scholarly journals Microstructural Modeling During Multi-Pass Rolling of a Nickel-Base Superalloy

Author(s):  
Kannan Subramanian ◽  
Harish P. Cherukuri

Superalloys are metallic alloys used for high temperature applications such as encountered in the aircraft industry and where resistance to deformation is a primary requirement. Alloy 718 is one such Nickel-base superalloy that resists deformation at elevated temperatures and is therefore difficult to hot work. One of the major hotworking operations is multi-pass shape rolling in which Alloy 718 undergoes multiple deformations in several passes along with reheating between passes. For a given composition of alloy, the high temperature flow stress is influenced to a large extent by the grain size of the microstructure. In the case of shape rolling in which the cross section changes from circular to oval in alternate passes, the correct working forces, which relate to gauge and shape control as well as to power requirements, can be estimated accurately only if the microstructure relevant to the specific pass of rolling is known. In addition, the microstructure present at the end of the rolling and cooling operations controls the product properties. Control of grain size is an increasingly important characteristic in hotworking. The narrow temperature range (980°C and 1120°C [1]) for hotworking of Alloy 718 makes the grain size control more difficult. During hotworking, Alloy 718 undergoes microscopic and mesoscopic events such as dynamic recrystallization (DRX), metadynamic recrystallization (MDRX) and static grain growth (SGG) depending on the temperature, strain rate and retained strain. Modeling these microstructural events is important in designing the rolling process. Due to the tremendous amount of time, cost and effort associated with experiments and industrial trials, numerical methods are resorted to because of the complexity of the variables involved in multi-pass rolling. One such popular numerical technique, finite element (FE) method can predict process variables such as strain, strain rate and temperature for the deformation process. In general, microstructural modeling relates these process variables to microstructural evolution. During microstructural modeling, constitutive equations describing the microstructural evolutions are developed using experiments, which can then be readily implemented in an FE package capable of modeling rolling processes.

Author(s):  
B. H. Kear ◽  
J. M. Oblak

A nickel-base superalloy is essentially a Ni/Cr solid solution hardened by additions of Al (Ti, Nb, etc.) to precipitate a coherent, ordered phase. In most commercial alloy systems, e.g. B-1900, IN-100 and Mar-M200, the stable precipitate is Ni3 (Al,Ti) γ′, with an LI2structure. In A lloy 901 the normal precipitate is metastable Nis Ti3 γ′ ; the stable phase is a hexagonal Do2 4 structure. In Alloy 718 the strengthening precipitate is metastable γ″, which has a body-centered tetragonal D022 structure.Precipitate MorphologyIn most systems the ordered γ′ phase forms by a continuous precipitation re-action, which gives rise to a uniform intragranular dispersion of precipitate particles. For zero γ/γ′ misfit, the γ′ precipitates assume a spheroidal.


2015 ◽  
Vol 658 ◽  
pp. 14-18
Author(s):  
Tanaporn Rojhirunsakool ◽  
Duangkwan Thongpian ◽  
Nutthita Chuankrerkkul ◽  
Panyawat Wangyao

Nickel-base superalloys have been used as high temperature materials in land-base gas turbine application. When subjected to long term, high temperature service, large crack propagation was observed. Typical refurbishment method of these turbines is carried out by using TIG welding followed by post-weld standard heat treatment. However, new crack initiation is found in the heat-affected zone after TIG welding. Pre-weld heat treatment has been discovered to improves final γ + γ’ microstructure. This study focuses on the effect of pre-weld heat treatment temperature on final γ + γ’ microstructure. Seven different conditions of pre-weld heat treatment temperature were investigated. Scanning electron microscopy studies were carried out after pre-weld and post-weld heat treatments to compare the γ + γ’ microstructure and capture microcracks. The best pre-weld heat treatment temperature produces uniform distribution of finely dispersed γ’ precipitates in the γ matrix without post-weld crack.


1986 ◽  
Vol 81 ◽  
Author(s):  
D. M. Shah ◽  
D. N. Duhl

AbstractMulticomponent nickel base intermetallics with the L12 structure were evaluated as high temperature structural materials. The compounds were based on the γ' composition of PWA 1480, a high strength single crystal nickel base superalloy. The best balance of properties in the compound was achieved with <111> oriented single crystals but no significant advantage could be demonstrated over the precipitation hardened superalloys. Insufficient impact resistance was a major deficiency of the L12 compounds. Other nickel base intermetallics were also evaluated but showed little advantage over superalloys.


Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1978 ◽  
Author(s):  
Xianqiang Fan ◽  
Zhipeng Guo ◽  
Xiaofeng Wang ◽  
Jie Yang ◽  
Jinwen Zou

A pre-hot-deformation process was applied for a polycrystalline nickel-base superalloy to active deformation twins and dislocations, and subsequent slow cooling treatment was used to achieve grain refinement and microstructure homogenization. The microstructural evolution of the alloy was investigated, and the corresponding underlying mechanism was discussed. It was found that twinning mainly occurred in large grains during pre-hot-deformation owing to the stress concentration surrounding the large grains. High density dislocations were found in large grains, and the dislocation density increased approaching the grain boundary. The average grain size was refined from 30 μm to 13 μm after slow cooling with a standard deviation of grain size decreasing from 10.8 to 2.8, indicating a homogeneous microstructure. The grain refinement and microstructure homogenization during cooling process could be achieved via (i) static recrystallization (SRX), (ii) interaction of twin tips and γ’ precipitates, and (iii) grain coarsening hindered by γ’ precipitates in grain boundaries.


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