NMR-Untersuchungen an 3,3-Difluor-2-ethyI-1,1,2-tris(diethoxyphosphoryI)-cyclopropan / NMR Investigation of 3,3-Difluoro-2-ethyl-1,1,2-tris(diethoxyphosphoryl)cyclopropane
1986 ◽
Vol 41
(1)
◽
pp. 63-69
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Keyword(s):
The 19F, 31P and 13C NMR spectra in double and triple resonance mode and the temperature dependence of the NMR parameters of the title compound are discussed in detail. The rotational behavior of the phosphoryl groups is described; two of these groups show equal barriers to rotation of 75 kJ mol-1, the third one is rotating freely at room temperature.
1987 ◽
Vol 42
(1)
◽
pp. 115-117
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1997 ◽
Vol 52
(4)
◽
pp. 373-376
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Keyword(s):
1996 ◽
Vol 61
(6)
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pp. 888-900
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1992 ◽
Vol 47
(12)
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pp. 1725-1735
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