Nanomechanical Characterization on Zinc and Tin Oxides Nanobelts

2002 ◽  
Vol 740 ◽  
Author(s):  
Minhua Zhao ◽  
Scott Mao ◽  
Zhong Lin Wang ◽  
Fengting Xu ◽  
John A Barnard

ABSTRACTNanobelts are a group of materials that have a rectangle-like cross section with typical widths of several hundred nanometers, width-to-thickness ratios of 5 to 10, and lengths of hundreds of micron meters. In this paper, nanoindentations were made on individual ZnO, SnO2 nanobelts and (0001) bulk ZnO by using AFM and Hysitron Triboscope indenters. It was shown that the indentation size effect was still obvious for the indentation depth under 50 nm. It is also demonstrated that nanomaching is possible on nanobelt using AFM tip.

2006 ◽  
Vol 312 ◽  
pp. 363-368 ◽  
Author(s):  
Chun Sheng Lu ◽  
Yiu Wing Mai ◽  
Yao Gen Shen

Based on nanoindentation techniques, the evaluation of hardness of two nanostructured thin films, AlN and Ti-Al-N, is discussed. In the case of AlN films, the indentation size effect of hardness can be modeled using the concept of geometrically necessary dislocations, whereas in the case of Ti-Al-N films, the measured hardness increases exponentially as the indentation depth decreases. The results show that, as thin films approach superhard, dislocation-based plastic deformation is gradually replaced by grain-boundary mediated deformation.


2016 ◽  
Vol 25 (5-6) ◽  
pp. 161-164 ◽  
Author(s):  
Asterios K. Kampouris ◽  
Avraam A. Konstantinidis

AbstractThe so-called indentation size effect (ISE) observed mainly in nanoindentation measurements with prismatic tips, is theoretically modeled in this article with the use of gradient theory. It is shown that the ISE, i.e. the dependence of the calculated hardness value on the indentation depth, is rather an artifact of the geometry of the tip used, than a phenomenon related to the material tested. The model predictions are compared with nanoindentation measurements of Al specimens.


2009 ◽  
Vol 24 (5) ◽  
pp. 1693-1699 ◽  
Author(s):  
N. Li ◽  
L. Liu ◽  
K.C. Chan

The deformation behavior and indentation size effect (ISE) in amorphous and crystallized Pd40Cu30Ni10P20 alloy were comparatively studied through instrumented nanoindentation. It was found that the two alloys showed different deformation behaviors, the amorphous alloy exhibited conspicuous pop-in events in the load-depth (P-h) curve, while the crystallized alloy showed a relatively smooth P-h curve. In addition, the indentation hardness was observed to decrease with increasing penetration depth in the two alloys, exhibiting a significant ISE. However, the crystallized alloy displayed a sharper reduction of hardness with indentation depth as compared to the amorphous alloy, indicating a more significant indentation size effect in the crystalline alloy. The structure difference and friction factor associated with the surface residual stress are taken into account to interpret the difference in the deformation behavior and indentation size effect of the two alloys.


Author(s):  
Y. D. Han ◽  
H. Y. Jing ◽  
S. M. L. Nai ◽  
C. M. Tan ◽  
L. Y. Xu ◽  
...  

In the present study, nanoindentation studies of the 95.8Sn-3.5Ag-0.7Cu lead-free solder were conducted over a range of maximum loads from 20mN to 100mN, under a constant ramp rate of 0.05s−1. The indentation scale dependence of hardness was investigated. The results revealed that the hardness is dependent on the indentation depth. As the maximum holding load increased, which corresponded to an increasing indentation depth, a decreasing trend in the hardness was observed.


2019 ◽  
Vol 6 (2) ◽  
pp. 18-00545-18-00545
Author(s):  
Shota HASUNUMA ◽  
Hirohisa MIYAZAKI ◽  
Takeshi OGAWA

2003 ◽  
Vol 86 (3) ◽  
pp. 441-448 ◽  
Author(s):  
George D. Quinn ◽  
Patrice Green ◽  
Kang Xu

Author(s):  
A. Bandini ◽  
D. Chicot ◽  
P. Berry ◽  
X. Decoopman ◽  
A. Pertuz ◽  
...  

1995 ◽  
Vol 10 (11) ◽  
pp. 2908-2915 ◽  
Author(s):  
M. Atkinson

The variation of apparent hardness observed in previously reported Vickers indentation tests of metals is reexamined. Common deseriptions of the effect are shown to be inaccurate: the variation of apparent hardness is monotonic but not simple. The effect is consistent with varying size of a previously postulated “plastic hinge” at the perimeter of the indent. This complexity confers uncertainty on the estimation of characteristic macrohardness from small scale tests. Association of the indentation size effect with friction and with strain hardening is confirmed.


2008 ◽  
Vol 56 (14) ◽  
pp. 3338-3343 ◽  
Author(s):  
Ju-Young Kim ◽  
Seung-Kyun Kang ◽  
Julia R. Greer ◽  
Dongil Kwon

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