scholarly journals The Chalcogenide Compound Fe2SnSe4: Synthesis and Crystal Structure Analysis by Powder X-ray Diffraction

2021 ◽  
Vol 24 (1) ◽  
Author(s):  
Pilar Delgado-Niño ◽  
Cecilia Chacón ◽  
Gustavo Marroquin ◽  
Gerzon E. Delgado
Minerals ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 181 ◽  
Author(s):  
Peter Paufler ◽  
Stanislav K. Filatov

At the dawn of crystal structure analysis, the close personal contact between researchers in Russia and Germany, well documented in the “Zeitschrift für Krystallographie und Mineralogie”, contributed significantly to the evolution of our present knowledge of the crystalline state. The impact of the Russian crystallographer E. S. Fedorov upon German scientists such as A. Schoenflies and P. Groth and the effect of these contacts for Fedorov are highlighted hundred years after the death of the latter. A creative exchange of ideas paved the way for the analysis of crystal structures with the aid of X-ray diffraction.


2007 ◽  
Vol 62 (6) ◽  
pp. 783-790 ◽  
Author(s):  
Carolin Wallenhorst ◽  
Kirill V. Axenov ◽  
Joseph S. M. Samec ◽  
Roland Fröhlich ◽  
Gerhard Erker

Reaction of the doubly deprotonated pyridine 2,6-dicarboxamido ligand (1) with (PCy3)2Cl2 Ru=CHPh (3a) in THF gave a mixture of (lig)(PCy3)Ru=CHPh isomers (4). The pentane soluble N,N,O-4 isomer was isolated by extraction and characterized by X-ray diffraction. The O,N, O-4 isomer was identified in the residue. Single crystals of the closely related complex (lig)(NHC) Ru=CHPh, O,N,O-5, were obtained from the reaction of 1 with (NHC)(PCy3)Cl2Ru=CHPh (3b) and used for the X-ray crystal structure analysis of the system


1995 ◽  
Vol 242 (3-4) ◽  
pp. 360-364 ◽  
Author(s):  
J. Akimoto ◽  
Y. Oosawa ◽  
K. Tokiwa ◽  
M. Hirabayashi ◽  
H. Ihara

The Fourier representation of the results of X-ray diffraction by crystals was first suggested by W. H. Bragg,** and later it was used by Havighurst and Compton† to obtain the distribution of scattering matter in crystals. W. L. Bragg‡ developed the two-dimensional representation of the Fourier series into a very convenient method of crystal analysis. He considered crystals having a centre of symmetry where it can be shown that if a projection of the atoms on the yz plane be considered the density of scattering matter per unit area of projection at the point y , z is given by


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