Plus primer application after air-abrasion presented the best results for improving the bond strength between Y-TZP ceramic and self-adhesive resin cement.

scholarly journals Shear Bond Strength of MDP-Containing Self-Adhesive Resin Cement and Y-TZP Ceramics: Effect of Phosphate Monomer-Containing Primers

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Jin-Soo Ahn ◽  
Young-Ah Yi ◽  
Yoon Lee ◽  
Deog-Gyu Seo
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Control Group ◽  
Air Abrasion ◽  
Adhesive Resin ◽  
Multiple Comparison Test ◽  
Ceramic Surfaces ◽  
Adhesive Resin Cement

Purpose. This study was conducted to evaluate the effects of different phosphate monomer-containing primers on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramics and MDP-containing self-adhesive resin cement.Materials and Methods. Y-TZP ceramic surfaces were ground flat with #600-grit SiC paper and divided into six groups (n=10). They were treated as follows: untreated (control), Metal/Zirconia Primer, Z-PRIME Plus, air abrasion, Metal/Zirconia Primer with air abrasion, and Z-PRIME Plus with air abrasion. MDP-containing self-adhesive resin cement was applied to the surface-treated Y-TZP specimens. After thermocycling, a shear bond strength test was performed. The surfaces of the Y-TZP specimens were analyzed under a scanning electron microscope. The bond strength values were statistically analyzed using one-way analysis of variance and the Student–Newman–Keuls multiple comparison test (P<0.05).Results. The Z-PRIME Plus treatment combined with air abrasion produced the highest bond strength, followed by Z-PRIME Plus application, Metal/Zirconia Primer combined with air abrasion, air abrasion alone, and, lastly, Metal/Zirconia Primer application. The control group yielded the lowest results (P<0.05).Conclusion. The application of MDP-containing primer resulted in increased bond strength between Y-TZP ceramics and MDP-containing self-adhesive resin cements.

scholarly journals Effect of decontamination methods on shear bond strength of resin cement to translucent monolithic zirconia

2020 ◽  
Vol 23 (4) ◽  
pp. 9p
Author(s):  
Mazen Ahmed Attia ◽  
Kamal Khaled Ebeid
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Strength Test ◽  
Resin Cement ◽  
Adhesive Resin ◽  
Tukey Test ◽  
Significant Difference ◽  
Monolithic Zirconia ◽  
Adhesive Resin Cement ◽  
Saliva Contamination

Objective. The aim of this study was to evaluate the effect of decontamination methods on shear bond strength of resin cement to translucent monolithic zirconia. Material and Methods. Eighty 4-mol yttria-stabilized tetragonal zirconia polycrystal specimens were fabricated. All specimens were subjected to saliva contamination and divided into four groups (n=20) according to the decontamination methods: 70% isopropanol (AL); zirclean (ZC); 5.25% sodium  ypochlorite (NaOCL); and no cleaning (NC). All specimens were bonded by using self-adhesive resin cement. Half of the specimens in each group (n=10) were subjected to thermocycling. All specimens were subjected to shear bond strength test in a universal testing machine. Failure modes were evaluated by using a scanning electron microscope (SEM). The data obtained were statistically analyzed by using one-way ANOVA followed by the HSD Tukey test (P < 0.05). Results. ANOVA test revealed a significant difference among the different decontamination methods (P < 0.05). No significant differences were found among NaOCL, ZC, and AL groups as revealed by the HSD Tukey test (P > 0.05). The effect of thermocycling was significantly different in all groups (P < 0.05); whereas, no significant difference was found in group ZC (P > 0.05). (SEM) analysis showed mixed failures in all groups except in group NC where only adhesive failure was observed. Conclusion. Saliva contamination during clinical evaluation significantly decreases the shear bond strength between self-adhesive resin cement and translucent monolithic zirconia. The cleaning gel has an impact on improving the bond strength between resin cement and translucent monolithic zirconia.   KEYWORDS Monolithic zirconia; Resin cement; Shear bond strength test; Translucent zirconia; Zirclean.

Development of a Cavity Disinfectant Containing Antibacterial Monomer MDPB

2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  
Keyword(s):  
Antibacterial Activity ◽  
Bond Strength ◽  
Bacterial Species ◽  
Oral Bacteria ◽  
Resin Cement ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Adhesive Resin Cement

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.

