Effect of Drying on Porous Characteristics of Orange Peel

2016 ◽  
Vol 12 (9) ◽  
pp. 921-928 ◽  
Author(s):  
Cansu Tamer ◽  
Asli Isci ◽  
Naciye Kutlu ◽  
Ozge Sakiyan ◽  
Serpil Sahin ◽  
...  

Abstract The purpose of the study was to determine the effects of different temperatures (40, 50 and 60 °C) and air velocities (1 and 2 m/s) on shrinkage, porosity, pore size distribution, color and microstructure of orange peel. Empirical models were also proposed to predict shrinkage and porosity as a function of moisture. A strong negative correlation was determined between moisture and shrinkage. Air temperature had no significant impact on the final shrinkage and porosity values. During drying, porosity of the samples first increased until a critical value, at which point further decrease in moisture resulted in collapse of pores. The porosity of the orange peel was correlated with moisture by a third-order polynomial. Pore size distribution curve of raw sample showed two major peaks, a wider and a sharper peak at around 19.8 and 7.18 μm, respectively. After drying, the peaks became shorter and the curve shifted to the left, indicating that the amount of pores and their diameter decreased. The SEM analysis revealed that at extreme process conditions, the orange peel surface was cracked and the characteristic distribution of the waxy components was obstructed.

1991 ◽  
Vol 251 ◽  
Author(s):  
Atsushi Takata ◽  
K. Ishizaki ◽  
Y. Kondo ◽  
T. Shioura

ABSTRACTOpen porous copper metals, which have high strength, high open porosity and well controlled pore size distribution, were produced by a hot isostatic press (HIP) process. They were sintered at different temperatures from 973 to 1273K under various HIPping pressures up to 200MPa. Pore size distribution and Young's modulus of the sintered samples were analyzed. The HIPped products have greater strength and higher open porosity than those of the normally sintered ones. The internal structural parameters such as pore size distribution were controlled by changing the HIPping pressure.


2019 ◽  
Author(s):  
Paul Iacomi ◽  
Philip L. Llewellyn

Material characterisation through adsorption is a widely-used laboratory technique. The isotherms obtained through volumetric or gravimetric experiments impart insight through their features but can also be analysed to determine material characteristics such as specific surface area, pore size distribution, surface energetics, or used for predicting mixture adsorption. The pyGAPS (python General Adsorption Processing Suite) framework was developed to address the need for high-throughput processing of such adsorption data, independent of the origin, while also being capable of presenting individual results in a user-friendly manner. It contains many common characterisation methods such as: BET and Langmuir surface area, t and α plots, pore size distribution calculations (BJH, Dollimore-Heal, Horvath-Kawazoe, DFT/NLDFT kernel fitting), isosteric heat calculations, IAST calculations, isotherm modelling and more, as well as the ability to import and store data from Excel, CSV, JSON and sqlite databases. In this work, a description of the capabilities of pyGAPS is presented. The code is then be used in two case studies: a routine characterisation of a UiO-66(Zr) sample and in the processing of an adsorption dataset of a commercial carbon (Takeda 5A) for applications in gas separation.


Author(s):  
Hong Qian ◽  
Ying Fang ◽  
Kao Wu ◽  
Hao Wang ◽  
Bin Li ◽  
...  

Abstract This study presents two methods to improve the air filtration performance of konjac glucomannan (KGM)-based aerogel air filters through physical structure design by changing the pore-size distribution and the surface area, using an air purifier. Results indicated that KGM-based aerogels had a comparable filtration effect with the commercial air filter with a longer purification time. This purification time could be shortened by over 50%, by changing the pore-size distribution from large size to small size or increase the surface area with the fold structure. This should boost the development of polysaccharide-based aerogel used as the air filter.


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