Effects of Grain Size and Carbides on the Creep Resistance and Rupture Properties of a Conventionally Cast Nickel-Base Superalloy / Die Einflüsse von Korngröße und Karbidteilchen auf die Kriechfestigkeit und die Brucheigenschaften einer gegossenen Nickel-Basis-Superlegierung

Author(s):  
Ahmet Baldan
Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1978 ◽  
Author(s):  
Xianqiang Fan ◽  
Zhipeng Guo ◽  
Xiaofeng Wang ◽  
Jie Yang ◽  
Jinwen Zou

A pre-hot-deformation process was applied for a polycrystalline nickel-base superalloy to active deformation twins and dislocations, and subsequent slow cooling treatment was used to achieve grain refinement and microstructure homogenization. The microstructural evolution of the alloy was investigated, and the corresponding underlying mechanism was discussed. It was found that twinning mainly occurred in large grains during pre-hot-deformation owing to the stress concentration surrounding the large grains. High density dislocations were found in large grains, and the dislocation density increased approaching the grain boundary. The average grain size was refined from 30 μm to 13 μm after slow cooling with a standard deviation of grain size decreasing from 10.8 to 2.8, indicating a homogeneous microstructure. The grain refinement and microstructure homogenization during cooling process could be achieved via (i) static recrystallization (SRX), (ii) interaction of twin tips and γ’ precipitates, and (iii) grain coarsening hindered by γ’ precipitates in grain boundaries.


2010 ◽  
Vol 654-656 ◽  
pp. 484-487
Author(s):  
Zhi Long Zhao ◽  
Chang Hui Ai ◽  
Lin Liu

Inconel 718C is a nickel-base alloy that is difficult to machine. This paper presents a study of the influence of grain size in as-cast workpieces on cutting forces of Inconel 718C. The end milling tests were performed to understand the effect of various grain structures on machinability of nickel-base superalloy under wet condition using carbide insert. The collected data of cutting forces were analyzed using polynomial regression methods. The results show that grain refining of Inconel 718C can effectively decrease cutting force and improve the machinability of nickel-base superalloy.


Author(s):  
Kannan Subramanian ◽  
Harish P. Cherukuri

Superalloys are metallic alloys used for high temperature applications such as encountered in the aircraft industry and where resistance to deformation is a primary requirement. Alloy 718 is one such Nickel-base superalloy that resists deformation at elevated temperatures and is therefore difficult to hot work. One of the major hotworking operations is multi-pass shape rolling in which Alloy 718 undergoes multiple deformations in several passes along with reheating between passes. For a given composition of alloy, the high temperature flow stress is influenced to a large extent by the grain size of the microstructure. In the case of shape rolling in which the cross section changes from circular to oval in alternate passes, the correct working forces, which relate to gauge and shape control as well as to power requirements, can be estimated accurately only if the microstructure relevant to the specific pass of rolling is known. In addition, the microstructure present at the end of the rolling and cooling operations controls the product properties. Control of grain size is an increasingly important characteristic in hotworking. The narrow temperature range (980°C and 1120°C [1]) for hotworking of Alloy 718 makes the grain size control more difficult. During hotworking, Alloy 718 undergoes microscopic and mesoscopic events such as dynamic recrystallization (DRX), metadynamic recrystallization (MDRX) and static grain growth (SGG) depending on the temperature, strain rate and retained strain. Modeling these microstructural events is important in designing the rolling process. Due to the tremendous amount of time, cost and effort associated with experiments and industrial trials, numerical methods are resorted to because of the complexity of the variables involved in multi-pass rolling. One such popular numerical technique, finite element (FE) method can predict process variables such as strain, strain rate and temperature for the deformation process. In general, microstructural modeling relates these process variables to microstructural evolution. During microstructural modeling, constitutive equations describing the microstructural evolutions are developed using experiments, which can then be readily implemented in an FE package capable of modeling rolling processes.


2015 ◽  
Vol 816 ◽  
pp. 551-556
Author(s):  
Su Gui Tian ◽  
Bao Shuai Wang ◽  
Xin Ding ◽  
De Long Shu ◽  
Jing Wu

Creep behavior of a heat treated single crystal nickel base superalloy containing Re/Ru under the test condition of 1100°C/137MPa high temperatures was investigated. The experimental results showed that the segregation extent of elements in the dendrite and inter-dendrite regions of single crystal superalloy decreases by heat treatment at high temperature. The creep life of the alloy at 1100°C/137MPa was measured to be 321 h displaying a better creep resistance. Wherein, significant amount of fine cubiodal γ′ particles precipitated in the γ matrix channels are considered to be the main reason of the alloy having the better creep resistance. The deformation feature of the alloy during steady state creep is dislocations slipping in the γ matrix and climbing over the rafted γ′ phase. But in the latter stage of creep, the deformation feature of the alloy is dislocations shearing into the rafted γ′ phase. As creep goes on, the main / secondary slipping dislocations in the alloy are alternately activated to result in the initiation and propagation of the cracks along the interface of the rafted γ′/γ phase up to fracture, which is thought to be the fracture mechanism of the alloy during creep.


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