Shear bond strength of a self-adhesive resin cement to resin-coated dentin

2013 ◽  
Vol 51 (1) ◽  
pp. 27
Author(s):  
Jee-Youn Hong ◽  
Cheol-Woo Park ◽  
Jeong-Uk Heo ◽  
Min-Ki Bang ◽  
Jae-Jun Ryu
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Cement ◽  
Adhesive Resin ◽  
Adhesive Resin Cement

scholarly journals Effect of cleaning agent, primer application and their combination on the bond strength of a resin cement to two yttrium-tetragonal zirconia polycrystal zirconia ceramics

2017 ◽  
Vol 11 (01) ◽  
pp. 006-011 ◽  
Author(s):  
William Matthew Negreiros ◽  
Glaucia Maria Bovi Ambrosano ◽  
Marcelo Giannini
Keyword(s):  
Bond Strength ◽  
Water Storage ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Coupling Agents ◽  
Zirconia Ceramics ◽  
Cleaning Agent ◽  
Failure Data ◽  
Significant Difference

ABSTRACT Objective: The objective of this study is to evaluate the effect of a cleaning agent and priming on the bond strength (BS) of a resin cement (RC) to zirconia ceramics after 24 h and 1 year of water-storage. Materials and Methods: Fifty-six Katana and 56 ZirCAD zirconia ceramic plates were prepared and each zirconia brand was divided into four groups (n = 14): (1) untreated; (2) treated with Ivoclean cleaning agent; (3) treated with Monobond Plus coupling agent; (4) treated with Ivoclean + Monobond Plus. Cleaning and coupling agents were applied to zirconia following the manufacturers' instructions. The RC was manipulated, inserted into tubes (0.75 mm diameter/1 mm height) that were positioned on the zirconia surfaces and light activated. Specimens were tested after 24 h and 1 year of water storage. A shear load was applied to the base of the RC cylinders (until failure. Data were analyzed by three-way ANOVA and Tukey tests (α = 5%). Results: No significant difference in BS was noted between zirconia ceramics, except when the combination of cleaning and coupling agents was used. This combination increased the BS for Katana zirconia. One year of water storage leads to a decrease in BS for all experimental groups. Conclusion: The combination of cleaning agent and priming can yield higher BS for Katana at 24 h. BS to zirconia ceramics reduced approximately 50% after 1 year.

scholarly journals Micro-Raman Vibrational Identification of 10-MDP Bond to Zirconia and Shear Bond Strength Analysis

2017 ◽  
Vol 2017 ◽  
pp. 1-7 ◽  
Author(s):  
Diego Martins De-Paula ◽  
Alessandro D. Loguercio ◽  
Alessandra Reis ◽  
Natasha Marques Frota ◽  
Radamés Melo ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Bond Strength ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Strength Analysis ◽  
Dihydrogen Phosphate ◽  
Adhesive Resin ◽  
Micro Raman Spectroscopy ◽  
Adhesive Resin Cement ◽  
Microshear Bond Strength

So far, there is no report regarding the micro-Raman vibrational fingerprint of the bonds between 10-methacryloyloxy-decyl dihydrogen phosphate (10-MDP) and zirconia ceramics. Thus, the aim of this study was to identify the Raman vibrational peaks related to the bonds of 10-MDP with zirconia, as well as the influence on microshear bond strength. Micro-Raman spectroscopy was employed to assess the vibrational peak of 10-MDP binding to zirconia. Microshear bond strength of the dual-cure resin cement to zirconia with the presence of 10-MDP in composition of experimental ceramic primer and self-adhesive resin cement was also surveyed. Statistical analysis was performed by one-way ANOVA and Tukey’s test (p<0.05). Peaks at 1545 cm−1 and 1562 cm−1 were found to refer to zirconia binding with 10-MDP. The presence of 10-MDP in both experimental ceramic primer and self-adhesive resin cement improved microshear bond strength to zirconia ceramic. It can be concluded that the nondestructive method of micro-Raman spectroscopy was able to characterize chemical bonds of 10-MDP with zirconia, which improves the bond strengths of resin cement.

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